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1. 发明申请

WO2006067190A1 PROCESS FOR THE MANUFACTURE OF 1,2-DICHLOROETHANE 审中-公开
标题翻译： 1,2-二氯乙烷的制备方法
公开(公告)号：WO2006067190A1
公开(公告)日：2006-06-29
申请号：PCT/EP2005/057045
申请日：2005-12-21
申请人： SOLVAY (Société Anonyme) , BALTHASART, Dominique , STREBELLE, Michel , LEMPEREUR, Michel
发明人： BALTHASART, Dominique , STREBELLE, Michel , LEMPEREUR, Michel
IPC分类号： C07C17/02 , C07C17/156 , C07C19/045 , C07C17/25 , C07C21/06 , C08F14/06
CPC分类号： C07C21/06 , C07C17/02 , C07C17/156 , C07C17/25 , C07C19/045 , Y02P20/582
摘要： Process for the manufacture of 1,2-dichloroethane starting with a hydrocarbon source according to which : a) the hydrocarbon source is subjected to cracking which produces a mixture of products containing ethylene and other constituents; b) the mixture of products containing ethylene is conveyed to at least one storage reservoir; c) a chlorination reactor and/or an oxychlorination reactor is (are) supplied with the previously stored mixture of products containing ethylene, in which reactors most of the ethylene present is converted to 1,2-dichloroethane; d) the 1,2-dichloroethane obtained is separated from the streams of products derived from the chlorination and oxychlorination reactors.
摘要翻译：从烃源开始制造1,2-二氯乙烷的方法，其中：a）烃源受到裂化，产生含乙烯和其它组分的产物的混合物; b）含有乙烯的产品的混合物被输送到至少一个储存容器; c）氯化反应器和/或氧氯化反应器与先前储存的含乙烯的产物混合物供应，其中大部分乙烯转化为1,2-二氯乙烷; d）将得到的1,2-二氯乙烷与衍生自氯化和氧氯化反应器的产物流分离。

2. 发明申请

WO2009147101A1 PROCESS FOR THE MANUFACTURE OF AT LEAST ONE ETHYLENE DERIVATIVE COMPOUND 审中-公开
标题翻译：至少一种乙烯衍生化合物的制造方法
公开(公告)号：WO2009147101A1
公开(公告)日：2009-12-10
申请号：PCT/EP2009/056640
申请日：2009-05-29
申请人： SOLVAY (Société Anonyme) , PETITJEAN, André , LEMPEREUR, Michel , BALTHASART, Dominique , STREBELLE, Michel
发明人： PETITJEAN, André , LEMPEREUR, Michel , BALTHASART, Dominique , STREBELLE, Michel
IPC分类号： C07C17/02 , C07C17/156 , C07C17/25 , C07C19/045 , C07C21/06
CPC分类号： C07C19/045 , C07C17/02 , C07C17/156 , C07C17/25 , Y02P20/582 , C07C21/06
摘要： Process for the manufacture of at least one ethylene derivative compound starting from a low value residual gas, preferably a ROG, according to which : a) the low value residual gas is subjected to a series of treatment steps in a low value residual gas recovery unit in order to remove the undesirable components present therein and to obtain a mixture of products containing ethylene and other constituents; b) the said mixture of products is fractionated in one fractionation step into one fraction containing almost all the ethylene (fraction A), optionally into one individual fraction of ethane and into one heavy fraction (fraction C); and c) fraction A is conveyed to the manufacture of at least one ethylene derivative compound.
摘要翻译：用于从低值残留气体（优选ROG）开始制造至少一种乙烯衍生物的方法，其中：a）低值残留气体在低值残余气体回收单元中进行一系列处理步骤以除去其中存在的不期望的组分并获得含有乙烯和其它组分的产物的混合物; b）将所述产物混合物在一个分馏步骤中分馏成含有几乎所有乙烯（馏分A）的一个馏分，任选地加入一个单独的乙烷馏分中，并分成一个重馏分（馏分C）; 和c）馏分A被输送至制造至少一种乙烯衍生物化合物。

3. 发明申请

WO2009147076A2 PROCESS FOR THE PRODUCTION OF LOW-CONCENTRATION ETHYLENE FOR CHEMICAL USE 审中-公开
标题翻译：生产用于化学使用的低浓度乙烯的方法
公开(公告)号：WO2009147076A2
公开(公告)日：2009-12-10
申请号：PCT/EP2009/056577
申请日：2009-05-28
申请人： SOLVAY (Société Anonyme) , KOTTER, Joachim , WINKLER, Hans-Dieter , MEWS, Peter , LEMPEREUR, Michel , BALTHASART, Dominique , STREBELLE, Michel
发明人： KOTTER, Joachim , WINKLER, Hans-Dieter , MEWS, Peter , LEMPEREUR, Michel , BALTHASART, Dominique , STREBELLE, Michel
IPC分类号： C07C11/04 , C10G9/00 , C10G65/04 , C10G70/04
CPC分类号： F25J3/0238 , C07C4/04 , C07C11/04 , C10G2300/1044 , C10G2300/1059 , C10G2300/1081 , C10G2400/20 , F25J3/0219 , F25J3/0252 , F25J2200/02 , F25J2200/74 , F25J2210/12 , F25J2215/62 , F25J2270/02 , Y02P30/40 , Y02P30/44 , Y02P30/462
摘要： Process for the production of ethylene for chemical use starting with a hydrocarbon source according to which: a) the hydrocarbon source is subjected to a first cracking step, namely a pyrolysis step carried out in a cracking oven, thus producing a mixture of cracking products; b) the said mixture of cracking products is subjected to a succession of treatment steps, including a compression step, which makes it possible to obtain a purified crude gas stream; c) the purified crude gas stream is then cooled to a temperature where hydrocarbons with 6 and more carbon atoms condense so that they can be removed from the purified crude gas stream; d) the resulting purified gas stream is afterwards supplied to one separating column, where a fraction containing hydrogen, methane and ethylene (fraction A) is separated at the head of the column and a heavy fraction (fraction C) is separated at the bottom of the column; e) a part of the reflux of this column is supplied to a refrigeration cycle leading to a fraction enriched with ethylene (fraction B); f) fraction A and fraction B are separately supplied to chemical use of ethylene.
摘要翻译：从烃源开始生产用于化学用途的乙烯的方法，其中：a）烃源经受第一裂化步骤，即在裂化炉中进行的热解步骤，从而产生裂化产物的混合物; b）所述裂化产物混合物经受一系列处理步骤，包括压缩步骤，这使得可以获得纯化的粗气流; c）然后将纯化的粗气流冷却至具有6个或更多个碳原子的烃冷凝的温度，使得它们可以从纯化的粗气流中除去; d）将所得纯化气流随后供给至一个分离塔，其中含有氢，甲烷和乙烯（馏分A）的馏分在塔头分离，重馏分（馏分C）在塔底部分离列; e）将该塔的一部分回流供给到导致富含乙烯（馏分B）的馏分的制冷循环中; f）馏分A和馏分B分别供给乙烯的化学用途。

4. 发明申请

WO2009106479A1 PROCESS FOR THE MANUFACTURE OF AT LEAST ONE ETHYLENE DERIVATIVE COMPOUND 审中-公开
标题翻译：至少一种乙烯衍生化合物的制造方法
公开(公告)号：WO2009106479A1
公开(公告)日：2009-09-03
申请号：PCT/EP2009/052005
申请日：2009-02-20
申请人： SOLVAY (Société Anonyme) , PETITJEAN, Andre , LEMPEREUR, Michel , BALTHASART, Dominique , STREBELLE, Michel , GIANSANTE, Massimo
发明人： PETITJEAN, Andre , LEMPEREUR, Michel , BALTHASART, Dominique , STREBELLE, Michel , GIANSANTE, Massimo
IPC分类号： C07C17/02 , C07C17/156 , C07C17/25 , C07C19/045 , C07C21/06
CPC分类号： C07C19/045 , C07C17/02 , C07C17/156 , C07C17/25 , Y02P20/582 , C07C21/06
摘要： Process for the manufacture of at least one ethylene derivative compound starting from a low value residual gas, preferably a ROG, according to which : a) the low value residual gas is subjected to a series of treatment steps in a low value residual gas recovery unit in order to remove the undesirable components present therein and to obtain a mixture of products containing ethylene and other constituents; b) the said mixture of products is separated into a fraction enriched with compounds which are lighter than ethylene, containing part of the ethylene (fraction A), into a fraction enriched with ethylene (fraction B) and into a heavy fraction (fraction C); c) fraction A and fraction B are separately conveyed to the manufacture of at least one ethylene derivative compound.
摘要翻译：用于从低值残留气体（优选ROG）开始制造至少一种乙烯衍生物的方法，其中：a）低值残留气体在低值残余气体回收单元中进行一系列处理步骤以除去其中存在的不期望的组分并获得含有乙烯和其它组分的产物的混合物; b）将所述产物混合物分离成富含化合物的馏分，所述化合物比乙烯轻，含有部分乙烯（馏分A））成为富含乙烯（馏分B）的馏分和重馏分（馏分C） ; c）馏分A和馏分B分别输送至制造至少一种乙烯衍生物化合物。

5. 发明申请

WO2009147100A1 PROCESS FOR THE MANUFACTURE OF 1,2-DICHLOROETHANE AND OF AT LEAST ONE ETHYLENE DERIVATIVE COMPOUND DIFFERENT FROM 1,2-DICHLOROETHANE 审中-公开
标题翻译： 1,2-二氯乙烷的制备方法和至少一种1,2-二氯乙烷的乙烯衍生物化合物的制备方法
公开(公告)号：WO2009147100A1
公开(公告)日：2009-12-10
申请号：PCT/EP2009/056638
申请日：2009-05-29
申请人： SOLVAY (Société Anonyme) , LEMPEREUR, Michel , BALTHASART, Dominique , STREBELLE, Michel , GIANSANTE, Massimo
发明人： LEMPEREUR, Michel , BALTHASART, Dominique , STREBELLE, Michel , GIANSANTE, Massimo
IPC分类号： C07C4/04 , C07C7/04 , C07C11/04 , C07C17/02 , C07C19/045
CPC分类号： C07C17/02 , C07C17/25 , C07C19/045 , C07C21/06 , Y02P20/582
摘要： Process for the manufacture of 1,2-dichlorethane and of at least one ethylene derivative compound which is different from 1,2-dichloroethane starting with a hydrocarbon source according to which : a) the hydrocarbon source is subjected to a simplified cracking which produces a mixture of products containing ethylene and other constituents; b) the said mixture of products is separated at least into a fraction enriched with compounds which are lighter than ethylene, containing part of the ethylene (fraction A), into a fraction enriched with ethylene (fraction B) and into a heavy fraction (fraction C); c) one fraction among fraction A and fraction B is conveyed to the manufacture of 1,2-dichloroethane and optionally of any compound derived there from, optionally after having been subjected to an acetylene hydrogenation, while the other fraction is conveyed to the manufacture of at least one ethylene derivative compound manufactured directly starting with ethylene which is different from 1,2-dichloroethane and optionally of any compound derived there from.
摘要翻译：制备1,2-二氯乙烷和至少一种不同于1,2-二氯乙烷的乙烯衍生物化合物的起始烃源的方法，其中：a）烃源经受简化的裂化，产生一种含乙烯和其他成分的产品混合物; b）将所述产物混合物至少分离成富含化合物的馏分，所述化合物比乙烯轻（含有部分乙烯（馏分A））的化合物加入富含乙烯（馏分B）的馏分中并加入重馏分 C）; c）馏分A和馏分B中的一个馏分被输送到制备1,2-二氯乙烷和任选地由任选地在其进行乙炔氢化之后衍生的任何化合物，而另一部分被输送到制造至少一种乙烯衍生物化合物直接从不同于1,2-二氯乙烷的乙烯开始，以及任选地衍生自其中的任何化合物。

6. 发明申请

WO2009147083A1 PROCESS FOR THE MANUFACTURE OF AT LEAST ONE ETHYLENE DERIVATIVE COMPOUND 审中-公开
标题翻译：至少一种乙烯衍生化合物的制造方法
公开(公告)号：WO2009147083A1
公开(公告)日：2009-12-10
申请号：PCT/EP2009/056600
申请日：2009-05-29
申请人： SOLVAY (Société Anonyme) , LEMPEREUR, Michel , BALTHASART, Dominique , STREBELLE, Michel , KÖTTER, Joachim , WINKLER, Hans-Dieter , MEWS, Peter
发明人： LEMPEREUR, Michel , BALTHASART, Dominique , STREBELLE, Michel , KÖTTER, Joachim , WINKLER, Hans-Dieter , MEWS, Peter
IPC分类号： C07C17/02 , C07C17/156 , C07C17/25 , C07C19/045 , C07C21/06
CPC分类号： C07C21/06 , C07C17/02 , C07C17/156 , C07C17/25 , Y02P20/582 , C07C19/045
摘要： Process for the manufacture of at least one ethylene derivative compound starting with a hydrocarbon source according to which : a) the hydrocarbon source is subjected to a simplified cracking which produces a mixture of products containing ethylene and other constituents; b) the said mixture of products is fractionated in one fractionation step into one fraction containing almost all the ethylene (fraction A), optionally into one individual fraction of ethane and into one heavy fraction (fraction C); and c) fraction A is conveyed to the manufacture of at least one ethylene derivative compound.
摘要翻译：用于从烃源开始制造至少一种乙烯衍生物的方法，其中：a）烃源经受简化的裂解，产生含乙烯和其它组分的产物的混合物; b）将所述产物混合物在一个分馏步骤中分馏成含有几乎所有乙烯（馏分A）的一个馏分，任选地加入一个单独的乙烷馏分中，并分成一个重馏分（馏分C）; 和c）馏分A被输送至制造至少一种乙烯衍生物化合物。

7. 发明申请

WO2007147870A1 PROCESS FOR THE MANUFACTURE OF 1,2-DICHLOROETHANE 审中-公开
标题翻译： 1,2-二氯乙烷的制备方法
公开(公告)号：WO2007147870A1
公开(公告)日：2007-12-27
申请号：PCT/EP2007/056187
申请日：2007-06-21
申请人： SOLVAY (Société Anonyme) , BALTHASART, Dominique , LEMPEREUR, Michel , STREBELLE, Michel
发明人： BALTHASART, Dominique , LEMPEREUR, Michel , STREBELLE, Michel
IPC分类号： C07C17/02 , C07C17/156 , C08F14/06 , C07C17/25
CPC分类号： C08F14/06 , C07C17/02 , C07C17/156 , C07C17/25 , C07C19/045 , C07C21/06 , C08F2/00 , C08F14/12 , Y02P20/582
摘要： Process for the manufacture of DCE starting with a hydrocarbon source according to which: a) the hydrocarbon source is subjected to a first cracking step, namely a pyrolysis step carried out in at least one cracking furnace, thus producing a mixture of cracking products; b) said mixture of cracking products is subjected to a series of treatment steps making it possible to obtain a mixture of products containing ethylene and other constituents; c) said mixture of products containing ethylene is subjected to a first separation step S1 which consists of separating said mixture of products inside a column C1, into a fraction enriched with the compounds that are lighter than ethylene containing some of the ethylene (fraction A) and into a fraction F1; d) fraction F1 is subjected to a second separation step S2 which consists of separating fraction F1 inside a column C2 into a fraction F2 and into a heavy fraction (fraction C); e) fraction F2 is subjected to a third separation step S3 which consists of separating fraction F2 inside a column C3 into a fraction enriched with ethylene (fraction B) and into a fraction F3 mainly composed of ethane; f) fraction A is conveyed to a chlorination reactor and fraction B is conveyed to an oxychlorination reactor, reactors in which most of the ethylene present in fractions A and B is converted to1,2-dichloroethane; and g) the 1,2-dichloroethane obtained is separated from the streams of products derived from the chlorination and oxychlorination reactors.
摘要翻译：用于从烃源开始制造DCE的方法，其中：a）烃源经受第一裂化步骤，即在至少一个裂解炉中进行的热解步骤，从而产生裂化产物的混合物; b）所述裂化产物的混合物经受一系列处理步骤，使得可以获得含有乙烯和其它组分的产物的混合物; c）含有乙烯的所述产物混合物进行第一分离步骤S1，该步骤包括将柱C1内的产物混合物分离成富含比含有一些乙烯（馏分A）的乙烯轻的化合物的级分，并进入分数F1; d）级分F1进行第二分离步骤S2，其由柱C2内的馏分F1分离成馏分F2和重馏分（馏分C）组成。 e）级分F2进行第三分离步骤S3，其由柱C3内的馏分F2分离成富乙烯（馏分B）的馏分和主要由乙烷组成的级分F3; f）级分A被输送到氯化反应器，馏分B输送到氧氯化反应器，其中存在于级分A和B中的大部分乙烯转化为1,2-二氯乙烷的反应器; 和g）将获得的1,2-二氯乙烷与衍生自氯化和氧氯化反应器的产物流分离。

8. 发明申请

WO2008000705A1 PROCESS FOR THE MANUFACTURE OF 1,2-DICHLOROETHANE 审中-公开
标题翻译： 1,2-二氯乙烷的制备方法
公开(公告)号：WO2008000705A1
公开(公告)日：2008-01-03
申请号：PCT/EP2007/056268
申请日：2007-06-22
申请人： SOLVAY (Société Anonyme) , STREBELLE, Michel , BALTHASART, Dominique
发明人： STREBELLE, Michel , BALTHASART, Dominique
IPC分类号： C07C17/02 , C07C19/045
CPC分类号： C07C17/25 , C07C17/02 , C07C17/156 , C07C17/389 , C07C19/045 , C07C21/06 , C08F14/06 , Y02P20/582 , C08F2/02
摘要： Process for the manufacture of 1,2-dichloroethane starting from a stream of ethane according to which: a) the stream of ethane is subjected to a catalytic oxydehydrogenation producing a gas mixture containing ethylene, unconverted ethane, water and secondary constituents; b) said gas mixture is optionally washed and dried thus producing a dry gas mixture; c) after an optional addit io nal purification step, the dry gas mixture is then conveyed to a chlorination reactor supplied with a flow of chlorine so that at least 10% of the ethylene is converted to 1,2-dichloroethane; d) the 1,2-dichloroethane formed in the chlorination reactor is optionally isolated from the stream of products derived from the chlorination reactor; e) the stream of products derived from the chlorination reactor, from which the 1,2-dichloroethane has optionally been extracted, is conveyed to an oxychlorination reactor in which the majority of the balance of ethylene is converted to 1,2-dichloroethane, after optionally having subjected the latter to an absorption/desorption step e'), during which the 1,2-dichloroethane formed in the chlorination reactor is optionally extracted if it has not previously been extracted; f) the 1,2-dichloroethane formed in the oxychlorination reactor is isolated from the stream of products derived from the oxychlorination reactor and is optionally added to the 1,2-dichloroethane formed in the chlorination reactor; g) the stream of products derived from the oxychlorination reactor, from which the 1,2-dichloroethane has been extracted, optionally containing an additional stream of ethane previously introduced in one of steps b) to f), is optionally recycled to step a) after having been optionally purged of gases and/or after an optional addit ional treatment in order to eliminate the chlorinated products contained therein.
摘要翻译：从乙烷流开始制造1,2-二氯乙烷的方法，其中：a）乙烷流进行催化氧化脱氢，产生含有乙烯，未转化的乙烷，水和二级成分的气体混合物; b）任选地将所述气体混合物洗涤和干燥，从而产生干燥气体混合物; c）在任选的附加纯化步骤之后，将干燥气体混合物输送到提供有氯气流的氯化反应器，使得至少10％的乙烯转化为1,2-二氯乙烷; d）在氯化反应器中形成的1,2-二氯乙烷任选地与衍生自氯化反应器的产物流分离; e）来自氯化反应器的产物流，其中1,2-二氯乙烷已经从其中提取，被输送到氧氯化反应器中，其中大部分余量的乙烯被转化为1,2-二氯乙烷，之后是任选地使后者进行吸收/解吸步骤e'），在此期间，如果先前没有提取过氯化反应器中形成的1,2-二氯乙烷可选地被提取; f）在氧氯化反应器中形成的1,2-二氯乙烷与衍生自氧氯化反应器的产物流分离，任选地加入到氯化反应器中形成的1,2-二氯乙烷中; g）来自氧氯化反应器的产物流，其中已经提取了1,2-二氯乙烷，任选地含有预先引入步骤b）至f）之一中的另外的乙烷流，任选地循环到步骤a）在可选地清除气体之后和/或在任选的添加剂处理之后，以消除其中所含的氯化产物。

9. 发明申请

WO2008000693A1 PROCESS FOR THE MANUFACTURE OF 1,2-DICHLOROETHANE 审中-公开
标题翻译： 1,2-二氯乙烷的制备方法
公开(公告)号：WO2008000693A1
公开(公告)日：2008-01-03
申请号：PCT/EP2007/056227
申请日：2007-06-22
申请人： SOLVAY (Société Anonyme) , STREBELLE, Michel , BALTHASART, Dominique
发明人： STREBELLE, Michel , BALTHASART, Dominique
IPC分类号： C07C17/02 , C07C17/156 , C08F14/06 , C07C17/25
CPC分类号： C07C17/25 , C07C17/02 , C07C17/156 , C07C19/045 , C07C21/06 , C08F2/10 , C08F14/06 , C08F14/12 , Y02P20/582
摘要： Process for the manufacture of 1,2-dichloroethane starting from a stream of ethane according to which: a) the stream of ethane is subjected to a catalytic oxydehydrogenation producing a gas mixture containing ethylene, unconverted ethane, water and secondary constituents; b) said gas mixture is optionally washed and dried thus producing a dry gas mixture; c) after an optional additional purification step, said dry gas mixture comprising the stream of products derived from the chlorination reactor R2 separated in step e) is subjected to an absorption A which consists of separating said gas mixture into a fraction enriched with the compounds that are lighter than ethylene containing some of the ethylene (fraction A) and into a fraction F1; d) fraction A is conveyed to a chlorination reactor R1 in which most of the ethylene present in fraction A is converted into 1,2-dichloroethane and the 1,2-dichloroethane obtained is separated from the stream of products derived from the chlorination reactor R1; e) fraction F1 is subjected to a desorption D1 which consists of separating fraction F1 into an ethylene fraction depleted of the compounds that are lighter than ethylene (fraction C) which is conveyed to a chlorination reactor R2, the stream of products derived from this reactor being added to the dry gas mixture subjected to step c) after having optionally extracted the 1,2- dichloroethane formed, and into a fraction F2; f) fraction F2 is subjected to a desorption D2 which consists of separating fraction F2 into a fraction enriched with ethylene (fraction B) and into a fraction F3, optionally containing the 1,2-dichloroethane formed in the chlorination reactor R2 then extracted, if it has not previously been extracted, which is recycled to the absorption A, optionally after an additional treatment intended to reduce the concentration, in fraction F3, of the compounds that are heavier than ethane; g) fraction B is conveyed to an oxychlorination reactor in which most of the ethylene present in fraction B is converted into 1,2-dichloroethane, the 1,2- dichloroethane obtained is separated from the stream of products derived from the oxychlorination reactor and is optionally added to the 1,2-dichloroethane formed in the chlorination reactor R1 and optionally to that formed in the chlorination reactor R2; and h) the stream of products derived from the oxychlorination reactor, from which the 1,2-dichloroethane has been extracted, optionally containing an additional stream of ethane previously introduced in one of steps b) to g), is optionally recycled to step a) after having been optionally purged of gases and/or after an optional treatment in order to eliminate the chlorinated products contained therein.
摘要翻译：从乙烷流开始制造1,2-二氯乙烷的方法，其中：a）乙烷流进行催化氧化脱氢，产生含有乙烯，未转化的乙烷，水和二级成分的气体混合物; b）任选地将所述气体混合物洗涤和干燥，从而产生干燥气体混合物; c）在任选的另外的纯化步骤之后，将包含源自步骤e）中分离的氯化反应器R2的产物流的所述干燥气体混合物经受吸收A，其包括将所述气体混合物分离成富含化合物的级分，比含有一些乙烯（级分A）的乙烯轻，并且分馏成级F1; d）将馏分A输送到氯化反应器R1，其中将馏分A中存在的大部分乙烯转化为1,2-二氯乙烷，将得到的1,2-二氯乙烷与衍生自氯化反应器R1的产物流分离 ; e）级分F1经受解吸D1，其由将馏分F1分离成不足乙烯（馏分C）的化合物的乙烯馏分组成，其被输送到氯化反应器R2，源自该反应器的产物流在任选地提取形成的1,2-二氯乙烷后加入到步骤c）的干燥气体混合物中，并加入到级分F2中; f）级分F2进行解吸D2，其由分离级分F2分成富乙烯（级分B）的级分，并且进入级分F3，任选地含有在氯化反应器R2中形成的1,2-二氯乙烷，然后萃取，如果以前没有提取，其被再循环到吸收剂A中，任选地在旨在降低重量比乙烷的化合物的级分F3中的浓度的额外处理之后; g）馏分B输送到氧氯化反应器，其中存在于馏分B中的大部分乙烯转化成1,2-二氯乙烷，所得的1,2-二氯乙烷与源自氧氯化反应器的产物流分离，并且是任选地加入到氯化反应器R1中形成的1,2-二氯乙烷中，任选地加入到氯化反应器R2中形成的1,2-二氯乙烷中; 和h）源自氧氯化反应器的产物流，其中已经从其中提取1,2-二氯乙烷，任选地含有先前在步骤b）至g）之一中引入的另外的乙烷流，任选地循环到步骤a ），或者在任选处理之后，为了消除其中所含的氯化产物。

10. 发明申请

WO2006067193A1 PROCESS FOR THE MANUFACTURE OF 1,2-DICHLOROETHANE 审中-公开
标题翻译： 1,2-二氯乙烷的制备方法
公开(公告)号：WO2006067193A1
公开(公告)日：2006-06-29
申请号：PCT/EP2005/057049
申请日：2005-12-21
申请人： SOLVAY (Société Anonyme) , STREBELLE, Michel , BALTHASART, Dominique
发明人： STREBELLE, Michel , BALTHASART, Dominique
IPC分类号： C07C17/02 , C07C17/156 , C07C19/045 , C07C21/06 , C07C17/25 , C08F14/06
CPC分类号： C07C21/06 , C07C17/02 , C07C17/156 , C07C17/25 , C07C19/045 , Y02P20/582
摘要： Process for the manufacture of 1,2-dichloroethane starting with a hydrocarbon source according to which: a) the hydrocarbon source is subjected to a first cracking step, namely a pyrolysis step performed in a cracking oven, thus producing a mixture of cracking products; b) the said mixture of cracking products is subjected to a succession of treatment steps ending with a drying step which makes it possible to obtain a mixture of products containing ethylene and other constituents; c) the said mixture of products containing ethylene derived from step b) is separated into at least one fraction containing ethylene and into a heavy fraction; d) the fraction(s) containing the ethylene is (are) conveyed to a chlorination reactor and/or to an oxychlorination reactor, in which reactors most of the ethylene present is converted to 1,2-dichloroethane; e) the 1,2-dichloroethane obtained is separated from the streams of products derived from the chlorination and oxychlorination reactors; the process being characterized in that a step for hydrogenating the acetylene is carried out upstream of the drying step ending the succession of treatment steps constituting step b) and/or on at least one of the fractions containing ethylene after separation during step c).
摘要翻译：从烃源开始制造1,2-二氯乙烷的方法，其中：a）烃源进行第一裂化步骤，即在裂化炉中进行的热解步骤，从而产生裂化产物的混合物; b）所述裂化产物混合物经历一系列以干燥步骤结束的处理步骤，其可以获得含有乙烯和其它组分的产物的混合物; c）将来自步骤b）的含有乙烯的所述产物混合物分离成至少一个含有乙烯的馏分和重馏分; d）将含有乙烯的馏分输送到氯化反应器和/或氧氯化反应器，其中反应器将大部分乙烯转化为1,2-二氯乙烷; e）将获得的1,2-二氯乙烷与衍生自氯化和氧氯化反应器的产物流分离; 该方法的特征在于，在干燥步骤的上游进行氢化乙炔的步骤，其结束步骤b）的处理步骤和/或在步骤c）中分离后含有乙烯的馏分中的至少一个馏分。

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