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1. 发明申请

WO2008005549A2 FLAVOR OILS WITH REDUCED SULFUR CONTENT AND USE IN ORAL CARE COMPOSITIONS 审中-公开
标题翻译：具有减少硫含量的油脂和口服护理组合物中的用途
公开(公告)号：WO2008005549A2
公开(公告)日：2008-01-10
申请号：PCT/US2007015601
申请日：2007-07-06
申请人： PROCTER & GAMBLE , SWAINE ROBERT LESLIE JR , ZEHENTBAUER GERHARD NORBERT , HOKE II STEVEN HAMILTON , HESTER MARC ALAN , RAMJI NIRANJAN , MCCLENATHAN DENISE MARIE
发明人： SWAINE ROBERT LESLIE JR , ZEHENTBAUER GERHARD NORBERT , HOKE II STEVEN HAMILTON , HESTER MARC ALAN , RAMJI NIRANJAN , MCCLENATHAN DENISE MARIE
CPC分类号： A23L1/222 , A23L27/12 , A23V2002/00 , A61K8/19 , A61K8/33 , A61K8/347 , A61K8/35 , A61K8/4973 , A61K8/676 , A61K8/922 , A61K2800/52 , A61Q11/00 , A23V2200/15 , A23V2250/5036 , A23V2250/2116 , A23V2250/214
摘要： The present invention relates to flavor oils including mint-, fruit- and spice-type flavors that are specially processed to substantially eliminate low-molecular weight sulfur compounds, in particular dimethyl sulfoxide (DMSO), which has been found to be the main precursor of malodorous species such as dimethyl sulfide and methyl mercaptan. These malodorous species are produced via oxidation-reduction reactions involving such sulfur-containing compounds present in flavor oils. A preferred processing method is an aqueous-washing process, which has advantages of being simple, inexpensive and easy to implement while importantly avoiding the problems of typical processes including non-selective removal of desirable components and subjecting the flavor oils to extreme conditions that may destroy other components and result in undesirable changes in flavor or odor character. Other processing methods to selectively remove non-desired components include (1) distillation to remove polar low boiling point components, (2) filtration through adsorbents selective for sulfur compounds, (3) countercurrent extraction and (4) column chromatography. The processing methods may optionally be followed by reengineering to add back desired components that may have been removed or altered during the processing. The specially processed flavor oils are particularly useful in oral care compositions comprising components with chemical reducing capability such as stannous ions, which react with the sulfur-containing compounds to produce malodorous products.
摘要翻译：本发明涉及风味油，其包括经特别加工以基本上消除低分子量硫化合物，特别是二甲基亚砜（DMSO）的薄荷，水果和香料型香料，其已被发现是主要前体恶臭物质如二甲硫醚和甲硫醇。这些恶臭物质通过涉及风味油中存在的含硫化合物的氧化还原反应产生。优选的处理方法是水洗方法，其优点是简单，便宜且易于实施，同时重要地避免了典型方法的问题，包括非选择性除去所需组分并使风味油经受可能破坏的极端条件其他组分，并导致风味或气味特征的不良变化。选择性除去不需要的组分的其它处理方法包括（1）蒸馏以除去极性低沸点组分，（2）通过对硫化合物选择性的吸附剂进行过滤，（3）逆流提取和（4）柱色谱法。处理方法可以可选地随后重新设计以添加可能在处理期间被移除或改变的期望的部件。经特殊处理的风味油特别适用于包含具有化学还原能力的组分的口腔护理组合物，例如亚锡离子，其与含硫化合物反应产生恶臭产物。

2. 发明申请

WO2008005550A3 FLAVOR OILS WITH REDUCED SULFUR CONTENT AND USE IN ORAL CARE COMPOSITIONS 审中-公开
公开(公告)号：WO2008005550A3
公开(公告)日：2008-07-03
申请号：PCT/US2007015603
申请日：2007-07-06
申请人： PROCTER & GAMBLE , HOKE II STEVEN HAMILTON , HESTER MARC ALAN , RAMJI NIRANJAN
发明人： HOKE II STEVEN HAMILTON , HESTER MARC ALAN , RAMJI NIRANJAN
IPC分类号： C11B9/02 , A23L1/221 , A61K8/97 , A61Q11/00 , C11B3/00
CPC分类号： A23L1/222 , A23L27/12 , A23V2002/00 , A61K8/19 , A61K8/33 , A61K8/347 , A61K8/35 , A61K8/4973 , A61K8/676 , A61K8/922 , A61K2800/52 , A61Q11/00 , A23V2200/15 , A23V2250/5036 , A23V2250/2116 , A23V2250/214
摘要： The present invention relates to flavor oils including mint-, fruit- and spice-type flavors that are specially processed to substantially eliminate low-molecular weight sulfur compounds, in particular dimethyl sulfoxide (DMSO), which has been found to be the main precursor of malodorous species such as dimethyl sulfide and methyl mercaptan. These malodorous species are produced via oxidation-reduction reactions involving such sulfur-containing compounds present in flavor oils. A preferred processing method is an aqueous-washing process, which has advantages of being simple, inexpensive and easy to implement while importantly avoiding the problems of typical processes including non-selective removal of desirable components and subjecting the flavor oils to extreme conditions that may destroy other components and result in undesirable changes in flavor or odor character. Other processing methods to selectively remove non-desired components include (1) distillation to remove polar low boiling point components, (2) filtration through adsorbents selective for sulfur compounds, (3) countercurrent extraction and (4) column chromatography. The processing methods may optionally be followed by reengineering to add back desired components that may have been removed or altered during the processing. The specially processed flavor oils are particularly useful in oral care compositions comprising components with chemical reducing capability such as stannous ions, which react with the sulfur-containing compounds to produce malodorous products.

3. 发明申请

WO2013019953A3 WATER-SOLUBLE SURFACTANT COMPOSITIONS HAVING IMPROVED TASTE 审中-公开
标题翻译：具有改善味道的水溶性表面活性剂组合物
公开(公告)号：WO2013019953A3
公开(公告)日：2013-09-12
申请号：PCT/US2012049330
申请日：2012-08-02
申请人： PROCTER & GAMBLE , HOKE II STEVEN HAMILTON , HAUGHT JOHN CHRISTIAN , HESTER MARC ALAN , CLAIR BRIAN DAVID
发明人： HOKE II STEVEN HAMILTON , HAUGHT JOHN CHRISTIAN , HESTER MARC ALAN , CLAIR BRIAN DAVID
IPC分类号： A61K8/55 , A61K8/41 , A61K8/44 , A61Q11/00 , A61Q11/02
CPC分类号： A61K8/55 , A61K8/41 , A61K8/44 , A61K8/556 , A61K2800/596 , A61Q11/00 , A61Q11/02
摘要： Treated surfactant composition containing a water-soluble surfactant and exhibiting improved taste, said composition comprising: a water-soluble surfactant selected from alkyl phosphate surfactants, alkyl phosphate ethoxylated surfactants, betaine surfactants, betaine ethoxylated surfactants, amine oxide surfactants, and mixtures thereof and water; wherein the composition further comprises: less than about 4%, by weight of the water-soluble surfactant, of total undesirable non-polar materials; less than about 2.5%, by weight of the water-soluble surfactant, of alcohols having a carbon chain length of greater than 4; less than about 1%, by weight of the water-soluble surfactant, of amine and amide materials; and less than about 1%, by weight of the water-soluble surfactant, undesirable non-polar materials selected from aldehydes, esters, ketones, and organic acids. Such compositions wherein the compositions have been subjected to liquid-liquid extraction processes.
摘要翻译：所述组合物包含：选自烷基磷酸酯表面活性剂，烷基磷酸酯乙氧基化表面活性剂，甜菜碱表面活性剂，甜菜碱乙氧基化表面活性剂，氧化胺表面活性剂及其混合物和水的水溶性表面活性剂，所述表面活性剂组合物包含水溶性表面活性剂， ; 其中所述组合物进一步包含：小于约4重量％的水溶性表面活性剂，总不希望的非极性物质; 小于约2.5％重量的水溶性表面活性剂的碳链长度大于4的醇; 小于约1重量％的水溶性表面活性剂的胺和酰胺材料; 和小于约1重量％的水溶性表面活性剂，选自醛，酯，酮和有机酸的不希望的非极性物质。其中组合物已经进行液 - 液萃取过程的这样的组合物。

4. 发明申请

WO2013019940A3 LIQUID-LIQUID EXTRACTION COMPOSITION USEFUL IN PROCESSING WATER-SOLUBLE SURFACTANTS 审中-公开
标题翻译：液体液体萃取组合物可用于加工水溶性表面活性剂
公开(公告)号：WO2013019940A3
公开(公告)日：2013-06-13
申请号：PCT/US2012049314
申请日：2012-08-02
申请人： PROCTER & GAMBLE , HOKE STEVEN HAMILTON II , HAUGHT JOHN CHRISTIAN , HESTER MARC ALAN , CLAIR BRIAN DAVID
发明人： HOKE STEVEN HAMILTON II , HAUGHT JOHN CHRISTIAN , HESTER MARC ALAN , CLAIR BRIAN DAVID
IPC分类号： B01D11/04 , A61Q11/02 , C11D3/43
CPC分类号： B01D11/0407
摘要： Compositions useful in liquid-liquid extraction processes for improving the taste of water-soluble surfactants, said composition comprising: from about 5% to about 60%, by weight of the composition, of water soluble surfactant; from about 10% to about 90%, by weight of the composition, of water; from about 10% to about 90%, by weight of the composition, of extraction solvent; at least 0.01%, by weight of the composition, of undesirable non-polar materials; wherein the extraction solvent is selected from solvents having individual Hansen solubility parameters of a dispersion force component (?D) ranging from about 15 to about 17 (MPa)0.5, a polar component (deltaP) ranging from 0 to about 9 (MPa)0.5 and a hydrogen bonding component (deltaH) ranging from 0 to about 11 (MPa)0.5.
摘要翻译：用于提高水溶性表面活性剂的味道的液体 - 液体萃取方法中的组合物，所述组合物包含：组合物重量的约5％至约60％的水溶性表面活性剂; 约10重量％至约90重量％的水; 约10重量％至约90重量％的提取溶剂; 至少0.01重量％的组合物，不期望的非极性材料; 其中萃取溶剂选自具有约15至约17（MPa）0.5范围内的分散力组分（ΔD）的单独Hansen溶解度参数的溶剂，范围为0至约9（MPa）0.5的极性组分（δP）和氢键组分（δH）为0至约11（MPa）0.5。

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