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1. 发明申请

WO2008051432A3 PATTERNING OF IONIC POLYMERS 审中-公开
标题翻译：离子聚合物的构图
公开(公告)号：WO2008051432A3
公开(公告)日：2009-04-09
申请号：PCT/US2007022219
申请日：2007-10-18
申请人： HARVARD COLLEGE , LAHAV MICHAL , WINKLEMAN ADAM , NAROVLYANSKY MAX , PEREZ-CASTILLEJOS RAQUEL , WEISS EMILY A , RODRIGUEZ LEONARD N J , WHITESIDES GEORGE M
发明人： LAHAV MICHAL , WINKLEMAN ADAM , NAROVLYANSKY MAX , PEREZ-CASTILLEJOS RAQUEL , WEISS EMILY A , RODRIGUEZ LEONARD N J , WHITESIDES GEORGE M
IPC分类号： G03F7/00
CPC分类号： G03F7/0002 , B82Y10/00 , B82Y40/00 , Y10T428/24479
摘要： In one aspect, methods of patterning of thin films of an ionotropic polymer (e.g., poly(acrylic acid)) are provided. These processes can create micron or sub-micron-scale patterns of ionotropic polymers such as cation crosslinked poly(acrylic acid) (CCL- PAA). In one embodiment, patterning may be performed within microfluidic channels by flowing a solution of crosslinking agent (e.g., metal cations such as Ag+, Ca2+, Pd2+, Al3+, La3+, and Ti4+) that can crosslink a portion of an ionotropic polymer in contact with the solution. In another embodiment, methods of patterning ionotropic polymers involve photolithography. Upon patterning a positive photoresist (e.g., diazonaphthoquinone- novolac resin) on a film of CCL-PAA, the exposed regions of CCL-PAA can be etched by an aqueous solution. Advantageously, the patterned, crosslinked polymer may also serve as both a reactant and a matrix for subsequent chemistry. For example, in some embodiments, the initial crosslinking cation can be exchanged for a second cation that could not be patterned photolithographically. Patterned films of CCL-PAA can also be used to host and template the reduction of metallic cations to metallic nanoparticles, and to fabricate porous, low-k dielectric substrates.
摘要翻译：一方面，提供了离子型聚合物（例如聚（丙烯酸））的薄膜图案化方法。这些方法可以产生离子型聚合物如阳离子交联的聚（丙烯酸）（CCL-PAA）的微米级或亚微米级的图案。在一个实施方案中，可以在微流体通道内通过使交联剂（例如金属阳离子如Ag +，Ca 2+，Pd 2+，Al 3+，La 3+和Ti 4+）的溶液流过微流体通道，所述溶液可以将部分离子型聚合物与解决方案。在另一个实施方案中，构图离子型聚合物的方法涉及光刻。在CCL-PAA膜上形成正性光致抗蚀剂（例如重氮萘酚 - 酚醛清漆树脂）之后，CCL-PAA的曝光区域可以通过水溶液进行蚀刻。有利地，图案化的交联聚合物也可以用作反应物和用于后续化学的基质。例如，在一些实施方案中，可以将初始交联阳离子交换为不能光刻图案化的第二阳离子。 CCL-PAA的图案化膜也可用于将金属阳离子还原为金属纳米颗粒，并制备多孔，低k电介质基底。

2. 发明申请

WO2009006409A2 DENSITY-BASED METHODS FOR SEPARATION OF MATERIALS, MONITORING OF SOLID SUPPORTED REACTIONS AND MEASURING DENSITIES OF SMALL LIQUID VOLUMES AND SOLIDS 审中-公开
标题翻译：基于密度的方法分离材料，监测固体支撑反应和测量小液体体积和固体密度
公开(公告)号：WO2009006409A2
公开(公告)日：2009-01-08
申请号：PCT/US2008068797
申请日：2008-06-30
申请人： HARVARD COLLEGE , PHILLIPS SCOTT T , WHITESIDES GEORGE M , MIRICA KATHERINE A , CARRILHO EMANUEL , MARTINEZ ANDRES W , SHEVKOPLYAS SERGEY S , SNYDER PHILLIP W , PEREZ-CASTILLEJOS RAQUEL , GUPTA MALANCHA , WINKLEMAN ADAM , GUDIKSEN KATHERINE L
发明人： PHILLIPS SCOTT T , WHITESIDES GEORGE M , MIRICA KATHERINE A , CARRILHO EMANUEL , MARTINEZ ANDRES W , SHEVKOPLYAS SERGEY S , SNYDER PHILLIP W , PEREZ-CASTILLEJOS RAQUEL , GUPTA MALANCHA , WINKLEMAN ADAM , GUDIKSEN KATHERINE L
IPC分类号： G01N33/53
CPC分类号： G01N33/5434 , B01L3/502761 , B01L3/502776 , B01L3/50825 , B01L2200/0652 , B01L2300/045 , B01L2300/0877 , B01L2300/089 , B01L2400/043 , B01L2400/0457 , B01L2400/0487 , G01N33/54333 , G01R33/1269
摘要： The ability to levitate, to separate, and to detect changes in density using diamagnetic particles suspended in solutions containing paramagnetic cations using an inhomogeneous magnetic field is described. The major advantages of this separation device are that: i) it is a simple apparatus that does not require electric power (a set of permanent magnets and gravity are sufficient for the diamagnetic separation and collection system to work); ii) it is compatible with simple optical detection (provided that transparent materials are used to fabricate the containers/channels where separation occurs; iii) it is simple to collect the separated particles for further processing; iv) it does not require magnetic labeling of the particles/materials; and v) it is small, portable. The method and kits provided provide for separation and collection of materials of different densities, diagnostics for detection of analytes of interest, monitoring of solid-supported chemical reactions and determination of densities of solid and liquid mixtures.
摘要翻译：描述了悬浮在使用不均匀磁场的含有顺磁性阳离子的溶液中的反磁性粒子悬浮，分离和检测密度变化的能力。该分离装置的主要优点是：i）它是一种不需要电力的简单装置（一组永磁体和重力足以使抗磁分离和收集系统工作）; ii）它与简单的光学检测兼容（只要透明材料用于制造分离发生的容器/通道; iii）收集分离的颗粒以便进一步处理是简单的; iv）它不需要磁性标记颗粒/材料; 和v）它小巧便携。所提供的方法和试剂盒用于分离和收集不同密度的物质，用于检测感兴趣分析物的诊断，固体支持的化学反应的监测以及固体和液体混合物密度的测定。

3. 发明申请

WO2008045745A2 CHEMICALLY-DIRECTED ELECTROSTATIC SELF-ASSEMBLY OF MATERIALS 审中-公开
标题翻译：化学静电自组装材料
公开(公告)号：WO2008045745A2
公开(公告)日：2008-04-17
申请号：PCT/US2007080392
申请日：2007-10-04
申请人： HARVARD COLLEGE , MCCARTY LOGAN S , WHITESIDES GEORGE M , WINKLEMAN ADAM
发明人： MCCARTY LOGAN S , WHITESIDES GEORGE M , WINKLEMAN ADAM
CPC分类号： B05D1/185 , B82Y30/00 , B82Y40/00 , Y10T156/10 , Y10T428/24942
摘要： A self-assembled article includes a surface comprising an chemical functionality having an immobilized charge; and a plurality of particles assembled on the surface of the core, said particles having a surface comprising an immobilized chemical functionality of a charge opposite that of the core.
摘要翻译：自组装制品包括包含具有固定电荷的化学官能团的表面; 以及组装在芯的表面上的多个颗粒，所述颗粒具有表面，其包含电荷相对于芯的电荷的固定化学官能团。

4. 发明申请

WO2007021741A3 METHODS OF USING A NANOTRANSFER PRINTING STAMP HAVING CONDUCTIVELY COATED SIDEWALLS 审中-公开
标题翻译：使用具有导电涂层的纳米级印刷印章的方法
公开(公告)号：WO2007021741A3
公开(公告)日：2007-05-31
申请号：PCT/US2006031028
申请日：2006-08-09
申请人： HARVARD COLLEGE , CAO TINGBING , XU QIAOBING , WINKLEMAN ADAM , WHITESIDES GEORGE
发明人： CAO TINGBING , XU QIAOBING , WINKLEMAN ADAM , WHITESIDES GEORGE
IPC分类号： G03F7/00
CPC分类号： C23C14/20 , B82Y30/00 , C23C14/0005 , C23C14/588 , G01N33/48707 , H01L21/76838
摘要： The known method of nanotransfer printing uses a stamp (10), coated with a metallic layer (40) of less than 10 nm thickness, to transfer the layer (40) from the raised portions (25) of the stamp (10) to a second surface (45). According to the present invention, the remaining layer on the sidewalls (35) and in the recessed portions (30) of the stamp (10) can be used for charge printing on a layer (65) of a material (60), or it can be used as electrodes in chemical and biological measurements.
摘要翻译：已知的纳米转印方法使用涂覆有小于10nm厚度的金属层（40）的印模（10），以将层（40）从印模（10）的凸起部分（25）转移到第二表面（45）。根据本发明，印模（10）的侧壁（35）和凹部（30）中的剩余层可以用于在材料（60）的层（65）上进行电荷印刷，或者可用作化学和生物测量中的电极。

5. 发明申请

WO2009113063A3 METHOD FOR FABRICATING NANO-SCALE PATTERNED SURFACES 审中-公开
标题翻译：用于制作纳米尺度图形表面的方法
公开(公告)号：WO2009113063A3
公开(公告)日：2010-08-19
申请号：PCT/IL2009000269
申请日：2009-03-10
申请人： YEDA RES & DEV COMPANY LTD N , NAAMAN RON , GOLAN BEN , FRADKLIN ZEEV , WINKLEMAN ADAM , ORON DAN
发明人： NAAMAN RON , GOLAN BEN , FRADKLIN ZEEV , WINKLEMAN ADAM , ORON DAN
IPC分类号： B81C1/00 , H01J1/304 , H01J1/34
CPC分类号： B81C1/00206 , B81C1/00031 , B81C2201/0132 , B81C2201/115 , G03F7/40
摘要： A method for fabrication of substrate having a nano-scale surface roughness is presented. The method comprises: patterning a surface of a substrate to create an array of spaced-apart regions of a light sensitive material; applying a controllable etching to the patterned surface, said controllable etching being of a predetermined duration selected so as to form a pattern with nano-scale features; and removing the light sensitive material, thereby creating a structure with the nano-scale surface roughness. Silanizing such nano-scale roughness surface with hydrophobic molecules results in the creation of super- hydrophobic properties characterized by both a large contact angle and a large tilting angle. Also, deposition of a photo-active material on the nano-scale roughness surface results in a photocathode with enhanced photoemission yield. This method also provides for fabrication of a photocathode insensitive to polarization of incident light.
摘要翻译：提出了一种具有纳米级表面粗糙度的基板的制造方法。该方法包括：图案化基板的表面以产生光敏材料的间隔开的区域的阵列; 对所述图案化表面施加可控制的蚀刻，所述可控蚀刻具有预定的持续时间，以便形成具有纳米尺度特征的图案; 并去除感光材料，从而产生具有纳米级表面粗糙度的结构。用疏水性分子对这样的纳米级粗糙表面进行硅烷化，导致产生了以接触角大和倾斜角大的特征的超疏水特性。而且，在纳米级粗糙度表面上沉积光活性材料导致光电阴极具有增强的光电转换率。该方法还提供对入射光的偏振不敏感的光电阴极的制造。

6. 发明申请

WO2009113063A8 METHOD FOR FABRICATING NANO-SCALE PATTERNED SURFACES 审中-公开
标题翻译：制造纳米图案化表面的方法
公开(公告)号：WO2009113063A8
公开(公告)日：2009-11-26
申请号：PCT/IL2009000269
申请日：2009-03-10
申请人： YEDA RES & DEV COMPANY LTD N , NAAMAN RON , GOLAN BEN , FRADKLIN ZEEV , WINKLEMAN ADAM , ORON DAN
发明人： NAAMAN RON , GOLAN BEN , FRADKLIN ZEEV , WINKLEMAN ADAM , ORON DAN
IPC分类号： B81C1/00
CPC分类号： B81C1/00206 , B81C1/00031 , B81C2201/0132 , B81C2201/115 , G03F7/40
摘要： A method for fabrication of substrate having a nano-scale surface roughness is presented. The method comprises: patterning a surface of a substrate to create an array of spaced-apart regions of a light sensitive material; applying a controllable etching to the patterned surface, said controllable etching being of a predetermined duration selected so as to form a pattern with nano-scale features; and removing the light sensitive material, thereby creating a structure with the nano-scale surface roughness. Silanizing such nano-scale roughness surface with hydrophobic molecules results in the creation of super- hydrophobic properties characterized by both a large contact angle and a large tilting angle. Also, deposition of a photo-active material on the nano-scale roughness surface results in a photocathode with enhanced photoemission yield. This method also provides for fabrication of a photocathode insensitive to polarization of incident light.
摘要翻译：提出了一种制造具有纳米级表面粗糙度的基板的方法。该方法包括：图案化衬底的表面以形成光敏材料的间隔开的区域的阵列; 对图案化表面施加可控蚀刻，所述可控蚀刻具有预定的持续时间，以便形成具有纳米级特征的图案; 并去除光敏材料，从而形成具有纳米级表面粗糙度的结构。用疏水分子将这种纳米级粗糙表面硅烷化导致产生以大接触角和大倾角为特征的超疏水特性。而且，在纳米级粗糙表面上沉积光敏材料导致光电阴极具有增强的光电发射产率。该方法还提供了制造对入射光的偏振不敏感的光电阴极。

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