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1. 发明申请

WO2014113795A1 PROCESS FOR PREPARING A MULTI-LAYER ELECTROCHROMIC STRUCTURE 审中-公开
标题翻译：制备多层电致发光结构的方法
公开(公告)号：WO2014113795A1
公开(公告)日：2014-07-24
申请号：PCT/US2014/012338
申请日：2014-01-21
申请人： KINESTRAL TECHNOLOGIES, INC.
发明人： CHOI, Hye Jin , BAILEY, Mark , BASS, John, David , VON KUGELGEN, Stephen, Winthrop , LACHMAN, Eric , TURNER, Howard, W.
IPC分类号： G02F1/15
CPC分类号： G02F1/1523
摘要： A wet chemistry process for preparing a multi-layer electrochromic structure comprising depositing a film of a liquid mixture comprising lithium, nickel, and at least one bleached state stabilizing element on a surface of a substrate and treating the deposited film to form an anodic electrochromic layer comprising a lithium nickel oxide composition on the surface of the substrate, the anodic electrochromic layer comprising lithium, nickel and the bleached state stabilizing element(s) wherein (i) the atomic ratio of lithium to the combined amount of nickel and the bleached state stabilizing element(s) in the lithium nickel oxide composition is at least 0.4:1, respectively, (ii) the atomic ratio of the combined amount of the bleached state stabilizing element(s) to the combined amount of nickel and the bleached state stabilizing elements in the lithium nickel oxide composition is at least about 0.025:1, respectively, and (iii) the bleached state stabilizing element(s) is/are selected from the group consisting of Y, Ti, Zr, Hf, V, Nb, Ta, Mo, W, B, Al, Ga, In, Si, Ge, Sn, P, Sb and combinations thereof.
摘要翻译：一种用于制备多层电致变色结构的湿式化学方法，包括在基材的表面上沉积包含锂，镍和至少一种漂白状态稳定元素的液体混合物的膜，并处理沉积膜以形成阳极电致变色层在基底表面上包含锂镍氧化物组合物，阳极电致变色层包含锂，镍和漂白状态稳定元素，其中（i）锂与镍的组合量的原子比和漂白状态稳定锂镍氧化物组合物中的元素分别为至少0.4:1，（ii）漂白状态稳定化元素的组合量与镍和漂白状态稳定元素的组合量的原子比在锂镍氧化物组合物中分别为至少约0.025:1，和（iii）漂白状态稳定化元素选自 m，由Y，Ti，Zr，Hf，V，Nb，Ta，Mo，W，B，Al，Ga，In，Si，Ge，Sn，P，Sb及其组合组成的组。

2. 发明申请

WO2014113801A1 ELECTROCHROMIC LITHIUM NICKEL GROUP 4 MIXED METAL OXIDES 审中-公开
标题翻译：电致发光镍铬合金组4混合金属氧化物
公开(公告)号：WO2014113801A1
公开(公告)日：2014-07-24
申请号：PCT/US2014/012351
申请日：2014-01-21
申请人： KINESTRAL TECHNOLOGIES, INC.
发明人： CHOI, Hye, Jin , BAILEY, Mark , BASS, John, David , VON KUGELGEN, Stephen, Winthrop , LACHMAN, Eric , TURNER, Howard, W. , BIGI, Julian, P.
IPC分类号： G02F1/15
CPC分类号： G02F1/1523 , C01G53/42 , C09K9/00 , Y10T428/265
摘要： Multi-layer electrochromic structures comprising an anodic electrochromic layer comprising a lithium nickel oxide composition on a first substrate, the anodic electrochromic layer comprising lithium, nickel and a Group 4 metal selected from titanium, zirconium, hafnium and a combination thereof, wherein (i) the atomic ratio of lithium to the combined amount of nickel and such Group 4 metal(s) in the anodic electrochromic layer is at least 0.4:1, respectively, (ii) the atomic ratio of the amount of such Group 4 metal(s) to the combined amount of nickel and such Group 4 metal(s) in the anodic electrochromic layer is at least about 0.025:1, respectively, and (iii) the anodic electrochromic layer exhibits an interplanar distance (d-spacing) of at least 2.5 Å as measured by X-ray diffraction (XRD), comprises at least 0.05 wt.% carbon, and/or has a coloration efficiency absolute value of at least 19 cm 2 /C.
摘要翻译：多层电致变色结构包括在第一衬底上包含锂镍氧化物组合物的阳极电致变色层，所述阳极电致变色层包含锂，镍和选自钛，锆，铪的第4族金属及其组合，其中（i）阳极电致变色层中锂与镍的组合量和4族金属的原子比分别为0.4：1以上，（ii）4族金属的原子比，至镍的组合量和阳极电致变色层中的这种第4族金属分别为至少约0.025:1，（iii）阳极电致变色层的平面间距（d-间距）至少为2.5 通过X射线衍射（XRD）测量，包含至少0.05重量％的碳，和/或具有至少19cm 2 /℃的着色效率绝对值。

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