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1. 发明申请

WO2007094950A1 A HIGH THROUGHPUT PROCESS FOR MANUFACTURING MOLECULAR SIEVES 审中-公开
标题翻译：用于制造分子筛的高速加工方法
公开(公告)号：WO2007094950A1
公开(公告)日：2007-08-23
申请号：PCT/US2007/002340
申请日：2007-01-29
申请人： EXXONMOBIL CHEMICAL PATENTS INC. , JOHNSON, Ivy, D. , LAI, Wenyih, Frank
发明人： JOHNSON, Ivy, D. , LAI, Wenyih, Frank
IPC分类号： B01J37/10 , B01J29/06 , C01B39/02
CPC分类号： C07B37/04 , B01J20/3028 , B01J29/04 , B01J29/06 , B01J29/40 , B01J29/7023 , B01J29/7038 , B01J29/80 , B01J29/86 , C01B37/02 , C01B39/02 , C01B39/04 , C01B39/40 , C07C2/66 , C07C6/126 , C07C29/36 , C07C51/235 , C09B67/0073 , C09B67/0096 , C10G45/64 , Y02P20/52 , C07C15/02 , C07C15/107 , C07C15/085 , C07C57/30 , C07C33/20
摘要： A method of crystallizing a crystalline molecular sieve having a pore size in the range of from about 2 to about 19 A, said method comprising the steps of (a) providing a mixture comprising at least one source of ions of tetravalent element (Y), at least one hydroxide source (OH'), and water, said mixture having a solid-content in the range of from about 15 wt.% to about 50 wt.%; and (b) treating said mixture to form the desired crystalline molecular sieve with stirring at crystallization conditions sufficient to obtain a weight hourly throughput from about 0.005 to about 1 hr - 1 , wherein said crystallization conditions comprise a temperature in the range of from about 200°C to about 500°C and a crystallization time less than 100 hr.
摘要翻译：一种结晶分子筛的方法，其结晶分子筛的孔径在约2至约19的范围内，所述方法包括以下步骤：（a）提供包含至少一种四价元素（Y）离子源的混合物，至少一种氢氧化物源（OH'）和水，所述混合物的固体含量范围为约15重量％至约50重量％; 和（b）在结晶条件下搅拌处理所述混合物以形成所需的结晶分子筛，其结晶条件足以获得约0.005至约1小时的重量小时产量。

2. 发明申请

WO2013039673A1 IMPROVED LIQUID PHASE ALKYLATION PROCESS 审中-公开
标题翻译：改进的液相烷基化方法
公开(公告)号：WO2013039673A1
公开(公告)日：2013-03-21
申请号：PCT/US2012/052334
申请日：2012-08-24
申请人： EXXONMOBIL CHEMICAL PATENTS INC. , VINCENT, Matthew, J. , HELTON, Terry, E. , JOHNSON, Ivy, D.
发明人： VINCENT, Matthew, J. , HELTON, Terry, E. , JOHNSON, Ivy, D.
IPC分类号： C01B39/48
CPC分类号： C01B39/48 , B01J29/70 , B01J2229/42
摘要： The present invention provides a process for producing a monoalkylated aromatic compound comprising the step of contacting an alkylatable aromatic compound with an alkylating agent in the presence of a catalyst composition under effective alkylation conditions, said catalyst composition comprising MCM-56 crystals produced by a seeded synthesis method and a binder, such that the crystal/binder weight ratio in the catalyst composition is from above 20/80 to about 80/20.
摘要翻译：本发明提供一种制备单烷基化芳族化合物的方法，包括在有效的烷基化条件下在催化剂组合物存在下使烷基化芳族化合物与烷基化剂接触的步骤，所述催化剂组合物包含通过接种合成产生的MCM-56晶体方法和粘合剂，使得催化剂组合物中的结晶/粘合剂重量比高于20/80至约80/20。

3. 发明申请

WO2004046034A1 HIGH ACTIVITY SMALL CRYSTAL ZSM-12 审中-公开
标题翻译：高活性小水晶ZSM-12
公开(公告)号：WO2004046034A1
公开(公告)日：2004-06-03
申请号：PCT/US2003/032853
申请日：2003-10-17
申请人： EXXONMOBIL CHEMICAL PATENTS INC. , JOHNSON, Ivy, D. , LAI, Wenyih, F.
发明人： JOHNSON, Ivy, D. , LAI, Wenyih, F.
IPC分类号： C01B39/42
CPC分类号： C07C6/126 , B01J23/80 , B01J29/7034 , B01J29/80 , B01J35/002 , B01J2229/20 , B01J2229/42 , C01B39/42 , C10G45/64 , C10G2400/30 , Y02P20/52 , Y10S423/33 , C07C15/08
摘要： A porous, crystalline material is described having the framework structure of ZSM-12 and a composition involving the molar relationship: X 2 0 3 :(n)Y0 2 wherein X is a trivalent element, Y is a tetravalent element and n is less than 60. The material has an average crystal size of the material is less than 0.1 micron and a Diffusion Parameter for mesitylene of at least 1000 x 10 -6 sec -1 when measured at a temperature of 100°C and a mesitylene pressure of 2 torr.
摘要翻译：描述了具有ZSM-12的骨架结构和涉及摩尔关系的组成的多孔结晶材料：X203：（n）Y02其中X是三价元素，Y是四价元素，n小于60.材料当在100℃的温度和2托的均三甲苯压力下测量时，材料的平均晶体尺寸小于0.1微米，均三甲苯的扩散参数为至少1000×10 -6秒-1 。

4. 发明申请

WO2008016477A2 A NOVEL MOLECULAR SIEVE COMPOSITION, A METHOD OF MAKING AND A PROCESS OF USING THE SAME 审中-公开
标题翻译：新型分子筛组合物，其制备方法及其使用方法
公开(公告)号：WO2008016477A2
公开(公告)日：2008-02-07
申请号：PCT/US2007/016004
申请日：2007-07-13
申请人： EXXONMOBIL CHEMICAL PATENTS INC. , ROTH, Wieslaw, J. , MERTENS, Machteld, M. , DE CLERCK, Els, C. , JOHNSON, Ivy, D.
发明人： ROTH, Wieslaw, J. , MERTENS, Machteld, M. , DE CLERCK, Els, C. , JOHNSON, Ivy, D.
IPC分类号： B01J29/70 , B01J35/00 , C01B39/48
CPC分类号： B01J29/7038 , B01J29/047 , B01J35/002 , C01B39/06 , C01B39/48 , C07C2/66 , C07C6/123 , C07C29/36 , C07C37/08 , C07C37/11 , C07C37/14 , C07C37/20 , C07C41/06 , C07C57/30 , C07C263/20 , C07C2529/70 , Y02P20/52 , C07C265/14 , C07C39/06 , C07C43/046 , C07C33/20 , C07C39/04 , C07C39/16
摘要： This disclosure relates to a crystalline MCM-22 family molecular sieve composition having, in its as-synthesized form, an X-ray diffraction pattern including a peak at d-spacing maximum of 12.33.fcO.23 Angstroms, a distinguishable peak at a d-spacing maximum between 12.57 to about 14.17 Angstroms and a non-discrete peak at a d-spacing maximum between 8.8 to 11. Angstroms, wherein the peak intensity of the d-spacing maximum between 12.57 to about 14.17 Angstroms is less than 90% of the peak intensity of the d-spacing maximum at 12.33±0.23 Angstroms. This disclosure also relates to methods of making the crystalline MCM-22 family molecular sieve composition.
摘要翻译：本公开涉及一种结晶MCM-22族分子筛组合物，其以其合成形式具有包含d间距最大值为12.33fcO.23的峰的X射线衍射图。埃，d处的可区分峰间距最大值在12.57至约14.17埃之间，并且在8.8至11之间的d间距最大值处的非离散峰。其中，在12.57至约14.17埃之间的d间距最大值的峰值强度小于 d间距最大峰值强度为12.33±0.23埃。本公开还涉及制备结晶MCM-22族分子筛组合物的方法。

5. 发明申请

WO2003059508A1 REFORMING CATALYST AND PROCESS 审中-公开
标题翻译：改造催化剂和工艺
公开(公告)号：WO2003059508A1
公开(公告)日：2003-07-24
申请号：PCT/US2003/001246
申请日：2003-01-14
申请人： EXXONMOBIL CHEMICAL PATENTS INC. , CRANE, Robert, A. , JOHNSON, Ivy, D. , KAPOOR, Vinaya, A. , THURTELL, John, H.
发明人： CRANE, Robert, A. , JOHNSON, Ivy, D. , KAPOOR, Vinaya, A. , THURTELL, John, H.
IPC分类号： B01J23/62
CPC分类号： C10G35/09 , B01J21/04 , B01J21/12 , B01J23/40 , B01J23/62 , B01J23/626 , B01J23/6527 , B01J23/8906 , B01J37/24 , C10G35/085
摘要： A platinum-containing aluminum oxide reforming catalyst is disclosed which is modified by incorporating silica therein. The resulting catalyst is used to reform naphtha yielding a reformate having a higher C5 and aromatic content than that achieved using a similar catalyst which contains no added silica.
摘要翻译：公开了一种含铂氧化铝重整催化剂，其通过在其中掺入二氧化硅而被改性。所得催化剂用于重整石脑油，得到具有比使用不含添加二氧化硅的类似催化剂所达到的重量比高的C5和芳族含量的重整产物。

6. 发明申请

WO2007094949A1 PROCESS FOR MANUFACTURING MOLECULAR SIEVE OF MFS FRAMEWORK TYPE AND ITS USE 审中-公开
标题翻译：制造MFS框架类型及其使用分子筛的方法
公开(公告)号：WO2007094949A1
公开(公告)日：2007-08-23
申请号：PCT/US2007/002339
申请日：2007-01-29
申请人： EXXONMOBIL CHEMICAL PATENTS INC. , MERTENS, Machteld, M. , VERBERCKMOES, An , JOHNSON, Ivy, D.
发明人： MERTENS, Machteld, M. , VERBERCKMOES, An , JOHNSON, Ivy, D.
IPC分类号： B01J29/70 , C01B39/48 , C07C2/04
CPC分类号： B01J29/7026 , C01B39/48 , C07C2/12 , C10G49/08 , C10G2400/20 , C10G2400/22 , C07C11/02
摘要： A method of making a crystalline molecular sieve of MFS framework type, said method comprising the steps of (a) adding at least one source of ions of tetravalent element (Y), at least one source of ions of trivalent element (X), at least one hydroxide source (OH>), at least one structure-directing-agent (R), at least one seed source (Seed), and water (H 2 O) to form a mixture having the following mole composition (expressed in term of oxide): YO 2 : (n) X 2 O 3 : (x)OH> : (y)R : (z)H 2 O + (m) Seed wherein the m is in the range of from about 10 wtppm to about 2 wt.% (based on total weight of the synthesis mixture), the n is in the range of from about 0.005 to 0.05, the x is in the range of from about 0.01 to about 0.3, the y is in the range of from about 0.03 to about 2; and the z is in the range of from about 3 to about 30; and (b) treating said mixture under crystallization conditions to form said crystalline molecular sieve substantially free of non-MFS material, wherein said crystallization conditions comprise a temperature in the range of from about 150°C to about 250°C, and crystallization time less than 100 hr, the weight hourly throughput is at least 0.001 hr -1 .
摘要翻译：一种制备MFS框架型结晶分子筛的方法，所述方法包括以下步骤：（a）将至少一种四价元素（Y）的离子的至少一种源，至少一种三价元素（X）的离子源加入至少一种氢氧化物源（OH>），至少一种结构导向剂（R），至少一种种子源（Seed）和水（H 2 O））以形成具有以下摩尔组成（以氧化物表示）：YO 2：（n）X 2 O 3：（x）OH>：（x） y）R：（z）H 2 O +（m）其中m为约10重量ppm至约2重量％（基于合成混合物的总重量）的种子，，n在约0.005至0.05的范围内，x在约0.01至约0.3的范围内，y在约0.03至约2的范围内; 并且z在约3至约30的范围内; 和（b）在结晶条件下处理所述混合物以形成基本上不含非MFS材料的所述结晶分子筛，其中所述结晶条件包括在约150℃至约250℃范围内的温度和更少的结晶时间超过100小时，重量小时产量至少为0.001小时-1。

7. 发明申请

WO2013048636A1 IMPROVED MCM-56 MANUFACTURE 审中-公开
标题翻译：改进的MCM-56制造
公开(公告)号：WO2013048636A1
公开(公告)日：2013-04-04
申请号：PCT/US2012/051181
申请日：2012-08-16
申请人： EXXONMOBIL CHEMICAL PATENTS INC. , JOHNSON, Ivy, D. , HRYCENKO, Nadya, A. , ROTH, Wieslaw, J. , HELTON, Terry, E.
发明人： JOHNSON, Ivy, D. , HRYCENKO, Nadya, A. , ROTH, Wieslaw, J. , HELTON, Terry, E.
IPC分类号： C01B39/48
CPC分类号： C01B39/48 , B01J29/70 , B01J29/74 , B01J29/76 , B01J29/78 , B01J2229/186 , B01J2229/42 , C07C2/66 , C07C2529/70 , Y02P20/52 , C07C15/073 , C07C15/085
摘要： The present invention provides an improved method for manufacturing high quality porous crystalline MCM-56 material. It also relates to the MCM-56 material manufactured by the improved method, catalyst compositions comprising same and use thereof in a process for catalytic conversion of hydrocarbon compounds. One such conversion process involves production of monoalkylated aromatic compounds, particularly ethylbenzene and cumene, by the liquid or partial liquid phase alkylation of alkylatable aromatic compound, particularly benzene.
摘要翻译：本发明提供了制造高品质多孔结晶MCM-56材料的改进方法。它还涉及通过改进方法制造的MCM-56材料，包含其的催化剂组合物以及在烃化合物的催化转化方法中的用途。一种这样的转化方法包括通过液体或部分液相烷基化的可烷基化芳族化合物，特别是苯来生产单烷基化芳族化合物，特别是乙苯和枯烯。

8. 发明申请

WO2022098453A1 PRODUCTION OF ALKYLAROMATIC COMPOUNDS 审中-公开
公开(公告)号：WO2022098453A1
公开(公告)日：2022-05-12
申请号：PCT/US2021/052895
申请日：2021-09-30
申请人： EXXONMOBIL CHEMICAL PATENTS INC.
发明人： PETERS, Aaron, W. , BRITTO, Reuben, J. , KNAEBLE, William, J. , JOHNSON, Ivy, D. , OLIVERI, Christopher, G.
IPC分类号： C07C6/12 , C07C15/085
摘要： A process for producing a mono-alkylated benzene comprises contacting benzene with di-alkylated benzene(s) and/or tri-alkylated benzene(s) in the presence of a transalkylation catalyst composition under transalkylation conditions to convert at least part of the di-alkylated benzene(s) and tri-alkylated benzene(s) to mono-alkylated benzene. The transalkylation catalyst composition comprises a treated zeolitic material having increased mesoporous surface area compared to the precursor catalyst composition from which it is made.

9. 发明申请

WO2020205354A1 MEL-TYPE ZEOLITE FOR CONVERTING AROMATIC HYDROCARBONS, PROCESS FOR MAKING AND CATALYTIC COMPOSITION COMPRISING SAID ZEOLITE 审中-公开
公开(公告)号：WO2020205354A1
公开(公告)日：2020-10-08
申请号：PCT/US2020/024616
申请日：2020-03-25
申请人： EXXONMOBIL CHEMICAL PATENTS INC.
发明人： LAI, Wenyih, F. , PODSIADLO, Paul , METZGER, Eric, D. , JOHNSON, Ivy, D. , KHEIR, Ali, A. , ZURLO, Dominick, A. , KEVILLE, Kathleen, M.
IPC分类号： B01J29/40 , C01B39/36 , B01J35/02 , B01J35/10 , C07C5/27 , B01J35/00 , B01J29/80 , C07C6/12 , C01B39/40
摘要： Novel MEL framework type zeolites can be made to have small crystallite sizes and desirable silica/SiCb molar ratios. Catalyst compositions comprising such MEL framework type zeolites can be particularly advantageous in isomerization C8 aromatic mixtures. An isomerization process for converting C8 aromatic hydrocarbons can advantageously utilize a catalyst composition comprising a MEL framework type zeolite.

10. 发明申请

WO2018160327A1 CATALYST COMPOSITIONS AND THEIR USE IN AROMATIC ALKYLATION PROCESSES 审中-公开
公开(公告)号：WO2018160327A1
公开(公告)日：2018-09-07
申请号：PCT/US2018/017245
申请日：2018-02-07
申请人： EXXONMOBIL CHEMICAL PATENTS INC.
发明人： IDE, Matthew, S. , LEVIN, Doron , LAI, Wenyih, F. , JOHNSON, Ivy, D. , WEIGEL, Scott, J. , LOVELESS, Brett, T.
IPC分类号： B01J29/18 , B01J29/70 , C07C2/66 , B01J35/10 , B01J20/18 , B01J35/00 , B01J29/80 , C07C6/12 , C07C15/085 , B01J29/06 , B01J29/08
CPC分类号： B01J29/18 , B01J20/18 , B01J20/28004 , B01J20/28057 , B01J20/3007 , B01J20/3078 , B01J29/7007 , B01J29/80 , B01J35/0006 , B01J35/002 , B01J35/1023 , B01J35/1061 , B01J2220/42 , B01J2229/186 , B01J2229/20 , B01J2229/36 , B01J2229/42 , C07C2/66 , C07C7/13 , C07C2529/18 , C07C2529/70 , C07C2529/80 , Y02P20/52 , C07C15/02 , C07C15/085 , C07C11/02
摘要： Catalyst composition which comprises a first zeolite having a BEA* framework type and a second zeolite having a MOR framework type and a mesopore surface area of greater than 30 m 2 /g is disclosed. These catalyst compositions are used to remove catalyst poisons from untreated feed streams having one or more impurities which cause deactivation of the downstream catalysts employed in hydrocarbon conversion processes, such as those that produce mono-alkylated aromatic compounds.

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