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1. 发明申请

WO2005012236A1 STABILIZED (METH)ACRYLOYLOXYALKYL ISOCYANATE, A PROCESS FOR STABILIZATION THEREOF AND A PROCESS FOR PREPARATION OF THE SAME 审中-公开
标题翻译：稳定的（甲基）丙烯酰氧基甲基异氰酸酯，其稳定化方法及其制备方法
公开(公告)号：WO2005012236A1
公开(公告)日：2005-02-10
申请号：PCT/JP2004/011017
申请日：2004-07-27
申请人： SHOWA DENKO K.K. , MORINAKA, Katsutoshi , ISHIKAWA, Toshiaki , HOSHI, Kazuyoshi
发明人： MORINAKA, Katsutoshi , ISHIKAWA, Toshiaki , HOSHI, Kazuyoshi
IPC分类号： C07C263/18
CPC分类号： C07C263/18 , C07C265/04
摘要： The present invention provides a stabilized (meth)acryloyloxyalkyl isocyanate, a process for stabilization thereof and a process for preparation of the same. More particularly, it provides a (meth)acryloyloxyalkyl isocyanate having a small hydrolyzable chlorine content and good storage stability, a process for stabilizing a (meth)acryloyloxyalkyl isocyanate prepared using phosgene which process comprises decreasing the amount of a hydrolyzable chlorine with purification and a process for preparation of a stabilized (meth)acryloyloxyalkyl isocyanate. An acidic gas such as carbon dioxide or the like was forcedly dissolved in (meth)acryloyloxyalkyl isocyanate, particularly (meth)acryloyloxyalkyl isocyanate which content of hydrolyzable chlorine is decreased with purification and thereby the storage stability of the (meth)acryloyloxyalkyl isocyanate is improved.
摘要翻译：本发明提供稳定的（甲基）丙烯酰氧基烷基异氰酸酯，其稳定化方法及其制备方法。更具体地说，它提供了具有小的可水解氯含量和良好储存稳定性的（甲基）丙烯酰氧基烷基异氰酸酯，稳定用光气制备的（甲基）丙烯酰氧基烷基异氰酸酯的方法，该方法包括通过纯化降低可水解氯的量和方法用于制备稳定的（甲基）丙烯酰氧基烷基异氰酸酯。特别是（甲基）丙烯酰氧基烷基异氰酸酯，特别是可水解氯的含量降低的（甲基）丙烯酰氧基烷基异氰酸酯等酸性气体，由此提高了（甲基）丙烯酰氧基烷基异氰酸酯的保存稳定性。

2. 发明申请

WO2005012237A1 PROCESS FOR PREPARING HIGH PURITY (METH)ACRYLOYLOXYALKYL ISOCYANATE 审中-公开
标题翻译：制备高纯度（甲基）丙烯酰氧基甲基异氰酸酯的方法
公开(公告)号：WO2005012237A1
公开(公告)日：2005-02-10
申请号：PCT/JP2004/011019
申请日：2004-07-27
申请人： SHOWA DENKO K.K. , MORINAKA, Katsutoshi , HOSHI, Kazuyoshi
发明人： MORINAKA, Katsutoshi , HOSHI, Kazuyoshi
IPC分类号： C07C263/20
CPC分类号： C07C263/18 , C07C263/20 , C07C265/04
摘要： A process for preparing a high purity (meth)acryloyloxyalkyl isocyanate having a very small hydrolyzable chlorine content is provided. The high purity (meth)acryloyloxyalkyl isocyanate is prepared by subjecting a hydrolyzable chlorine containing (meth)acryloyloxyalkyl isocyanate to mixing treatment with an epoxy compound and an amine at a temperature of from 110 to 160oC to prepare a mixture; and preparing a high purity (meth)acryloyloxyalkyl isocyanate from the resulting mixture with distillation. In particular, it is possible to effectively prevent (meth)acryloyloxyalkyl isocyanate from polymerization during the distillation by adding a polymerization inhibitor such as phenothiazine and the like.
摘要翻译：提供了制备具有非常小的可水解氯含量的高纯度（甲基）丙烯酰氧基烷基异氰酸酯的方法。高纯度（甲基）丙烯酰氧基烷基异氰酸酯通过在110〜160℃的温度下使含有水解性氯的（甲基）丙烯酰氧基烷基异氰酸酯与环氧化合物和胺进行混合处理来制备异氰酸酯。并通过蒸馏从所得混合物中制备高纯度（甲基）丙烯酰氧基烷基异氰酸酯。特别地，可以通过加入阻聚剂如吩噻嗪等在蒸馏期间有效地防止（甲基）丙烯酰氧基烷基异氰酸酯聚合。

3. 发明申请

WO2005075445A2 (METH) ACRYLOYL GROUP-CONTAINING OXETANE COMPOUND AND PRODUCTION METHOD THEREOF 审中-公开
标题翻译：（METH）含丙烯酸基团的含氧化合物及其制备方法
公开(公告)号：WO2005075445A2
公开(公告)日：2005-08-18
申请号：PCT/JP2005/002381
申请日：2005-02-09
申请人： SHOWA DENKO K.K. , KAMATA, Hirotoshi , MORINAKA, Katsutoshi , UCHIDA, Hiroshi
发明人： KAMATA, Hirotoshi , MORINAKA, Katsutoshi , UCHIDA, Hiroshi
IPC分类号： C07D305/00
CPC分类号： C07D305/06
摘要： The present invention relates to an oxetane compound containing a (meth)acryloyl group represented by formula (1) having a high copolymerizability with compounds containing a (meth) acryloyl group, and to a production method of an oxetane compound containing a (meth) acryloyl group which is characterized by reacting an isocyanate compound having a (meth) acryloyl group represented by formula (5) with an oxetane compound containing a hydroxyl group represented by formula (In the formula, R 1 represents a hydrogen atom or a methyl group, A represents -OR 2 - or a bond, R 2 represents a divalent hydrocarbon group which may contain an oxygen atom in the main chain, R 3 represents a linear or branched alkylene group having 1 to 6 carbon atoms, and R 4 represents a linear or branched alkyl group having 1 to 6 carbon atoms.)
摘要翻译：本发明涉及含有与（甲基）丙烯酰基的化合物具有高共聚性的由式（1）表示的（甲基）丙烯酰基的氧杂环丁烷化合物，以及含有（甲基）丙烯酰基其特征在于使具有式（5）表示的（甲基）丙烯酰基的异氰酸酯化合物与式（5）所示的含有羟基的氧杂环丁烷化合物反应（式中，R 1表示氢原子或甲基，A表示-OR 2 - 或键，R 2表示可在主链中含有氧原子的二价烃基，R 3表示碳原子数为1〜6的直链或支链亚烷基，R 4表示碳原子数为1〜6的直链或支链烷基。）

4. 发明申请

WO2005103822A2 PHOTOSENSITIVE RESIN COMPOSITION, CURED PRODUCT THEREOF AND PRODUCTION METHOD OF PRINTED CIRCUIT BOARD USING THE SAME 审中-公开
标题翻译：光敏树脂组合物，其固化产物及其印刷电路板的制造方法
公开(公告)号：WO2005103822A2
公开(公告)日：2005-11-03
申请号：PCT/JP2005/008100
申请日：2005-04-21
申请人： SHOWA DENKO K.K. , ISHIGAKI, Satoru , UCHIDA, Hiroshi , MIYAJIMA, Yoshio , MORINAKA, Katsutoshi
发明人： ISHIGAKI, Satoru , UCHIDA, Hiroshi , MIYAJIMA, Yoshio , MORINAKA, Katsutoshi
IPC分类号： G03F7/00
CPC分类号： G03F7/027 , C08G18/0823 , C08G18/4854 , C08G18/672 , C08G18/755 , C09D175/16 , G03F7/032 , G03F7/033 , G03F7/035 , G03F7/038 , G03F7/0388 , H05K3/287 , Y10T428/31855 , C08G18/6692
摘要： There are provided a novel photosensitive resin composition, a cured film of which has ample flexibility, and which yields an insulating protective coating having superior soldering heat resistance, thermal degradation resistance and electroless gold plating resistance. The photosensitive resin composition as claimed in the present invention comprises: a photopolymerizeable component containing a urethane acrylate compound (A) and a compound (B) having an ethylenic unsaturated group other than said urethane acrylate compound (A), a thermosetting resin (C), a photopolymerization initiator (D) and a thermal polymerization catalyst (E); wherein, said urethane acrylate compound (A) is the reaction product of an isocyanate compound (a-1) of the following general formula (1): CH2=CH-COO-R-NCO (1) (wherein, R represents a hydrocarbon group having 1 to 30 carbon atoms) with a polyhydroxy compound (a-2).
摘要翻译：提供了一种新颖的感光性树脂组合物，其固化膜具有充分的柔软性，并且产生具有优异的耐焊接耐热性，耐热劣化性和无电镀金电镀性的绝缘保护涂层。本发明的感光性树脂组合物包含：含有氨基甲酸酯丙烯酸酯化合物（A）和除所述氨基甲酸酯丙烯酸酯化合物（A）以外具有乙烯性不饱和基团的化合物（B）的光聚合性成分，热固性树脂（C），光聚合引发剂（D）和热聚合催化剂（E）; 其中所述氨基甲酸酯丙烯酸酯化合物（A）是以下通式（1）的异氰酸酯化合物（a-1）：CH 2 = CH-COO-R-NCO（1）（其中R表示烃具有1至30个碳原子的基团）与多羟基化合物（a-2）反应。

5. 发明申请

WO2008099903A2 FINE PATTERN TRANSFER MATERIAL 审中-公开
标题翻译：精细图案转印材料
公开(公告)号：WO2008099903A2
公开(公告)日：2008-08-21
申请号：PCT/JP2008/052476
申请日：2008-02-07
申请人： SHOWA DENKO K.K. , FUJITA, Toshio , UCHIDA, Hiroshi , MORINAKA, Katsutoshi , HIROSE, Katsumasa
发明人： FUJITA, Toshio , UCHIDA, Hiroshi , MORINAKA, Katsutoshi , HIROSE, Katsumasa
IPC分类号： G03F7/00 , G03F7/075
CPC分类号： G03F7/0002 , B82Y10/00 , B82Y40/00 , G11B5/855
摘要： [Purpose] To provide a transfer material that can favorably form a fine pattern by nanoimprinting. [Resolution Means] The nanoimprinting transfer material is a fine pattern resin composition that includes an organosilicon compound and a metal compound of a metal from groups 3 through 14 of the periodic table.
摘要翻译： [目的]提供可以通过纳米压印有利地形成精细图案的转印材料。分辨方法纳米压印转印材料是包含有机硅化合物和周期表第3〜14族金属的金属化合物的精细图案树脂组合物。

6. 发明申请

WO2006049264A1 ETHYLENICALLY UNSATURATED GROUP-CONTAINING ISOCYANATE COMPOUND AND PROCESS FOR PRODUCING THE SAME, AND REACTIVE MONOMER, REACTIVE (METH)ACRYLATE POLYMER AND ITS USE 审中-公开
标题翻译：含有异亚烯基的含异氰酸酯基的化合物及其制备方法和反应性单体，反应性（甲基）丙烯酸酯聚合物及其用途
公开(公告)号：WO2006049264A1
公开(公告)日：2006-05-11
申请号：PCT/JP2005/020325
申请日：2005-10-31
申请人： SHOWA DENKO K.K. , NOZAWA, Kaneo , MORINAKA, Katsutoshi , SASAKI, Toru , MUROFUSHI, Katsumi
发明人： NOZAWA, Kaneo , MORINAKA, Katsutoshi , SASAKI, Toru , MUROFUSHI, Katsumi
IPC分类号： C07C263/10 , C07C265/04 , C08F299/00
CPC分类号： C07C265/04 , B33Y70/00 , C07C271/16 , C07C271/34 , C07C275/22 , C07C275/24 , C07C275/30 , C07C333/04 , C07C2601/14 , C07C2603/18 , C07C2603/74 , C08F222/1006 , C08F222/22 , G03F7/027 , H05K3/287 , Y10T428/24917
摘要： There are provided a novel ethylenically unsaturated group-containing isocyanate compound, a process for producing the same, and a reactive monomer produced from the isocyanate compound, a reactive polymer and its use. The ethylenically unsaturated group-containing isocyanate compound according to the present invention is represented by formula (I).
摘要翻译：提供了一种新颖的含烯键式不饱和基团的异氰酸酯化合物，其制备方法以及由异氰酸酯化合物，反应性聚合物及其用途制备的反应性单体。本发明的含烯属不饱和基团的异氰酸酯化合物由式（I）表示。

7. 发明申请

WO2005103823A1 PHOTOSENSITIVE COMPOSITION FOR BLACK MATRIX 审中-公开
标题翻译：黑色矩阵的光敏组合物
公开(公告)号：WO2005103823A1
公开(公告)日：2005-11-03
申请号：PCT/JP2005/008270
申请日：2005-04-22
申请人： SHOWA DENKO K.K. , ISHIGAKI, Satoru , ONISHI, Mina , MUROFUSHI, Katsumi , MORINAKA, Katsutoshi
发明人： ISHIGAKI, Satoru , ONISHI, Mina , MUROFUSHI, Katsumi , MORINAKA, Katsutoshi
IPC分类号： G03F7/00
CPC分类号： G03F7/035 , G03F7/0007 , G03F7/027 , G03F7/032
摘要： The invention provides a photosensitive composition for a black matrix, comprising binder resin (A) which contains a urethane acrylate compound produced by reaction between an isocyanate compound (a-1) represented by formula (1) and a polyhydroxy compound (a-2), CH 2 =CH-COO-R-NCO (1), (wherein R represents a hydrocarbon group having 1 to 30 carbon atoms), black-base pigment (B). The composition may further comprise ethylenic unsaturated monomer (C), photopolymerization initiator (D) and organic solvent (E). The mass contents of the components other than organic solvent (E) is 10-40 % for binder resin (A), 25-60 % for black-base pigment (B), 5-20 % for ethylenic unsaturated monomer and 2-25 % for photopolymerization initiator (D). By using the composition, a pattern having a thin film property and a high light-shielding property can be easily formed by a photolithography method, and the composition has sufficient sensitivity, resolution, developability, durability and curing speed.
摘要翻译：本发明提供一种黑色基质用感光性组合物，其含有粘合剂树脂（A），其含有通过式（1）表示的异氰酸酯化合物（a-1）与多羟基化合物（a-2）反应而生成的氨基甲酸酯丙烯酸酯化合物，，CH 2 = CH-COO-R-NCO（1），（其中R表示碳原子数1〜30的烃基），黑色颜料（B）。组合物还可以包含烯属不饱和单体（C），光聚合引发剂（D）和有机溶剂（E）。有机溶剂（E）以外的成分的质量含量对于粘合剂树脂（A）为10-40％，黑色基色素（B）为25-60％，烯属不饱和单体为5-20％，2-25 ％的光聚合引发剂（D）。通过使用该组合物，可以通过光刻法容易地形成具有薄膜性质和高遮光性的图案，并且该组合物具有足够的灵敏度，分辨率，显影性，耐久性和固化速度。

8. 发明申请

WO2005092842A1 METHOD FOR PRODUCING (METH)ACRYLATE DERIVATIVE HAVING ISOCYANATE GROUP 审中-公开
标题翻译：生产具有异氰酸酯基团的（甲基）丙烯酸酯衍生物的方法
公开(公告)号：WO2005092842A1
公开(公告)日：2005-10-06
申请号：PCT/JP2005/005655
申请日：2005-03-22
申请人： SHOWA DENKO K.K. , NOZAWA, Kaneo , MORINAKA, Katsutoshi
发明人： NOZAWA, Kaneo , MORINAKA, Katsutoshi
IPC分类号： C07C263/20
CPC分类号： C07C263/20 , C07C263/16 , C07C265/04
摘要： The invention aims to provide a method whereby (meth)acrylate derivatives having an isocyanate group can be obtained in high yield by dehydrochlorination of 3-chloropropionate derivatives having an isocyanate group under industrially advantageous and mild conditions, and the content of residual hydrolyzable chlorine can be reduced. A method for producing a (meth)acrylate derivative having an isocyanate group comprises performing dehydrochlorination of a 3-chloropropionate derivative having an isocyanate group in the presence of a basic nitrogen compound having a tertiary nitrogen, the tertiary nitrogen of the basic nitrogen compound having
摘要翻译：本发明的目的在于提供一种方法，可以在工业上有利且温和的条件下，通过使具有异氰酸酯基的3-氯丙酸酯衍生物的脱氯化氢以高产率获得具有异氰酸酯基的（甲基）丙烯酸酯衍生物，残留的可水解氯的含量可以为降低。一种具有异氰酸酯基的（甲基）丙烯酸酯衍生物的制造方法包括：在具有叔氮的碱性氮化合物的存在下，对具有异氰酸酯基的3-氯丙酸酯衍生物进行脱氯化氢，碱式氮化合物的叔氮具有

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