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1. 发明申请

WO2013101999A1 PROCESS FOR THE PRODUCTION OF FURFURAL 审中-公开
标题翻译：生产过程的过程
公开(公告)号：WO2013101999A1
公开(公告)日：2013-07-04
申请号：PCT/US2012/071936
申请日：2012-12-28
申请人： E. I. DU PONT DE NEMOURS AND COMPANY
发明人： FAGAN, Paul Joseph , OZER, Ronnie , TILL, Eric J.
IPC分类号： C07D307/48 , B01J27/053 , B01J29/82
CPC分类号： C07D307/50
摘要： Furfural is produced by mixing an aqueous feedstock solution containing C 5 sugar and/or C 6 sugar with a heated, high boiling, water-miscible solvent, such as sulfolane, and a soluble acid catalyst. Furfural product and water are distilled off through a multistage distillation column, leaving non-volatile solvent behind. Typical furfural yields with sulfolane as the reaction solvent are about 80% at as high as 99% conversion. Also, certain by-products (e.g., humins) solubilized in the reaction solvent can be precipitated by addition of water or aqueous feedstock solution and then removed by filtration, thereby providing a convenient and effective way of removing these undesirable byproducts from the reaction mixture.
摘要翻译：糠醛通过将含有C5糖和/或C6糖的原料水溶液与加热的，沸点高的水混溶性溶剂如环丁砜和可溶性酸催化剂混合而制备。通过多级蒸馏塔蒸馏出糠醛产物和水，留下非挥发性溶剂。以环丁砜作为反应溶剂的典型糠醛产率为高达99％转化率的约80％。此外，溶解在反应溶剂中的某些副产物（例如，胡氏体）可以通过加入水或原料溶液沉淀，然后通过过滤除去，从而提供从反应混合物中除去这些不期望的副产物的方便有效的方法。

2. 发明申请

WO2017210525A1 PROCESS FOR THE PRODUCTION OF FURFURAL USING A WATER-IMMISCIBLE ORGANIC SOLVENT 审中-公开
标题翻译：使用水不溶性有机溶剂生产糠醛的方法
公开(公告)号：WO2017210525A1
公开(公告)日：2017-12-07
申请号：PCT/US2017/035626
申请日：2017-06-02
申请人： E. I. DU PONT DE NEMOURS AND COMPANY
发明人： CARLSON, Torren Ryan , DICKINSON, Jacob G. , DREW, David William , FAGAN, Paul Joseph , GALLAGHER, Francis G. , HUTCHENSON, Keith W. , LIBERIS, Isabel , MERSMAN, Kenneth , SUNSHINE, Gregg
IPC分类号： C07D307/48
摘要： The disclosure relates to a process for the production of a furan derivative from C 5 and/or C 6 sugars. The process utilizes a water-immiscible organic solvent system comprising at least one alkyl phenol and at least one alkylated naphthalene.
摘要翻译：本公开涉及从C 5和/或C 6糖生产呋喃衍生物的方法。该方法使用包含至少一种烷基酚和至少一种烷基化萘的与水不混溶的有机溶剂体系。

3. 发明申请

WO2015077573A1 HIGH FORCE AND HIGH STRESS DESTRUCTURING OF CELLULOSIC BIOMASS 审中-公开
标题翻译：细胞生物质的高强度和高应力分解
公开(公告)号：WO2015077573A1
公开(公告)日：2015-05-28
申请号：PCT/US2014/066835
申请日：2014-11-21
申请人： E. I. DU PONT DE NEMOURS AND COMPANY
发明人： DE SILVA, Wathudura Indika Namal , FAGAN, Paul Joseph , GALLAGHER, F. Glenn , HUANG, Zheng-Zheng , LIU, Guangliang Gary , PERELMAN, Aaron , MILLAN, Luis Fernando Romero , SHPILSKY, Anton , SLANAC, Daniel A. , WALSH, Maria
IPC分类号： C08H8/00 , A23K1/12 , C12P19/02
CPC分类号： C12P19/14 , A23K10/30 , A23K20/189 , A61K31/717 , A61K38/47 , C08B30/02 , C08B30/12 , C08H8/00 , C12P7/10 , C12P7/14 , C12P19/02 , C12P19/20 , C12P2201/00 , C12Y302/01004 , C13K1/02 , C13K13/002 , Y02E50/16 , Y02P60/877
摘要： A process for mechanical destructuring of cellulosic biomass was developed that makes use of a short application of high compression, impact, and shearing forces. The biomass may be destructured using a specific energy input that is less than 40% of the total combustible energy of the biomass. The destructured biomass, with or without saccharification and/or in-feed glycosyl hydrolase enzymes, may be used in feed applications.
摘要翻译：开发了纤维素生物质的机械结构化过程，其利用了高压缩，冲击和剪切力的短期应用。生物质可以使用小于生物质的总可燃能量的40％的比能量输入来解构。具有或不具有糖化和/或进食糖基水解酶的破坏生物质可用于饲料应用中。

4. 发明申请

WO2013102027A1 PROCESS FOR THE PRODUCTION OF FURFURAL 审中-公开
标题翻译：生产过程的过程
公开(公告)号：WO2013102027A1
公开(公告)日：2013-07-04
申请号：PCT/US2012/071992
申请日：2012-12-28
申请人： E. I. DU PONT DE NEMOURS AND COMPANY
发明人： CORBIN, David Richard , FAGAN, Paul Joseph , OZER, Ronnie , RAJAGOPALAN, Bhuma , TILL, Eric J.
IPC分类号： C07D307/48 , B01J29/04 , B01J27/053
CPC分类号： C07D307/50
摘要： Furfural is produced by mixing an aqueous feedstock solution containing C 5 sugar and/or C 6 sugar with a heated high boiling, water-miscible solvent, such as sulfolane, and a solid acid catalyst. Furfural product and water can be distilled off, leaving non-volatile solvent behind. Furfural yields of over 70% at as high as 99% conversion have been obtained with this process with sulfolane as the reaction solvent and zeolite beta as the solid acid catalyst. Also, certain by-products (e.g., humins) solubilized in the reaction solvent can be precipitated by addition of water or aqueous feedstock solution and then removed by filtration, thereby providing a convenient and effective way of removing these undesirable byproducts from the reaction mixture.
摘要翻译：通过将含有C5糖和/或C6糖的水性原料溶液与加热的高沸点，水混溶性溶剂如环丁砜和固体酸催化剂混合来制备糠醛。糠醛产品和水可以蒸馏出来，留下非挥发性溶剂。用环丁砜作为反应溶剂和沸石β作为固体酸催化剂，该方法已经获得高达99％转化率的糠醛产率超过70％。此外，溶解在反应溶剂中的某些副产物（例如，胡氏体）可以通过加入水或原料溶液沉淀，然后通过过滤除去，从而提供从反应混合物中除去这些不期望的副产物的方便有效的方法。

5. 发明申请

WO2013102015A1 PROCESS FOR THE PRODUCTION OF FURFURAL 审中-公开
标题翻译：生产过程的过程
公开(公告)号：WO2013102015A1
公开(公告)日：2013-07-04
申请号：PCT/US2012/071964
申请日：2012-12-28
申请人： E. I. DU PONT DE NEMOURS AND COMPANY
发明人： CORBIN, David Richard , FAGAN, Paul Joseph , FERGUSSON, Stuart B. , HUTCHENSON, Keith W. , MCKINNON, Michael Stephen , OZER, Ronnie , RAJAGOPALAN, Bhuma , SENGUPTA, Sourav Kumar , TILL, Eric J.
IPC分类号： C07D307/38 , B01J29/06 , B01J27/053
CPC分类号： C07D307/50 , C07D307/48 , Y02P20/127
摘要： Furfural is produced by contacting a feedstock solution containing C5 sugar and/or C6 sugar with a solid acid catalyst using reactive distillation. Both high yield and high conversion are obtained, without production of insoluble char in the reaction vessel. Degradation of furfural is minimized by its low residence time in contact with the solid acid catalyst. Higher catalyst lifetime can be achieved because the catalyst is continually washed with the refluxing aqueous solution and not sitting in high-boiling byproducts like humins, which are known to be deleterious to catalyst lifetime.
摘要翻译：通过使用反应蒸馏将含有C5糖和/或C6糖的原料溶液与固体酸催化剂接触来制备糠醛。获得高产率和高转化率，而在反应容器中不产生不溶性焦炭。通过其与固体酸催化剂接触的低停留时间来使糠醛的降解最小化。可以实现更高的催化剂寿命，因为催化剂连续地用回流水溶液洗涤，而不是位于已知对催化剂寿命有害的高沸点副产物如胡氏。

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