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1. 发明申请

WO2006100313A3 METHOD FOR MAKING A CHLOROHYDRIN 审中-公开
标题翻译：制备氯罗坦的方法
公开(公告)号：WO2006100313A3
公开(公告)日：2006-11-09
申请号：PCT/EP2006062439
申请日：2006-05-19
申请人： SOLVAY , KRAFFT PHILIPPE , GILBEAU PATRICK , BALTHASART DOMINIQUE , SMETS VALENTINE
发明人： KRAFFT PHILIPPE , GILBEAU PATRICK , BALTHASART DOMINIQUE , SMETS VALENTINE
IPC分类号： C07C29/62 , C07C31/36 , C07C31/42
CPC分类号： B01D3/143 , C07C29/62 , C07C29/82 , C07D301/02 , C07D301/06 , C07D301/26 , C07D303/08 , C07C31/36
摘要： The invention concerns a method for making a chlorohydrin including the following steps: (a) reacting a polyhydroxylated aliphatic hydrocarbon, an ester of polyhydroxylated hydrocarbon, or a mixture thereof, and a chlorinating agent and an organic acid to obtain a mixture containing chlorohydrin and chlorohydrin esters; (b) subjecting at least part of the mixture obtained at step (a) to one or more treatments in steps subsequent to step (a); (c) adding polyhydroxylated aliphatic hydrocarbon at least at one of the steps subsequent to step (a), so that it reacts, at a temperature not less than 20 °C, with the chlorohydrin esters so as to form at least partly polyhydroxylated aliphatic hydrocarbon esters.
摘要翻译：本发明涉及一种制备氯代醇的方法，包括以下步骤：（a）使多羟基化脂族烃，多羟基化烃或其混合物的酯与氯化剂和有机酸反应，得到含有氯代醇和氯代醇的混合物酯; （b）使步骤（a）获得的混合物的至少一部分在步骤（a）之后的步骤中进行一次或多次处理; （c）至少在步骤（a）之后的步骤之一中加入多羟基化脂族烃，使其在不低于20℃的温度下与氯醇酯反应，以形成至少部分多羟基化脂族烃酯。

2. 发明申请

WO2006100312A3 PROCESS FOR PRODUCING A CHLORHYDRIN FROM A MULTIHYDROXYLATED ALIPHATIC HYDROCARBON AND/OR ESTER THEREOF IN THE PRESENCE OF METAL SALTS 审中-公开
标题翻译：在多金属盐酸盐和/或其中存在的金属盐生产氯仿的方法
公开(公告)号：WO2006100312A3
公开(公告)日：2006-11-02
申请号：PCT/EP2006062438
申请日：2006-05-19
申请人： SOLVAY , GILBEAU PATRICK , DE ANDOLENKO IVAN , KRAFFT PHILIPPE , GIELEN FREDDY
发明人： GILBEAU PATRICK , DE ANDOLENKO IVAN , KRAFFT PHILIPPE , GIELEN FREDDY
IPC分类号： C07C29/62 , C07C29/82 , C07C31/36
CPC分类号： B01D3/143 , C07C29/62 , C07C29/82 , C07D301/02 , C07D301/06 , C07D301/26 , C07D303/08 , C07C31/36
摘要： Process for producing a chlorohydrin by reaction between a multihydroxylated- aliphatic hydrocarbon, an ester of a multihydroxylated-aliphatic hydrocarbon, or a mixture thereof, and a chlorinating agent, according to which the multihydroxylated-aliphatic hydrocarbon, the ester of a multihydroxylated- aliphatic hydrocarbon, or the mixture thereof used contains at least one solid or dissolved metal salt, the process comprising a separation operation to remove at least part of the metal salt.
摘要翻译：通过多羟基化脂族烃，多羟基化脂肪族烃的酯或其混合物之间的反应生产氯代醇的方法和氯化剂，根据该方法，多羟基化脂族烃，多羟基化脂族烃的酯，或其使用的混合物含有至少一种固体或溶解的金属盐，该方法包括去除至少部分金属盐的分离操作。

3. 发明申请

WO2006100312A9 PROCESS FOR PRODUCING A CHLORHYDRIN FROM A MULTIHYDROXYLATED ALIPHATIC HYDROCARBON AND/OR ESTER THEREOF IN THE PRESENCE OF METAL SALTS 审中-公开
标题翻译：在多金属盐酸盐和/或其中存在的金属盐生产氯仿的方法
公开(公告)号：WO2006100312A9
公开(公告)日：2007-05-18
申请号：PCT/EP2006062438
申请日：2006-05-19
申请人： SOLVAY , GILBEAU PATRICK , DE ANDOLENKO IVAN , KRAFFT PHILIPPE , GIELEN FREDDY
发明人： GILBEAU PATRICK , DE ANDOLENKO IVAN , KRAFFT PHILIPPE , GIELEN FREDDY
IPC分类号： C07C29/62 , C07C29/82 , C07C31/36
CPC分类号： B01D3/143 , C07C29/62 , C07C29/82 , C07D301/02 , C07D301/06 , C07D301/26 , C07D303/08 , C07C31/36
摘要： Process for producing a chlorohydrin by reaction between a multihydroxylated- aliphatic hydrocarbon, an ester of a multihydroxylated-aliphatic hydrocarbon, or a mixture thereof, and a chlorinating agent, according to which the multihydroxylated-aliphatic hydrocarbon, the ester of a multihydroxylated- aliphatic hydrocarbon, or the mixture thereof used contains at least one solid or dissolved metal salt, the process comprising a separation operation to remove at least part of the metal salt.
摘要翻译：通过多羟基化脂族烃，多羟基化脂肪族烃的酯或其混合物之间的反应生产氯代醇的方法和氯化剂，根据该方法，多羟基化脂族烃，多羟基化脂族烃的酯，或其使用的混合物含有至少一种固体或溶解的金属盐，该方法包括去除至少部分金属盐的分离操作。

4. 发明申请

WO2006100315A3 METHOD FOR MAKING A CHLOROHYDRIN BY CHLORINATING A POLYHYDROXYLATED ALIPHATIC HYDROCARBON 审中-公开
标题翻译：通过氯化聚甲基丙烯酸氢氯酸盐制备氯代醇的方法
公开(公告)号：WO2006100315A3
公开(公告)日：2006-11-16
申请号：PCT/EP2006062444
申请日：2006-05-19
申请人： SOLVAY , KRAFFT PHILIPPE , GILBEAU PATRICK , BALTHASART DOMINIQUE , SMETS VALENTINE
发明人： KRAFFT PHILIPPE , GILBEAU PATRICK , BALTHASART DOMINIQUE , SMETS VALENTINE
IPC分类号： C07C29/62 , C07C29/88 , C07C31/36 , C07C31/42
CPC分类号： B01D3/143 , C07C29/62 , C07C29/82 , C07D301/02 , C07D301/06 , C07D301/26 , C07D303/08 , C07C31/36
摘要： The invention concerns a method for making a chlorohydrin including the following steps: (a) reacting a polyhydroxylated aliphatic hydrocarbon, an ester of a polyhydroxylated aliphatic hydrocarbon, or a mixture thereof, whereof the alkali and/or alkaline-earth metal content is not more than 5g/kg, an oxidizing agent and an organic acid to obtain a mixture containing at least chlorohydrin and by-products; (b) subjecting at least part of the mixture obtained at step (a) to one or more treatments in steps subsequent to step (a); oxidizing at a temperature not less than 800 °C at least at one of the steps subsequent to step (a).
摘要翻译：本发明涉及一种制备氯代醇的方法，包括以下步骤：（a）使多羟基化脂族烃，多羟基化脂族烃或其混合物的酯与碱金属和/或碱土金属含量不多于 5g / kg以上，氧化剂和有机酸，得到至少含有氯代醇和副产物的混合物; （b）使步骤（a）获得的至少部分混合物在步骤（a）之后的步骤中进行一次或多次处理; 在步骤（a）之后的至少一个步骤中，在不低于800℃的温度下进行氧化。

5. 发明申请

WO2008101866A3 PROCESS FOR MANUFACTURING EPICHLOROHYDRIN 审中-公开
标题翻译：制备EPICHLOROHYDRIN的方法
公开(公告)号：WO2008101866A3
公开(公告)日：2009-11-05
申请号：PCT/EP2008051830
申请日：2008-02-15
申请人： SOLVAY , GILBEAU PATRICK , KRAFFT PHILIPPE
发明人： GILBEAU PATRICK , KRAFFT PHILIPPE
IPC分类号： C07D303/08
CPC分类号： C07D301/24
摘要： Process for manufacturing epichlorohydrin comprising the following steps: a) in a liquid reaction medium, a mixture of 1,3 - dichloro - 2 - propanol and 2,3 - dichloro - 1 - propanol, in which the 1,3 - dichloro - 2 - propanol content is at least 10 wt%, is reacted with at least one basic compound in order to form epichlorohydrin and a salt; and b) at least one part of the liquid reaction medium from step a) is subjected to a settling operation in which at least a first fraction containing most of the epichlorohydrin which was contained in the part of the reaction medium from step a) before the settling operation and a second fraction containing most of the salt which was contained in the part of the reaction medium from step a) before the settling operation are separated.
摘要翻译：制备表氯醇的方法，包括以下步骤：a）在液体反应介质中，1,3-二氯-2-丙醇和2,3-二氯-1-丙醇的混合物，其中1,3-二氯-2 - 丙醇含量为至少10重量％，与至少一种碱性化合物反应以形成表氯醇和盐; 和b）将来自步骤a）的液体反应介质的至少一部分进行沉淀操作，其中至少第一级分含有大部分表氯醇，反应介质部分中包含的步骤a）在沉降操作之前分离沉淀操作和含有来自步骤a）的部分反应介质中大部分盐的第二级分。

6. 发明申请

WO2008110588A3 PROCESS FOR THE MANUFACTURE OF DICHLOROPROPANOL 审中-公开
标题翻译：二氯丙醇制备方法
公开(公告)号：WO2008110588A3
公开(公告)日：2008-10-30
申请号：PCT/EP2008052972
申请日：2008-03-13
申请人： SOLVAY , KRAFFT PHILIPPE , GILBEAU PATRICK , BALTHASART DOMINIQUE , PAGANIN MAURIZIO
发明人： KRAFFT PHILIPPE , GILBEAU PATRICK , BALTHASART DOMINIQUE , PAGANIN MAURIZIO
IPC分类号： C07C29/62 , C07C31/36
CPC分类号： C07C29/62 , C07C29/82 , C07C29/86 , C07C31/36
摘要： Process for manufacturing dichloropropanol according to which: a) in a liquid reaction medium containing water, which is in contact with a gaseous phase, glycerol is reacted with hydrogen chloride under a partial pressure of hydrogen chloride in the gaseous phase greater than 0.2 bar absolute, and b) at least part of the liquid reaction medium and optionally part of the gaseous phase from step (a) is (are) subjected to at least one separation operation and, prior to said separation operation, the part of the liquid reaction medium and the part of the gaseous phase from step (a) is (are) subjected to: bi) at least one treatment for reducing the weight ratio between the hydrogen chloride and the water in the part of the liquid reaction medium so as to attain a ratio less than or equal to the weight ratio between the hydrogen chloride and the water in the binary azeotropic hydrogen chloride/water composition at total pressure of the separation operation, and/or bii) at least one treatment for reducing the weight ratio between the water and the dichloropropanol in the part of the liquid reaction medium so as to attain a ratio less than or equal to the weight ratio between the water and the dichloropropanol in the ternary water/dichloropropanol/hydrogen chloride azeotrope at total pressure of the separation operation.
摘要翻译：制备二氯丙醇的方法，其中：a）在含有与气相接触的水的液体反应介质中，在大于0.2巴绝对压力的气相中，氯化氢在氯化氢的分压下与氯化氢反应，和b）至少部分液体反应介质和任选地来自步骤（a）的气相的一部分进行至少一个分离操作，并且在所述分离操作之前，将部分液体反应介质和来自步骤（a）的气相的部分（b）进行至少一种处理以减少液体反应介质的部分中的氯化氢和水之间的重量比，以获得比例小于或等于在分离操作的总压力下的二元共沸氯化氢/水组合物中的氯化氢和水之间的重量比，和/或bii）至少一种处理用于降低液体反应介质部分的水和二氯丙醇之间的重量比，以获得小于或等于三元水/二氯丙醇/氯化氢共沸物中水和二氯丙醇之间的重量比的比例分离操作的总压力。

7. 发明申请

WO2006100318A9 METHOD FOR MAKING AN EPOXIDE STARTING WITH A POLYHYDROXYLATED ALIPHATIC HYDROCARBON AND A CHLORINATING AGENT 审中-公开
标题翻译：用聚甲基丙烯酸二氯化碳和氯化剂制备环氧化物的方法
公开(公告)号：WO2006100318A9
公开(公告)日：2006-11-16
申请号：PCT/EP2006062459
申请日：2006-05-19
申请人： SOLVAY , KRAFFT PHILIPPE , GILBEAU PATRICK , BALTHASART DOMINIQUE , SMETS VALENTINE
发明人： KRAFFT PHILIPPE , GILBEAU PATRICK , BALTHASART DOMINIQUE , SMETS VALENTINE
IPC分类号： C07D303/08 , C07C29/62 , C07C31/34 , C07D301/26
CPC分类号： B01D3/143 , C07C29/62 , C07C29/82 , C07D301/02 , C07D301/06 , C07D301/26 , C07D303/08 , C07C31/36
摘要： The invention concerns a method for making an epoxide which consists in subjecting in a reaction medium resulting from the reaction between a polyhydroxylated aliphatic hydrocarbon, an ester of a polyhydroxylated aliphatic hydrocarbon, or a mixture thereof, and a chlorinating agent, the reaction medium containing at least 10 mg of chlorohydrin per kg of reaction medium, to a subsequent chemical reaction without any intermediate treatment.
摘要翻译：本发明涉及一种制备环氧化物的方法，该方法包括在由多羟基化脂族烃，多羟基化脂族烃或其混合物的酯与氯化剂之间的反应得到的反应介质中进行，所述反应介质含有每kg反应介质至少10mg氯代醇，进行后续化学反应，无需任何中间处理。

8. 发明申请

WO2011054769A2 PROCESS FOR MANUFACTURING A PRODUCT DERIVED FROM EPICHLOROHYDRIN 审中-公开
标题翻译：用于制造从EPICHLOROHYDRIN衍生的产品的方法
公开(公告)号：WO2011054769A2
公开(公告)日：2011-05-12
申请号：PCT/EP2010066532
申请日：2010-10-29
申请人： SOLVAY , GILBEAU PATRICK
发明人： GILBEAU PATRICK
IPC分类号： C08G59/06
CPC分类号： C08G59/063 , C08G59/022
摘要： Process for manufacturing a product derived from epichlorohydrin by conversion of epichlorohydrin starting from a raw material comprising epichlorohydrin, in which use is made of an alkylating agent as an additive, said alkylating agent being added to at least one step of the process or formed in at least one step of the process, in an additional amount relative to the amount of this alkylating agent possibly present as an impurity in the raw material, said alkylating agent being chosen from halogen-substituted, sulphate-substituted, sulphonate-substituted, carbonate-substituted and phosphate-substituted organic compounds and mixtures of at least two of them.
摘要翻译：通过从包含表氯醇的原料开始转化表氯醇的方法，其中使用烷基化剂作为添加剂，所述烷基化剂加入到该方法的至少一个步骤中或形成于该方法的至少一步相对于原料中作为杂质可能存在的该烷基化剂的量的额外量，所述烷基化剂选自卤素取代的，硫酸酯取代的，磺酸酯取代的，碳酸酯取代的和磷酸酯取代的有机化合物及其至少两种的混合物。

9. 发明申请

WO2009000773A8 MANUFACTURE OF DICHLOROPROPANOL 审中-公开
标题翻译：二氯丙醇的制备
公开(公告)号：WO2009000773A8
公开(公告)日：2010-01-14
申请号：PCT/EP2008057876
申请日：2008-06-20
申请人： SOLVAY , KRAFFT PHILIPPE , GILBEAU PATRICK
发明人： KRAFFT PHILIPPE , GILBEAU PATRICK
IPC分类号： C07C29/62 , C07C31/20 , C07C31/22 , C07C31/36 , C07D301/26 , C07D303/08 , C08G59/02
CPC分类号： C08G59/06 , C07C29/62 , C07D301/26 , C07D303/08 , C07C31/36
摘要： Manufacture of dichloropropanol Process for manufacturing dichloropropa nol wherein a glycerol-based product comprising at least one diol containi ng at least 3 carbon atoms other than 1,2- propanediol, is reacted with a chlorinati ng agent, and of products derived from dichloropropanol such as ep ichlorohydrin and epoxy resins. No figure.
摘要翻译：二氯丙醇的制造二氯丙醇的制造方法其中含有至少一种含有至少3个碳原子的二醇以外的1,2-二醇的二醇的甘油基产物与二氢化合物以及衍生自二氯丙醇的产物如环氧氯丙烷和环氧树脂。没有数字

10. 发明申请

WO2009016149A3 PROCESS FOR MANUFACTURING GLYCIDOL 审中-公开
标题翻译：制备甘油的方法
公开(公告)号：WO2009016149A3
公开(公告)日：2009-04-02
申请号：PCT/EP2008059862
申请日：2008-07-28
申请人： SOLVAY , GILBEAU PATRICK
发明人： GILBEAU PATRICK
IPC分类号： C07D301/26 , C07D301/32 , C07D303/14
CPC分类号： C07D301/26 , C07D301/32 , C07D303/14
摘要： Process for manufacturing glycidol comprising at least the following steps: a) glycerol and a chlorinating agent are reacted to form monochloropropanediol in a first reaction medium; and b) at least one part of the reaction medium from step a) is reacted with at least one basic compound to form glycidol and a salt in a second reaction medium, the organic component of which has a monochloropropanediol content before reaction with the basic compound greater than 100 g/kg of organic component.
摘要翻译：制备缩水甘油的方法至少包括以下步骤：a）甘油和氯化剂在第一反应介质中反应形成一氯丙二醇; 和b）将来自步骤a）的反应介质的至少一部分与至少一种碱性化合物反应以在第二反应介质中形成缩水甘油和盐，其中有机组分在与碱性化合物反应之前具有一氯丙二醇含量大于100g / kg的有机组分。

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