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1. 发明申请

WO2006028817A3 OPTIMIZED LIQUID-PHASE OXIDATION 审中-公开
公开(公告)号：WO2006028817A3
公开(公告)日：2006-03-16
申请号：PCT/US2005/030856
申请日：2005-08-29
申请人： EASTMAN CHEMICAL COMPANY
发明人： DE VREEDE, Marcel , PARTIN, Lee, Reynolds , STRASSER, Wayne, Scott , WONDERS, Alan, George
IPC分类号： C07C51/21 , C07C51/235
摘要： Disclosed is an optimized process for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

2. 发明申请

WO2006028755A1 OPTIMIZED LIQUID-PHASE OXIDATION 审中-公开
标题翻译：优化液相氧化
公开(公告)号：WO2006028755A1
公开(公告)日：2006-03-16
申请号：PCT/US2005/030549
申请日：2005-08-29
申请人： EASTMAN CHEMICAL COMPANY
发明人： WONDERS, Alan George , PARTIN, Lee, Reynolds , STRASSER, Wayne Scott , DE VREEDE, Marcel
IPC分类号： C07B33/00
CPC分类号： C07C51/235 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthali c acid (CTA), such CTA product can be purified and separated by more economic altechniques than could be employed if the CTA were formed by a conventional high- temperature oxidation process.
摘要翻译：公开了一种用于更有效和经济地进行可氧化化合物的液相氧化的优化方法。这种液相氧化在气泡塔反应器中进行，其在相对低的温度下提供高效反应。当氧化的化合物是对二甲苯并且来自氧化反应的产物是粗对苯二甲酸（CTA）时，如果CTA由常规的高分子化合物形成，则可以通过更经济的技术来纯化和分离这种CTA产物，温度氧化过程。

3. 发明申请

WO2018017382A1 A FURAN-2,5-DICARBOXYLIC ACID PURGE PROCESS 审中-公开
标题翻译：呋喃-2,5-二羧酸酸洗过程
公开(公告)号：WO2018017382A1
公开(公告)日：2018-01-25
申请号：PCT/US2017/041842
申请日：2017-07-13
申请人： EASTMAN CHEMICAL COMPANY
发明人： FONTENOT, Kevin, John , JANKA, Mesfin, Ejerssa , PARKER, Kenny, Randolph , SHAIKH, Ashfaq, Shahanawaz , PARTIN, Lee, Reynolds , SUMMER, Charles, Edwan, Jr. , KIRK, Shane, Kipley , MOODY, Paula , BOWERS, Bradford, Russell , MORROW, Michael, Charles
IPC分类号： C07D307/68 , B01J10/00 , B01J23/889
摘要： Disclosed is an oxidation process to produce a crude carboxylic acid product carboxylic acid product. The process comprises oxidizing a feed stream comprising at least one oxidizable compound to generate a crude carboxylic acid slurry comprising furan-2,5-dicarboxylic acid (FDCA) and compositions thereof. Also disclosed is a process to produce a dry purified carboxylic acid product by utilizing various purification methods on the crude carboxylic acid.
摘要翻译：公开了生产粗羧酸产物羧酸产物的氧化方法。该方法包括氧化包含至少一种可氧化化合物的进料流以产生包含呋喃-2,5-二甲酸（FDCA）及其组合物的粗制羧酸浆液。还公开了通过对粗制羧酸使用各种纯化方法来生产干燥纯化的羧酸产物的方法。

4. 发明申请

WO2014014979A1 AN OXIDATION PROCESS TO PRODUCE A PURIFIED CARBOXYLIC ACID PRODUCT VIA SOLVENT DISPLACEMENT AND POST OXIDATION 审中-公开
标题翻译：通过溶剂置换和氧化后制备纯化羧酸产物的氧化方法
公开(公告)号：WO2014014979A1
公开(公告)日：2014-01-23
申请号：PCT/US2013/050794
申请日：2013-07-17
申请人： EASTMAN CHEMICAL COMPANY
发明人： JANKA, Mesfin, Ejerssa , PARKER, Kenny, Randolph , MOODY, Paula , SHAIKH, Ashfaq, Shahanawaz , PARTIN, Lee, Reynolds , BOWERS, Bradford, Russell , MORROW, Michael, Charles
IPC分类号： C07D307/46 , C07D307/48 , C07D307/40
CPC分类号： C07D307/68
摘要： Disclosed is a process to produce a dry purified carboxylic acid product comprising furan-2,5-dicarboxylic acid (FDCA). The process comprises oxidizing at least one oxidizable compound selected from the following group: 5-(hydroxymethyl)furfural (5-HMF), 5-HMF esters (5-R(CO)OCH 2 -furfural where R = alkyl, cycloalkyl and aryl), 5-HMF ethers (5-R'OCH 2 -furfural, where R' = alkyl, cycloalkyl and aryl), 5-alkyl furfurals (5-R"-furfural, where R" = alkyl, cycloalkyl and aryl), mixed feed-stocks of 5-HMF and 5-HMF esters and mixed feed-stocks of 5-HMF and 5-HMF ethers and mixed feed-stocks of 5- HMF and 5-alkyl furfurals to generate a crude carboxylic acid slurry comprising FDCA, removing impurities from a crude carboxylic acid slurry in a liquid displacement zone to form a low impurity slurry stream. The low impurity slurry stream is further treated in a secondary oxidation zone to produce a secondary oxidation slurry stream which is routed to a crystallization zone to form a crystallized slurry stream. The crystallized slurry stream is cooled in a cooling zone and the resulting cooled crystallized slurry stream is routed to a solid-liquid separation zone to generate a purified wet cake stream comprising FDCA that is dried in a drying zone to generate a dry carboxylic acid product stream comprising purified FDCA (pFDCA).
摘要翻译：公开了生产包含呋喃-2,5-二羧酸（FDCA）的干燥纯化的羧酸产物的方法。该方法包括氧化至少一种选自如下组的可氧化的化合物：5-（羟甲基）糠醛（5-HMF），5-HMF酯（5-R（CO）OCH 2 2 - 糠醛其中 R 5 =烷基，环烷基和芳基），5-HMF醚（5-R'OCH 2 - 糠醛，其中R'=烷基，环烷基和芳基），5-烷基糠醛（5-R“ 其中R“=烷基，环烷基和芳基），5-HMF和5-HMF酯的混合原料以及5-HMF和5-HMF醚的混合原料和5-HMF的混合原料和5-烷基糠醛以产生包含FDCA的粗制羧酸浆液，从液体置换区中的粗制羧酸浆液中除去杂质以形成低杂质浆液流。低杂质浆料流在第二氧化区进一步处理以产生第二氧化浆料流，将其送至结晶区以形成结晶浆料流。将结晶的浆料物流在冷却区中冷却，并将得到的冷却的结晶的浆料物流输送至固液分离区以产生包含FDCA的经纯化的湿饼物流，其在干燥区中干燥以产生干燥的羧酸产物物流包含纯化的FDCA（pFDCA）。

5. 发明申请

WO2013191940A1 METHOD FOR PRODUCING PURIFIED DIALKYL-FURAN-2,5-DICARBOXYLATE VAPOR 审中-公开
标题翻译：纯化的二烷基 - 呋喃-2,5-二羧酸盐蒸气的生产方法
公开(公告)号：WO2013191940A1
公开(公告)日：2013-12-27
申请号：PCT/US2013/044922
申请日：2013-06-10
申请人： EASTMAN CHEMICAL COMPANY
发明人： PARTIN, Lee, Reynolds , SHAIKH, Ashfaq, Shahanawaz , JANKA, Mesfin, Ejerssa , PARKER, Kenny, Randolph
IPC分类号： C07D307/68
CPC分类号： C07D307/68
摘要： Disclosed is a process to produce a purified vapor comprising dialkyl- furan-2,5-dicarboxylate (DAFD). Furan-2,5-dicarboxylic acid (FDCA) and an alcohol in an esterification zone to generate a crude diester stream containing dialkyl furan dicarboxylate (DAFD), unreacted alcohol, 5- (alkoxycarbonyl)furan-2-carboxylic acid (ACFC), and alkyl furan-2-carboxylate (AFC). The crude diester stream is fed to a flash evaporation zone to produce a vapor alcohol composition and a first liquid DAFD rich composition. At least a portion of the remaining alcohol can be separated from the first liquid DAFD rich composition to produce a second alcohol vapor and a second liquid DAFD rich composition, followed by separating AFC from the second liquid DAFD rich composition to product an AFC vapor and a partially purified DAFD rich composition, followed by separating a portion of the DAFD from the partially purified DAFD rich composition to produce a purified DAFD vapor.
摘要翻译：公开了一种生产包含二烷基 - 呋喃-2,5-二羧酸二烷基酯（DAFD）的纯化蒸气的方法。呋喃-2,5-二羧酸（FDCA）和醇在酯化区中产生含有呋喃二羧酸二烷基酯（DAFD），未反应的醇，5-（烷氧基羰基）呋喃-2-羧酸（ACFC）的粗二酯流，和呋喃-2-羧酸烷基酯（AFC）。将粗二酯流进料到闪蒸区域以产生蒸气醇组合物和富含第一液体DAFD的组合物。剩余的醇的至少一部分可以与富含第一液体DAFD的组合物分离，以产生第二醇蒸气和富含第二液态DAFD的组合物，然后将AFC与第二种富含液体DAFD的组合物分离，以产生AFC蒸气和部分纯化的富含DAFD的组合物，然后从部分纯化的富含DAFD的组合物中分离一部分DAFD以产生纯化的DAFD蒸气。

6. 发明申请

WO2006028767A1 OPTIMIZED LIQUID-PHASE OXIDATION IN A BUBBLE COLUMN REACTOR 审中-公开
标题翻译：泡沫柱反应器中优化的液相氧化
公开(公告)号：WO2006028767A1
公开(公告)日：2006-03-16
申请号：PCT/US2005/030650
申请日：2005-08-29
申请人： EASTMAN CHEMICAL COMPANY
发明人： WONDERS, Alan, George , JENKINS, Howard Wood, Jr. , PARTIN, Lee, Reynolds , STRASSER, Wayne, Scott , DE VREEDE, Marcel
IPC分类号： B01J19/24 , B01J10/00 , B01F3/04 , C07C51/235
CPC分类号： B01J4/002 , B01F3/04262 , B01F3/04496 , B01F2003/04361 , B01J8/008 , B01J8/1818 , B01J8/22 , B01J8/228 , B01J2208/003 , B01J2208/00539 , B01J2208/0061 , B01J2219/0004 , C07C51/235 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.
摘要翻译：公开了一种用于更有效和经济地进行可氧化化合物的液相氧化的优化方法和装置。这种液相氧化在气泡塔反应器中进行，其在相对低的温度下提供高效反应。当氧化的化合物是对二甲苯并且来自氧化反应的产物是粗对苯二甲酸（CTA）时，可以通过更经济的技术将这种CTA产物纯化和分离，如果CTA通过常规的高温氧化过程。

7. 发明申请

WO2006028752A2 OPTIMIZED LIQUID-PHASE OXIDATION 审中-公开
公开(公告)号：WO2006028752A2
公开(公告)日：2006-03-16
申请号：PCT/US2005/030546
申请日：2005-08-29
申请人： EASTMAN CHEMICAL COMPANY
发明人： WONDERS, Alan, George , LIN, Robert , DE VREEDE, Marcel , PARTIN, Lee, Reynolds , STRASSER, Wayne, Scott
IPC分类号： C07B33/00 , C07C51/21 , C07C51/235
CPC分类号： B01J8/1872 , B01J8/1836 , B01J8/22 , B01J19/006 , B01J2208/0015 , C07C51/21 , C07C51/235 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

8. 发明申请

WO2018017382A8 A FURAN-2,5-DICARBOXYLIC ACID PURGE PROCESS 审中-公开
标题翻译：呋喃-2,5-二羧酸酸洗过程
公开(公告)号：WO2018017382A8
公开(公告)日：2018-01-25
申请号：PCT/US2017/041842
申请日：2017-07-13
申请人： EASTMAN CHEMICAL COMPANY
发明人： FONTENOT, Kevin, John , JANKA, Mesfin, Ejerssa , PARKER, Kenny, Randolph , SHAIKH, Ashfaq, Shahanawaz , PARTIN, Lee, Reynolds , SUMNER, Charles, Edwan, Jr. , KIRK, Shane, Kipley , MOODY, Paula , BOWERS, Bradford, Russell , MORROW, Michael, Charles
IPC分类号： C07D307/68 , B01J10/00 , B01J23/889
摘要： Disclosed is an oxidation process to produce a crude carboxylic acid product. The process comprises oxidizing a feed stream comprising at least one oxidizable compound to generate a crude carboxylic acid slurry comprising furan-2,5-dicarboxylic acid (FDCA) and compositions thereof. Also disclosed is a process to produce a dry purified carboxylic acid product by utilizing various purification methods on the crude carboxylic acid.
摘要翻译：公开了生产粗羧酸产物的氧化方法。该方法包括氧化包含至少一种可氧化化合物的进料流以产生包含呋喃-2,5-二甲酸（FDCA）及其组合物的粗制羧酸浆液。还公开了通过对粗制羧酸使用各种纯化方法来生产干燥纯化的羧酸产物的方法。

9. 发明申请

WO2014035813A1 AN OXIDATION PROCESS TO PRODUCE A CRUDE DRY CARBOXYLIC ACID PRODUCT 审中-公开
标题翻译：一种生产羧酸羧酸产品的氧化方法
公开(公告)号：WO2014035813A1
公开(公告)日：2014-03-06
申请号：PCT/US2013/056362
申请日：2013-08-23
申请人： EASTMAN CHEMICAL COMPANY
发明人： JANKA, Mesfin, Ejerssa , SHAIKH, Ashfaq, Shahanawaz , PARKER, Kenny, Randolph , PARTIN, Lee, Reynolds
IPC分类号： C07D307/48 , C07D307/46
CPC分类号： C07D307/68 , C07D307/48
摘要： Disclosed is a process to produce a dry purified carboxylic acid product comprising furan-2,5-dicarboxylic acid (FDCA). The process comprises oxidizing at least one oxidizable compound selected from the following group: 5-(hydroxymethyl)furfural (5-HMF), 5-HMF esters (5-R(CO)OCH 2 -furfural where R = alkyl, cycloalkyl and aryl), 5-HMF ethers (5-R'OCH 2 -furfural, where R' = alkyl, cycloalkyl and aryl), 5-alkyl furfurals (5-R"-furfural, where R" = alkyl, cycloalkyl and aryl), mixed feed-stocks of 5-HMF and 5-HMF esters and mixed feed-stocks of 5-HMF and 5-HMF ethers and mixed feed-stocks of 5-HMF and 5-alkyl furfurals to generate a crude carboxylic acid slurry comprising FDCA, cooling a crude carboxylic acid slurry in cooling zone to form a cooled slurry stream. The cooled slurry stream is routed to a solid-liquid separation zone to generate a crude wet cake stream comprising FDCA that is dried in a drying zone to generate a dry carboxylic acid product stream comprising crude FDCA (cFDCA).
摘要翻译：公开了一种生产包含呋喃-2,5-二羧酸（FDCA）的干燥纯化羧酸产物的方法。该方法包括氧化至少一种选自以下组的可氧化化合物：5-（羟甲基）糠醛（5-HMF），5-HMF酯（5-R（CO）OCH 2 - 糠醛，其中R =烷基，环烷基和芳基），5-HMF醚（5-R'OCH 2 - 糠醛，其中R'=烷基，环烷基和芳基），5-烷基糠醛（5-R“ - 糠醛，其中R”=烷基，环烷基和芳基），混合进料 5-HMF和5-HMF酯的原料和5-HMF和5-HMF醚的混合原料和5-HMF和5-烷基糠醛的混合原料以产生包含FDCA的粗制羧酸浆料，冷却在冷却区中的粗羧酸浆料以形成冷却的浆料流。将冷却的浆料流送至固液分离区，以产生包含FDCA的粗湿饼流，其在干燥区中干燥以产生包含粗FDCA（cFDCA）的干燥羧酸产物流。

10. 发明申请

WO2013191938A1 ESTERIFICATION OF FURAN-2,5-DICARBOXYLIC ACID TO A DIALKYL-FURAN-2,5-DICARBOXYLATE VAPOR WITH RECTIFICATION 审中-公开
标题翻译：将FURAN-2,5-DICARBOXY酸酸化到具有重整的二烷基 - 呋喃-2,5-二氯乙酸盐蒸气
公开(公告)号：WO2013191938A1
公开(公告)日：2013-12-27
申请号：PCT/US2013/044919
申请日：2013-06-10
申请人： EASTMAN CHEMICAL COMPANY
发明人： PARTIN, Lee, Reynolds , SHAIKH, Ashfaq, Shahanawaz , JANKA, Mesfin, Ejerssa , PARKER, Kenny, Randolph
IPC分类号： C07D307/68
CPC分类号： C07D307/68
摘要： A process for the manufacture of dialkyl furan-2,5-dicarboxylate (DAFD) vapor composition by feeding furan-2,5-dicarboxylic acid ("FDCA") to an esterification reactor and in the presence of an alcohol compound such as methanol, conducting an esterification reaction to form an esterification vapor containing DAFD, unreacted alcohol compound, 5-(alkoxycarbonyl)furan-2-carboxylic acid (ACFC), and water, and continuously passing the esterification vapor through an ACFC condensing zone, that can be integral with the esterification reactor, in which at least a portion of the ACFC in the esterification vapor is converted to a liquid phase condensate, and continuously discharging the esterification vapor from the ACFC condensing zone as a DAFD vapor. There is also a DAFD vapor composition containing DAFD, water, unreacted alcohol, and by-products.
摘要翻译：通过将呋喃-2,5-二羧酸（“FDCA”）加入到酯化反应器中并在醇化合物如甲醇存在下制备呋喃-2,5-二羧酸二烷基酯（DAFD）蒸气组合物的方法，进行酯化反应以形成含有DAFD，未反应的醇化合物，5-（烷氧基羰基）呋喃-2-羧酸（ACFC）和水的酯化蒸气，并连续使酯化蒸气通过ACFC冷凝区，其可以是积分的酯化反应器中，将酯化蒸气中的至少一部分ACFC转化为液相冷凝物，并且将来自ACFC冷凝区的酯化蒸气作为DAFD蒸气连续排出。还有一种含有DAFD，水，未反应的醇和副产物的DAFD蒸汽组合物。

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