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1. 发明申请

WO2018059745A1 PROCESS FOR PRODUCTION OF ALLYL ALCOHOL 审中-公开
标题翻译：生产烯丙醇的方法
公开(公告)号：WO2018059745A1
公开(公告)日：2018-04-05
申请号：PCT/EP2017/060108
申请日：2017-04-27
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： CHODIMELLA, Venkata, Pramod , LANGE, Jean Paul, Andre, Marie, Joseph, Ghislain , SESHAN, Kulathu, Iyer
IPC分类号： C07C29/60 , C07C29/80 , C07C33/03 , C07C51/25 , C07C57/04
摘要： The invention relates to a process for producing allyl alcohol, the process comprising: dehydrating a C3-oxygenate comprising monopropylene glycol or 1,3-propanediol; wherein the dehydration is performed in the presence of a basic catalyst. The C3-oxygenate may be derived from a biomass conversion process and subsequently converted to acrylic acid.
摘要翻译：本发明涉及生产烯丙醇的方法，所述方法包括：使包含单丙二醇或1,3-丙二醇的C3-含氧化合物脱水; 其中脱水在碱性催化剂存在下进行。 C3-含氧化合物可以源自生物质转化过程并随后转化为丙烯酸。

2. 发明申请

WO2017114831A1 PROCESS FOR CONVERTING ALKANES AND/OR ALKENES TO ALKENES AND CARBOXYLIC ACIDS 审中-公开
标题翻译：将烯烃和/或烯烃转化成烯烃和羧酸的方法
公开(公告)号：WO2017114831A1
公开(公告)日：2017-07-06
申请号：PCT/EP2016/082713
申请日：2016-12-27
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： FISCHER, Kai, Jürgen , LANGE, Jean Paul, Andre, Marie, Joseph, Ghislain , VAN ROSSUM, Guus , SCHOONEBEEK, Ronald, Jan , PEREZ GOLF, Carmelo
IPC分类号： C07C51/215 , C07C51/25 , C07C51/42 , C07C51/48 , C07C53/08 , C07C53/122 , C07C53/124 , C07C53/126 , C07C53/128 , C07C57/04 , C07C57/08 , C07C57/03
CPC分类号： C07C51/48 , C07C51/215 , C07C51/25 , C07C51/252 , C07C51/44 , C07C53/122 , C07C53/124 , C07C53/126 , C07C53/128 , C07C57/04 , C07C57/08 , C07C57/03 , C07C53/08
摘要： The present invention provides a process for oxidatively converting alkanes and/or alkenes containing 2 to 6 carbon atoms ("C 2 -C 6 ") to C 2 -C 6 alkenes and C 2 -C 6 carboxylic acids, comprising a reaction step which comprises contacting a stream comprising oxygen and said C 2 -C 6 alkane and/or alkene with a mixed metal oxide catalyst, to produce a stream comprising C 2 -C 6 alkene, water and one or more C 2 -C 6 carboxylic acids, a carboxylic acid separation step which comprises contacting said stream comprising alkene, water and one or more C 2 -C 6 carboxylic acids with a selective solvent, resulting in absorption or extraction of the C 2 -C 6 carboxylic acids by the solvent, a solvent recovery step which comprises separating said absorbed or extracted C 2 -C 6 carboxylic acids from the solvent, resulting in a product stream comprising said one or more C 2 -C 6 carboxylic acids and a stream comprising recovered solvent, and optionally a recycling step which comprises recycling at least a portion of the stream comprising recovered solvent to the carboxylic acid separation step, wherein the selective solvent is an oxygen-containing organic compound having (i) a Hansen solubility parameter distance R a with respect to the C 2 -C 6 carboxylic acid as determined at 25 °C of 15 MPa 1/2 or less, preferably 12 MPa 1/2 or less, more preferably 10 MPa 1/2 or less; (ii) a 1-octanol/water partition coefficient logP ow as determined at 25 °C and pH 7 of at least 0, preferably at least 0.5, more preferably at least 1.0, even more preferably at least 1.5, yet even more preferably at least 2.0, most preferably at least 3.0; and (iii) a boiling point at atmospheric pressure that is at least 5 °C higher, preferably at least 10 °C higher, more preferably at least 20 °C higher than the boiling point of the one or more C 2 -C 6 carboxylic acids.
摘要翻译：本发明提供了用于氧化转化含有2至6个碳原子（“C 2 -C 6”）的烷烃和/或烯烃的方法， “）与C 2 -C 6烯烃和C 2 -C 6羧酸的反应，包括反应该方法包括使包含氧和所述C 2 -C 6烷烃和/或烯烃的物流与混合金属氧化物催化剂接触以产生包含C 2 / 2 -C 6链烯烃，水和一种或多种C 2 -C 6羧酸的羧酸分离步骤，其中羧酸分离步骤包括使包含烯烃，水和一种或多种C 2 -C 6羧酸的所述物流与选择性溶剂接触，导致C 2吸收或提取C 2 通过溶剂回收步骤，所述溶剂回收步骤包括将所述被吸收或提取的C 2 -C 6低聚物分离，来自s的羧酸得到包含所述一种或多种C 2 -C 6羧酸的产物流和包含回收溶剂的物流，以及任选的再循环步骤，所述再循环步骤包括至少再循环所述流的一部分包含回收的溶剂至所述羧酸分离步骤，其中所述选择性溶剂为含氧有机化合物，所述含氧有机化合物具有（i）相对于所述羧酸分离步骤的Hansen溶解度参数距离R a，如在25℃下测定为15MPa 1/2或更低，优选12MPa 1/2或更低，优选12MPa 1/2或更低， 2或更小，更优选10MPa 1/2或更小; （ii）在25℃和pH 7下测定的1-辛醇/水分配系数logP low为至少0，优选至少0.5，更优选至少1.0，甚至更优选在至少1.5，甚至更优选至少2.0，最优选至少3.0; 和（iii）大气压下的沸点比所述一种或多种C

3. 发明申请

WO2018073132A1 THERMOPLASTIC COMPOSITE 审中-公开
标题翻译：热塑性复合材料
公开(公告)号：WO2018073132A1
公开(公告)日：2018-04-26
申请号：PCT/EP2017/076249
申请日：2017-10-13
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： LANGE, Jean Paul, Andre, Marie, Joseph, Ghislain
IPC分类号： C08H8/00 , C08L1/02
CPC分类号： C08L95/00 , C08H8/00 , C08J5/045 , C08J2395/00 , C08J2497/02 , C08L1/02 , C08L2205/16 , C08L97/02
摘要： A reinforced composite material comprises a blend of a thermoplastic matrix and cellulosic fibers, wherein the thermoplastic matrix comprises a tarry residue fraction from a lignocellulosic biomass liquefaction process. A process for the manufacture of the reinforced composite material comprises subjecting a lignocellulosic biomass to liquefaction in the presence of a liquefaction solvent to form a liquefaction product and a tarry residue; separating the tarry residue from the liquefaction product; and blending the tarry residue with cellulosic fibers to form a recyclable reinforced thermoplastic composite material.
摘要翻译：增强复合材料包含热塑性基质和纤维素纤维的共混物，其中热塑性基质包含来自木质纤维素生物质液化方法的焦油残渣部分。制造增强复合材料的方法包括使木质纤维素生物质在液化溶剂存在下液化以形成液化产物和焦油残余物; 从液化产物中分离焦油残渣; 并将焦油残渣与纤维素纤维混合以形成可再循环的增强热塑性复合材料。

4. 发明申请

WO2017134139A1 A METHOD OF PREPARING GLYCOLIC ACID (HOCH2COOH) 审中-公开
标题翻译：一种制备甘油酸（HOCH2COOH）的方法
公开(公告)号：WO2017134139A1
公开(公告)日：2017-08-10
申请号：PCT/EP2017/052210
申请日：2017-02-02
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： LANGE, Jean Paul, Andre, Marie, Joseph, Ghislain , MEURS, Jan, Hermen, Hendrik , RIGUTTO, Marcello, Stefano , STIL, Hans, Arie
IPC分类号： C07C29/149 , C07C51/367 , C07C59/06 , C07C31/20
CPC分类号： C07C51/367 , C07C29/149 , C07C59/06 , C07C31/202
摘要： The present invention provides a method of preparing glycolic acid ( HOCH 2 COOH ), the method at least comprising the steps of: (a) providing an aqueous oxalic acid (HOOCCOOH) containing stream having a molar ratio of water/oxalic acid of above 5.0; (b) subjecting the aqueous oxalic acid (HOOCCOOH) containing stream provided in step (a) to hydrogenation in the presence of a hydrogenation metal catalyst and hydrogen, thereby obtaining a glycolic acid (HOCH 2 COOH ) containing stream; and (c) optionally subjecting the glycolic acid containing stream obtained in step (b) to hydrogenation in the presence of a hydrogenation metal catalyst and hydrogen, thereby obtaining an ethylene glycol ( HOCH 2 CH 2 OH ) containing stream.
摘要翻译：本发明提供了制备乙醇酸（HOCH 2 COOH）的方法，所述方法至少包括以下步骤：（a）提供草酸水溶液（HOOCCOOH ）含水流，其中水/草酸的摩尔比大于5.0; （b）使步骤（a）中提供的含草酸（HOOCCOOH）的含水物流在氢化金属催化剂和氢存在下进行氢化，从而获得含有乙醇酸（HOCHCOOH）的乙醇酸（HOCH 2 COOH）流; 和（c）任选地使在步骤（b）中获得的含乙醇酸的料流在氢化金属催化剂和氢存在下进行氢化，从而获得乙二醇（HOCH 2 CH 2 OH）的流。

5. 发明申请

WO2017114817A1 CARBOXYLIC ACID EXTRACTION FROM AQUEOUS STREAMS 审中-公开
标题翻译：从水流中萃取羧酸
公开(公告)号：WO2017114817A1
公开(公告)日：2017-07-06
申请号：PCT/EP2016/082689
申请日：2016-12-27
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： LANGE, Jean Paul, Andre, Marie, Joseph, Ghislain , FISCHER, Kai, Jürgen , PEREZ GOLF, Carmelo
IPC分类号： C07C57/07 , C07C53/124 , C07C51/12
CPC分类号： C07C51/48 , C07C57/04 , C07C53/124 , C07C53/122 , C07C53/126
摘要： The invention provides a process for the recovery of C 3 -C 6 carboxylic acid from an aqueous stream, comprising providing an aqueous stream comprising C 3 -C 6 carboxylic acid, contacting said aqueous stream comprising C 3 -C 6 carboxylic acid with an extractive solvent in a liquid-liquid extraction unit, to produce a first stream comprising extractive solvent and C 3 -C 6 carboxylic acid and a second stream comprising water, feeding said first stream comprising extractive solvent and C 3 -C 6 carboxylic acid to a solvent recovery unit, to produce a third stream comprising carboxylic acid and a fourth stream comprising extractive solvent, and optionally recycling at least a portion of the fourth stream comprising extractive solvent to the liquid- liquid extraction unit, wherein the extractive solvent is an oxygen-containing organic compound having (i) a Hansen solubility parameter distance R a with respect to the carboxylic acid as determined at 25 °C of MPa 1/2 or less, preferably 12 MPa 1/2 or less, more preferably 10 MPa 1/2 or less; (ii) a 1-octanol/water partition coefficient logP OW as determined at 25 °C and pH 7 of at least 0, preferably at least 0.5, more preferably at least 1.0, even more preferably at least 1.5, yet even more preferably at least 2.0, most preferably at least 3.0; and (iii) a boiling point at atmospheric pressure that is at least 5 °C higher, preferably at least 10 °C higher, more preferably at least 20 °C higher than the boiling point of the C 3 -C 6 carboxylic acid.
摘要翻译：本发明提供了从含水物流中回收C 3 -C 6羧酸的方法，包括提供包含C 使所述包含C 3 -C 6羧酸的含水物流与萃取物溶剂在液 - 液萃取单元中反应以产生包含萃取溶剂和C 3 -C 6羧酸的第一物流和包含水的第二物流，将所述第一物流包括萃取溶剂和C 3 -C 6羧酸至溶剂回收单元，以产生包含羧酸的第三物流和包含萃取溶剂的第四物流，并且任选地再循环所述第四物流的至少一部分包含萃取溶剂到所述液 - 液萃取单元，其中所述萃取溶剂是含氧有机化合物，所述含氧有机化合物具有（i）汉森溶解度参数在25℃下测定的相对于羧酸的三元距离R a为1/2或更小，优选12MPa 1/2或更小，或更低，更优选10MPa 1/2或更低; （ii）如在25℃和pH7下测定的至少0，优选至少0.5，更优选至少1.0，甚至更优选在25℃下测定的1-辛醇/水分配系数logP_00WO 至少1.5，甚至更优选至少2.0，最优选至少3.0; 和（iii）大气压力下的沸点比C 3的沸点高至少5℃，优选至少10℃，更优选至少20℃， C 6 -C 6羧酸。

6. 发明申请

WO2017103009A2 HYDROGENATION OR HYDROGENOLYSIS OF AN OXYGENATE 审中-公开
标题翻译：一种氧化物的氢化或氢解
公开(公告)号：WO2017103009A2
公开(公告)日：2017-06-22
申请号：PCT/EP2016/081294
申请日：2016-12-15
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： DE VLIEGER, Dionysius, Jacobus, Maria , LANGE, Jean Paul, Andre, Marie, Joseph, Ghislain , EDULJI, Smita , COLIJN, Hendrik, Albertus
IPC分类号： C07C29/149
CPC分类号： C07C29/141 , B01J23/462 , Y02P20/52 , C07C31/202
摘要： A process for the hydrogenation or hydrogenolysis of an oxygenate is disclosed. The process takes place in a reactor in the presence of a catalyst, hydrogen and liquid water and the catalyst comprises one or more elements from Groups 8 to 11 of the periodic table dispersed on a hydrothermally stable oxide support.
摘要翻译：公开了一种用于含氧化合物的氢化或氢解的方法。该方法在催化剂，氢和液态水存在下在反应器中进行，催化剂包含分散在水热稳定的氧化物载体上的周期表第8至11族的一种或多种元素。

7. 发明申请

WO2020094526A1 PROCESS FOR THE RECOVERY OF FURFURAL 审中-公开
公开(公告)号：WO2020094526A1
公开(公告)日：2020-05-14
申请号：PCT/EP2019/079990
申请日：2019-11-01
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： CHHEDA, Juben, Nemchand , LANGE, Jean Paul, Andre, Marie, Joseph, Ghislain
IPC分类号： C07D307/48 , C07D307/50
摘要： The present invention relates to a process for the extraction of furfural from a biphasic dehydration reaction mixture in a resource- and energy-efficient manner by the use of one or more adsorption units to increase the recovery of furfural and enrich the furfural content of an organic solvent stream.

8. 发明申请

WO2019030293A1 METHOD FOR PREPARING A CATALYST AND METHOD FOR PRODUCING 1,4-BUTANEDIOL AND/OR TETRAHYDROFURAN FROM FURAN 审中-公开
公开(公告)号：WO2019030293A1
公开(公告)日：2019-02-14
申请号：PCT/EP2018/071531
申请日：2018-08-08
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： VAN GELDER, Jeroen, Karel , LANGE, Jean Paul, Andre, Marie, Joseph, Ghislain , WADMAN, Sipke, Hidde
IPC分类号： B01J23/656 , C07C29/17 , B01J21/18 , B01J35/02 , B01J37/02
摘要： A method for preparing a metal-impregnated, carbon-supported catalyst composition is provided. The method comprises providing a carbon support particle having a smallest dimension of greater than 0.5 millimeters; contacting the carbon support particle with an organic impregnation solution comprising an organic solvent and at least one first metal-containing compound, wherein the first metal-containing compound comprises at least one first metal selected from groups 8, 9 and 10 of the periodic table, to form a first metal-impregnated carbon support particle; and drying the first metal-impregnated carbon support particle.

9. 发明申请

WO2019030289A1 METHOD FOR PREPARING A CATALYST AND METHOD FOR PRODUCING 1,4-BUTANEDIOL AND/OR TETRAHYDROFURAN FROM FURAN 审中-公开
公开(公告)号：WO2019030289A1
公开(公告)日：2019-02-14
申请号：PCT/EP2018/071523
申请日：2018-08-08
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： LANGE, Jean Paul, Andre, Marie, Joseph, Ghislain , WADMAN, Sipke, Hidde , VAN GELDER, Jeroen Karel
IPC分类号： B01J23/656 , C07C29/17 , B01J21/18 , B01J35/02 , B01J37/02
摘要： A method for preparing a metal-impregnated, carbon- supported catalyst composition is provided. The method comprises providing a carbon support particle having a smallest dimension of greater than 0.5 millimeters; contacting the carbon support particle with a basic aqueous impregnation solution comprising a base having a pK b of at most 9 and at least one first metal-containing compound, wherein the first metal-containing compound comprises at least one first metal selected from groups 8, 9 and 10 of the periodic table, to form a first metal-impregnated carbon support particle; and drying the first metal-impregnated carbon support particle.

10. 发明申请

WO2017114820A1 ACETIC ACID EXTRACTION FROM LIQUID AND VAPOROUS AQUEOUS STREAMS 审中-公开
标题翻译：从液体和蒸汽水流中提取乙酸
公开(公告)号：WO2017114820A1
公开(公告)日：2017-07-06
申请号：PCT/EP2016/082692
申请日：2016-12-27
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： FISCHER, Kai, Jürgen , LANGE, Jean Paul, Andre, Marie, Joseph, Ghislain , PEREZ GOLF, Carmelo
IPC分类号： C07C51/43 , C07C51/44 , C07C51/48 , C07C53/08
CPC分类号： C07C51/48 , C07C51/43 , C07C51/44 , C07C53/08
摘要： The invention provides a process for the recovery of acetic acid from a liquid or vaporous aqueous stream, comprising providing a liquid or vaporous aqueous stream comprising acetic acid, contacting said aqueous stream comprising acetic acid with an extractive solvent in an extractive distillation unit, to produce a first stream comprising extractive solvent and acetic acid and a second stream comprising water, feeding said first stream comprising extractive solvent and acetic acid to a solvent recovery unit, to produce a third stream comprising acetic acid and a fourth stream comprising extractive solvent, optionally subjecting the second stream comprising water to a condensation step to allow liquid-liquid separation of entrained extractive solvent and water and optionally recycling at least part of said entrained extractive solvent to the extractive distillation unit, and optionally recycling at least a portion of the fourth stream comprising extractive solvent to the extractive distillation unit, wherein the extractive solvent is an oxygen-containing organic compound having (i) a Hansen solubility parameter distance Ra with respect to acetic acid as determined at 25 °C of 15 MPa 1/2 or less, preferably 12 MPa 1/2 or less, more preferably 10 MPa 1/2 or less; (ii) a 1-octanol/water partition coefficient logP0w as determined at 25 °C and pH 7 of at least 0, preferably at least 0.5, more preferably at least 1.0, even more preferably at least 1.5, yet even more preferably at least 2.0, most preferably at least 3.0; and (iii) a boiling point at atmospheric pressure that is least 5 °C higher, preferably at least 10 °C higher, more preferably at least 20 °C higher than the boiling point of acetic acid.
摘要翻译：本发明提供了从液体或蒸气水流中回收乙酸的方法，包括提供包含乙酸的液体或蒸气水流，使所述包含乙酸的水流与萃取溶剂在萃取蒸馏单元中，产生包含萃取溶剂和乙酸的第一物流和包含水的第二物流，将包含萃取溶剂和乙酸的所述第一物流供给至溶剂回收单元，以产生包含乙酸和第四物流包含萃取溶剂，任选地使包含水的第二物流经历冷凝步骤以允许夹带的萃取溶剂和水的液 - 液分离并且任选地将至少部分所述夹带的萃取溶剂再循环至萃取蒸馏单元，将第四物流的至少一部分包含萃取溶剂到达萃取蒸馏单元，其中萃取溶剂为含氧有机化合物，其具有（i）在25℃下测定的相对于乙酸的汉森溶解度参数距离Ra为15MPa 1/2 / 或更小，优选12MPa 1/2或更小，更优选10MPa 1/2或更小; （ii）如在25℃和pH 7下测定的至少0，优选至少0.5，更优选至少1.0，甚至更优选至少1.5，还甚至更优选在20℃下测定的1-辛醇/水分配系数logP 0 w 至少2.0，最优选至少3.0; 和（iii）大气压下的沸点比乙酸的沸点高至少5℃，优选高至少10℃，更优选高至少20℃。

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