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1. 发明申请

WO2008046816A1 PROCESS FOR STABILIZING FLUOROPOLYMER HAVING ION EXCHANGE GROUPS 审中-公开
标题翻译：具有离子交换聚合物稳定氟聚合物的方法
公开(公告)号：WO2008046816A1
公开(公告)日：2008-04-24
申请号：PCT/EP2007/060986
申请日：2007-10-16
申请人： SOLVAY SOLEXIS S.p.A. , ARCELLA, Vincenzo , CIRILLO, Luca , GHIELMI, Alessandro , MERLO, Luca , MILLEFANTI, Stefano
发明人： ARCELLA, Vincenzo , CIRILLO, Luca , GHIELMI, Alessandro , MERLO, Luca , MILLEFANTI, Stefano
IPC分类号： C08F8/22 , C08F14/18 , C08J5/22
CPC分类号： C08J5/2237 , C08F8/22 , C08F214/18 , C08F214/26 , C08J2327/18 , H01M8/1023 , H01M8/1025 , H01M8/1039 , H01M8/1072 , H01M2300/0082 , Y02P70/56
摘要： The invention pertains to a process for stabilizing a semi-crystalline fluoropolymer comprising ion exchange groups, said process comprising: suspending at least one semi-crystalline fluoropolymer having ion exchange groups [polymer (I)] in at least one fluorinated organic dispersing medium [medium (M)] so as to obtain a dispersion (D) of polymer (I) in a dispersing medium (M); contacting said dispersion (D) with fluorine under irradiation with U. V. radiation so as to obtain a stabilized polymer. Still objects of the invention are a stable semi-crystalline fluoropolymer as above defined having a low amount of unstable ends groups of -COF type, the use of the stabilized fluoropolymer obtained by the process or of the stable fluoropolymer in fuel cells devices, a membrane and a membrane-electrode assembly comprising said fluoropolymers.
摘要翻译：本发明涉及一种稳定包含离子交换基团的半结晶含氟聚合物的方法，所述方法包括：在至少一种氟化有机分散介质[介质中]悬浮至少一种具有离子交换基团[聚合物（I）]的半结晶含氟聚合物（M）]，得到分散介质（M）中的聚合物（I）的分散液（D）。在用U.V辐射照射下使所述分散体（D）与氟接触，以获得稳定的聚合物。本发明的另一目的是如上定义的稳定的半结晶含氟聚合物，其具有少量-COF型的不稳定端基，通过该方法获得的稳定的含氟聚合物或在燃料电池装置中使用稳定的含氟聚合物，膜以及包含所述含氟聚合物的膜 - 电极组件。

2. 发明申请

WO2008077894A1 PROCESS FOR OPERATING A FUEL CELL IN DRY CONDITIONS 审中-公开
标题翻译：在干燥条件下操作燃料电池的方法
公开(公告)号：WO2008077894A1
公开(公告)日：2008-07-03
申请号：PCT/EP2007/064360
申请日：2007-12-20
申请人： SOLVAY SOLEXIS S.p.A. , ARCELLA, Vincenzo , GHIELMI, Alessandro , MERLO, Luca
发明人： ARCELLA, Vincenzo , GHIELMI, Alessandro , MERLO, Luca
IPC分类号： H01M8/10 , H01M8/04 , C08J5/22
CPC分类号： C08J5/2237 , C08J2327/18 , H01M8/04007 , H01M8/04089 , H01M8/04126 , H01M8/1025 , H01M8/1039 , H01M8/1067
摘要： The invention pertains to a process for operating a polymer electrolyte membrane fuel cell (PEMFC), said PEMFC comprising:(a) a membrane comprising at least one fluorinated ionomer [polymer (I)] comprising recurring units derived from tetrafluoroethylene (TFE) and from at least one monomer of formula (M): wherein m is an integer between 1 and 6 and X' is chosen among halogens (Cl, F, Br, I), -O - M + , wherein M + is a cation selected among H + , NH 4 + , K + , Li + , Na + or mixtures thereof, said polymer (I) having an equivalent weight (EW) of from 700 to 850 g/eq.; (b) a cathode; (c) an anode; said process comprising: (i) feeding gaseous reactants at the electrodes at a relative humidity of at most 66 %; (ii) maintaining an average current density between 0.05 and 1.5 A/cm 2 ; and(iii) maintaining an average temperature of more than 65 °C.
摘要翻译：本发明涉及一种操作聚合物电解质膜燃料电池（PEMFC）的方法，所述PEMFC包括：（a）包含至少一种氟化离聚物[聚合物（I）]的膜，其包含衍生自四氟乙烯（TFE）的重复单元和至少一种式（M）的单体：其中m是1至6之间的整数，X'选自卤素（Cl，F，Br，I），-O - +，其中M + +是选自H +，NH 4 +，SO 2 +的阳离子，

3. 发明申请

WO2010142772A1 FLUOROIONOMERS DISPERSIONS HAVING LOW SURFACE TENSION, LOW LIQUID VISCOSITY AND HIGH SOLID CONTENT 审中-公开
标题翻译：具有低表面张力，低液体粘度和高固体含量的荧光剂分散体
公开(公告)号：WO2010142772A1
公开(公告)日：2010-12-16
申请号：PCT/EP2010/058182
申请日：2010-06-10
申请人： SOLVAY SOLEXIS S.p.A. , MERLO, Luca , GHIELMI, Alessandro , ARCELLA, Vincenzo
发明人： MERLO, Luca , GHIELMI, Alessandro , ARCELLA, Vincenzo
IPC分类号： C08F8/22 , C08J5/22 , H01M8/10
CPC分类号： H01M8/1039 , B01J39/20 , C08J5/2281 , C08J2327/18 , H01M8/1025 , H01M8/106 , H01M8/1062 , H01M2008/1095 , H01M2300/0082 , Y02E60/523 , Y02P70/56 , Y10T428/24752
摘要： The invention pertains to a process for manufacturing certain (per)fluoroionomer liquid compositions, comprising, inter alia, at least one of fluorination and treatment with a polar solvent, to the liquid compositions therefrom having an improved solids content/surface tension/liquid viscosity compromise, to the use of the same for manufacturing composite membranes and to composite membranes obtainable therefrom.
摘要翻译：本发明涉及用于制造某些（全）氟代离聚物液体组合物的方法，其特别包括氟极化和极性溶剂处理中的至少一种，其具有改进的固体含量/表面张力/液体粘度损害的液体组合物，使用它们制造复合膜和可从其获得的复合膜。

4. 发明申请

WO2008000718A1 ASSEMBLIES FOR ELECTROCHEMICAL DEVICES 审中-公开
标题翻译：电化学装置组装
公开(公告)号：WO2008000718A1
公开(公告)日：2008-01-03
申请号：PCT/EP2007/056318
申请日：2007-06-25
申请人： SOLVAY SOLEXIS S.p.A. , ARCELLA, Vincenzo , MERLO, Luca , GHIELMI, Alessandro
发明人： ARCELLA, Vincenzo , MERLO, Luca , GHIELMI, Alessandro
IPC分类号： H01M8/24 , H01M8/02 , H01M8/10 , H01M2/14
CPC分类号： H01M8/1004 , H01M4/8605 , H01M4/90 , H01M4/921 , H01M4/926 , H01M8/0234 , H01M8/0239 , H01M8/0243 , H01M8/0271 , H01M8/0289 , H01M8/1023 , H01M8/1025 , H01M8/1039 , H01M8/1067 , H01M8/1093 , Y02E60/521 , Y02P70/56
摘要： MEA 7-layer assemblies with gasket, comprising: - a film of ionomeric membrane (3), containing functional acid groups -SO 3 H and/or -COOH, having in at least one direction, called direction x, a size variation lower than 0.08%; - two GDL sheets (1) and (2) in porous material having on one surface an electrocatalytic layer, not shown in the Figures, of which: - the first sheet DGL (1) is coextensive with the membrane (3) surface, positioned so as to overlap thereto; - the second sheet GDL (2), having a lower width but the same length of the film of membrane (3), measured in the x direction; - the two sheets (1) and (2) placed so that the electrocatalytic layer comes into contact, respectively, with each of the two membrane faces; - a gasket positioned according to a frame shape along the assembly perimeter.
摘要翻译：具有垫圈的MEA 7层组件包括： - 离子交换膜（3）的膜，其含有至少一个方向的官能酸基-SO 3 H和/或-COOH，称为方向 x，尺寸变化小于0.08％; - 多孔材料中的两个GDL片（1）和（2）在一个表面上具有电催化层，图中未示出，其中： - 第一片DGL（1）与膜（3）表面共同延伸，定位以便与之重叠; - 第二片材GDL（2），其在x方向上测量的膜（3）的膜的宽度较低但长度相同; - 将两个片（1）和（2）放置成使得电催化层分别与两个膜面中的每一个接触; - 沿着组件周边根据框架形状定位的垫圈。

5. 发明申请

WO2008000724A1 ASSEMBLIES FOR ELECTROCHEMICAL DEVICES 审中-公开
标题翻译：电化学装置组装
公开(公告)号：WO2008000724A1
公开(公告)日：2008-01-03
申请号：PCT/EP2007/056328
申请日：2007-06-25
申请人： SOLVAY SOLEXIS S.p.A. , ARCELLA, Vincenzo , MERLO, Luca , GHIELMI, Alessandro
发明人： ARCELLA, Vincenzo , MERLO, Luca , GHIELMI, Alessandro
IPC分类号： H01M8/24 , H01M8/02 , H01M8/10 , H01M2/14
CPC分类号： H01M4/921 , H01M4/8605 , H01M4/90 , H01M4/926 , H01M8/0234 , H01M8/0239 , H01M8/0243 , H01M8/0271 , H01M8/1004 , H01M8/1018 , H01M8/1023 , H01M8/1039 , H01M8/1067 , H01M8/1093 , Y02P70/56
摘要： 7-layer MEA assemblies with gasket, comprising: - a film of ionomeric membrane (3) having size variations in the two orthogonal plane directions, x and y, lower than 4%, determined according to the formula: (A-B)x100/B, wherein: - B is the membrane length in the x or y direction, after drying under vacuum for a time of 1 h at 105°C and at a residual pressure lower than 30 mBar; - A is the membrane length in the same direction where B is measured after membrane treatment in distilled water at 100°C for 30 minutes; - two GDL sheets (1) and (2) made of a porous material having on one surface an electrocatalytic layer coextensive with the membrane (3) sur- face; - the two sheets (1) and (2) positioned so that the electrocatalytic layer comes into contact, respectively, with each of the two membrane faces; - a gasket (4) positioned according to a frame shape along the assembly perimeter.
摘要翻译：具有垫圈的7层MEA组件，包括： - 根据以下公式确定在两个正交平面方向上具有尺寸变化的离聚物膜（3）的薄膜，x和y低于4％，（AB）×100 / B 其中：-B是在真空下干燥1个小时，105℃，残余压力低于30mBar的x或y方向的膜长度; - A是在100℃下在蒸馏水中处理30分钟后，在相同方向上测量B的膜长度; - 两个由多孔材料制成的GDL片（1）和（2），其在一个表面上具有与膜（3）表面共同延伸的电催化层; - 两个片（1）和（2）被定位成使得电催化层分别与两个膜面中的每一个接触; - 沿着组装周边根据框架形状定位的垫圈（4）。

6. 发明申请

WO2008000719A1 ASSEMBLIES FOR ELECTROCHEMICAL DEVICES 审中-公开
标题翻译：电化学装置组装
公开(公告)号：WO2008000719A1
公开(公告)日：2008-01-03
申请号：PCT/EP2007/056320
申请日：2007-06-25
申请人： SOLVAY SOLEXIS S.P.A. , ARCELLA, Vincenzo , MERLO, Luca , GHIELMI, Alessandro
发明人： ARCELLA, Vincenzo , MERLO, Luca , GHIELMI, Alessandro
IPC分类号： H01M8/24 , H01M8/02 , H01M8/10 , H01M2/14
CPC分类号： H01M8/1004 , H01B1/122 , H01M4/8605 , H01M8/0234 , H01M8/0239 , H01M8/0243 , H01M8/0245 , H01M8/0271 , H01M8/0273 , H01M8/0276 , H01M8/0284 , H01M8/0286 , H01M8/1023 , H01M8/1039 , H01M8/1067 , H01M8/1093 , H01M2300/0082 , Y02P70/56
摘要： 7-layer MEA assemblies with gasket, comprising: a film of ionomeric membrane (3) having size variations in the two orthogonal planedirections, x and y, lower than 4%, determined by the (A-B)x100/B ratio wherein: B is the membrane length in the x or y direction, after drying under vacuum for a time of 1 h at 105°C and at a residual pressure lower than 30 mBar; A is the membrane length in the same direction in which B is measured after treatment in distilled water at 100°C for 30 minutes; two GDL sheets (1) and (2) made of porous material having on one surface an electrocatalytic layer, of which: one (1 ) coextensive with the membrane (3) surface; the second one (2) having a length equal to that of the film of membrane (3), measured in the x direction, and lower width; the two sheets (1 ) and (2) positioned so that the electrocatalytic layer comes into contact, respectively, with each of the two membrane faces; a gasket (4) disposed according to a frame shape along the assembly perimeter covering the two uncovered strips of membrane (3) parallel to the x direction.
摘要翻译：具有垫圈的7层MEA组件包括：由（AB）×100 / B比确定的在两个正交平面方向上具有尺寸变化的离聚物膜（3）的膜，x和y低于4％，其中：B是膜长度在x或y方向，在真空下干燥1个小时，105℃，残余压力低于30mBar; A是在100℃下在蒸馏水中处理30分钟后测量B的相同方向的膜长度; 由多孔材料制成的两个GDL片（1）和（2）在一个表面上具有电催化层，其中：一（1）与膜（3）表面共同延伸; 第二个（2）的长度等于膜（3）的膜的长度，在x方向上测量，并且具有较低的宽度; 所述两片（1）和（2）分别定位成使得所述电催化层分别与所述两个膜面中的每一个接触; 沿着组装周边的框架形状布置的垫片（4），其覆盖平行于x方向的膜（3）的两个未覆盖条带。

7. 发明申请

WO2008000709A1 CATALYST-POLYMER LIQUID DISPERSION FOR FUEL CELL APPLICATIONS 审中-公开
标题翻译：用于燃料电池应用的催化聚合物液体分散体
公开(公告)号：WO2008000709A1
公开(公告)日：2008-01-03
申请号：PCT/EP2007/056291
申请日：2007-06-25
申请人： SOLVAY SOLEXIS S.P.A. , GHIELMI, Alessandro , MERLO, Luca , NUCIDA, Gilberto , ARCELLA, Vincenzo
发明人： GHIELMI, Alessandro , MERLO, Luca , NUCIDA, Gilberto , ARCELLA, Vincenzo
IPC分类号： H01M8/10
CPC分类号： H01M4/881 , H01M4/8828 , H01M4/92 , H01M4/926 , H01M2300/0082
摘要： Catalyst-polymer liquid dispersion (LD) comprising (i) catalyst particles, (ii) polymer particles consisting of at least one (per)fluoro sulfonyl fluoride polymer in the -SO 2 F form, and (iii) an aqueous suspending medium. Catalyst coated membrane precursor (CCMP), catalyst coated membrane (CCM) and catalytic ionomeric ink (CII) derived therefrom and methods for their manufacture. Catalyst coated membrane (CCM-CII) derived from said (CII).
摘要翻译：催化剂 - 聚合物液体分散体（LD），其包含（i）催化剂颗粒，（ii）由-SO 2 2 F形式的至少一种（全）氟磺酰氟聚合物组成的聚合物颗粒，和（iii ）水性悬浮介质。催化剂涂覆膜前体（CCMP），催化剂涂覆膜（CCM）和催化离聚物油墨（CII）及其制备方法。衍生自所述（CII）的催化剂涂覆膜（CCM-CII）。

8. 发明申请

WO2007116031A1 POLYMERISATION PROCESS 审中-公开
标题翻译：聚合过程
公开(公告)号：WO2007116031A1
公开(公告)日：2007-10-18
申请号：PCT/EP2007/053418
申请日：2007-04-06
申请人： SOLVAY SOLEXIS S.P.A. , ARCELLA, Vincenzo , KAPELIOUCHKO, Valeri , FERRERO, Stefano , GARGIULO, Aniello
发明人： ARCELLA, Vincenzo , KAPELIOUCHKO, Valeri , FERRERO, Stefano , GARGIULO, Aniello
IPC分类号： C08F14/18 , C08F2/01 , B01F7/00
CPC分类号： C08F2/01 , B01F7/00975 , B01F7/166 , B01F7/1665 , C08F14/18 , C08F14/26 , Y10S526/918 , C08F2/02
摘要： The invention pertains to a polymerisation process for the manufacture of a fluoropolymer [polymer (F)], said process comprising polymerising at least one fluorinated monomer in a polymerization medium, wherein said polymerization medium is mixed by means of a stirring system comprising at least two counter-rotating impellers. It has been surprisingly observed that the polymerization advantageously occurs without fouling or deposit formation on the reactor walls. Moreover, the polymerization process advantageously occurs with improved homogeneity, without composition, pressure or temperature gradients, thus enabling obtaining homogeneous polymer composition with no risk of local overheating. Finally, polymer (F) obtained from the process of the invention possesses advantageously improved morphology (percentage of organized structures, i.e. of particles of regular shape) and, hence, advantageously good free flowing properties which make it suitable for being processed by compression moulding with no need of intermediate milling or grinding process or other size reduction process. Still objects of the invention are a fluoropolymer [polymer (F)], and a moulding process.
摘要翻译：本发明涉及用于制造含氟聚合物[聚合物（F）]的聚合方法，所述方法包括在聚合介质中聚合至少一种氟化单体，其中所述聚合介质通过包含至少两个反向旋转叶轮已经令人惊讶地观察到聚合有利地在反应器壁上没有污垢或沉积物形成。此外，聚合方法有利地在没有组成，压力或温度梯度的情况下具有改进的均匀性，因此能够获得均匀的聚合物组合物，而没有局部过热的风险。最后，从本发明方法获得的聚合物（F）具有有利地改进的形态（有组织结构的百分比，即规则形状的颗粒的百分比），并且因此有利地是良好的自由流动性，使其适合于通过压缩模塑加工不需要中间铣削或磨削加工或其他尺寸缩小工艺。本发明的另一个目的是含氟聚合物[聚合物（F）]和成型工艺。

9. 发明申请

WO2008122619A1 SOLAR CELL MODULE 审中-公开
标题翻译：太阳能电池模块
公开(公告)号：WO2008122619A1
公开(公告)日：2008-10-16
申请号：PCT/EP2008/054117
申请日：2008-04-04
申请人： SOLVAY SOLEXIS S.p.A. , TONIOLO, Paolo , SRINIVASAN, Padmanabhan , MARRANI, Alessio , BESANA, Giambattista , ARCELLA, Vincenzo
发明人： TONIOLO, Paolo , SRINIVASAN, Padmanabhan , MARRANI, Alessio , BESANA, Giambattista , ARCELLA, Vincenzo
IPC分类号： H01L31/048 , H01L31/0216 , C09K3/10 , C08J7/04 , H01L31/075
CPC分类号： H02S50/15 , B32B27/322 , H01L31/048 , H01L31/0481 , Y02E10/50
摘要： The present invention pertains to a solar cell module comprising at least one photovoltaic element (4) encapsulated between a front layer (3) on its light- receiving surface side and a back layer (3), said front layer comprising at least one layer comprising a tetrafluoroethylene (TFE).polymer [polymer (F)], said polymer (F) comprising: - recurring units derived from TFE; and - from 15 to 25 % wt of recurring units derived from at least one perfluoromonomer [monomer (CM)] chosen among: ' (i) perfluoroalkylvinylethers complying with formula CF
摘要翻译：本发明涉及一种太阳能电池模块，其包括封装在其光接收表面侧上的前层（3）和背层（3）之间的至少一个光电元件（4），所述前层包括至少一层包含四氟乙烯（TFE）聚合物[聚合物（F）]，所述聚合物（F）包含： - 衍生自TFE的重复单元; 和 - 至少一种全氟单体[单体（CM）]衍生的重复单元的15至25重量％，其选自：（i）符合式CF的全氟烷基乙烯基醚

10. 发明申请

WO2007096348A1 CABLES HAVING A LOW SMOKE RELEASE 审中-公开
标题翻译：具有低烟雾释放的电缆
公开(公告)号：WO2007096348A1
公开(公告)日：2007-08-30
申请号：PCT/EP2007/051592
申请日：2007-02-20
申请人： SOLVAY SOLEXIS S.P.A. , ABUSLEME, Julio A. , ARCELLA, Vincenzo , ZANGARA, Anthony V
发明人： ABUSLEME, Julio A. , ARCELLA, Vincenzo , ZANGARA, Anthony V
IPC分类号： C08L27/12 , C08K3/00 , H01B3/44
CPC分类号： H01B3/445
摘要： Cables comprising: primary cables coated by a perfluoropolymer; and a jacket formed of a polymeric composition comprising: (A) an ethylene, tetrafluoroethylene (TFE) and/or chlorotrifluoroethylene (CTFE) copolymer, and one or more hydrogenated monomers; (B) one or more inorganic fire-retardants, optionally treated with dispersing agents.
摘要翻译：电缆包括：由全氟聚合物涂覆的主电缆; 和由聚合物组合物形成的护套，其包含：（A）乙烯，四氟乙烯（TFE）和/或三氟氯乙烯（CTFE）共聚物和一种或多种氢化单体; （B）一种或多种无机阻燃剂，任选用分散剂处理。

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