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1. 发明申请

WO2020084082A1 AQUEOUS COMPOSITIONS COMPRISING OMEGA NITROOXY-1-ALKANOLS 审中-公开
公开(公告)号：WO2020084082A1
公开(公告)日：2020-04-30
申请号：PCT/EP2019/079093
申请日：2019-10-24
申请人： DSM IP ASSETS B.V.
发明人： BAATI, Nadia , RIEBEL, Peter , WILDERMANN, Angela
IPC分类号： A23K20/10 , A23K50/10
摘要： The invention relates to safe aqueous compositions of ω-nitrooxy-C3-10alkane-1-ols.

2. 发明申请

WO2014097172A1 NITROGEN MONOXIDE AS CIS/TRANS ISOMERIZATION CATALYSTS FOR UNSATURATED COMPOUNDS 审中-公开
标题翻译：不饱和化合物的硝基一氧化碳/转异构化催化剂
公开(公告)号：WO2014097172A1
公开(公告)日：2014-06-26
申请号：PCT/IB2013/061083
申请日：2013-12-18
申请人： DSM IP ASSETS B.V.
发明人： STEMMLER, René, Tobias , GREINER, Nadine , WILDERMANN, Angela
IPC分类号： C07C29/56 , C07C45/67 , C07C43/313 , C07C33/02 , C07C49/203 , C07D319/06 , C07C29/80 , C07C45/82
CPC分类号： C07C43/313 , C07B2200/09 , C07C29/56 , C07C33/02 , C07C45/67 , C07C49/203
摘要： The present invention relates to a process of a cis/trans isomerization of an unsaturated compound A being selected from the group consisting of unsaturated ketones, unsaturated ketals, unsaturated aldehydes, unsaturated acetals, unsaturated carboxylic acids, esters of an unsaturated carboxylic acid and amides of an unsaturated carboxylic acid using nitrogen monoxide as cis/trans isomerization catalyst. It has been observed that the isomerization is very efficient and fast.
摘要翻译：本发明涉及不饱和化合物A的顺式/反式异构化方法，其选自不饱和酮，不饱和缩酮，不饱和醛，不饱和缩醛，不饱和羧酸，不饱和羧酸的酯和酰胺的酰胺使用一氧化氮作为顺式/反式异构化催化剂的不饱和羧酸。已经观察到异构化非常有效和快速。

3. 发明申请

WO2006018310A2 PROCESS FOR THE WORKING-UP OF A VITAMIN E- AND VITAMIN E-ACETATE-CONTAINING MIXTURE OR PRODUCT STREAM 审中-公开
标题翻译：维生素E和维生素E含乙酸酯混合物或产品流程的工作过程
公开(公告)号：WO2006018310A2
公开(公告)日：2006-02-23
申请号：PCT/EP2005/008982
申请日：2005-08-19
申请人： DSM IP ASSETS B.V. , PIETZONKA, Werner , RUCKSTUHL, Peter , WILDERMANN, Angela
发明人： PIETZONKA, Werner , RUCKSTUHL, Peter , WILDERMANN, Angela
IPC分类号： C07D311/72 , B01D3/14 , F25J3/02
CPC分类号： C07D311/72
摘要： The invention relates to a process for the working-up of a vitamin E (VE)- and/or vitamin E acetate (VEA)-containing product stream, which is substantially characterized by purification of a vitamin E-containing product stream, acetylation of at least a part of the purified vitamin E and purification of at least a part of the acetylated vitamin E, the purification of vitamin E and vitamin E acetate preferably being effected by distillation, for example rectification. A preferred process according to the invention is characterized in that a vitamin E-containing product stream is fed to a first rectification column (105), low-boiling products and unspecified isomers of vitamin E being taken off at the top (105a) of this first rectification column virtually without loss of useful substance, and a purified, vitamin E-containing stream being taken off at the side (105b) and/or at the bottom (105c) of the rectification column (105), at least a part of the side take-off or of the bottom take-off or at least a part of the side and bottom take-off is passed, for acetylation of vitamin E, into an acetylation stage (111), at least a part of the product stream emerging from the acetylation stage is passed into a second rectification column (115) or is taken off as useful product having a purity of ≥ 92 % by weight, and in a second rectification column, the VEA useful product is obtained as a side take-off having a purity of ≥ 97 % by weight.
摘要翻译：本发明涉及一种用于处理含维生素E（VE）和/或维生素E乙酸酯（VEA）的产品流）的方法，其基本特征在于纯化含维生素E的产物流，乙酰化纯化的维生素E的至少一部分和至少一部分乙酰化维生素E的纯化，维生素E和维生素E乙酸酯的纯化优选通过蒸馏进行，例如精馏。根据本发明的优选方法的特征在于将含维生素E的产物流加入到第一精馏塔（105）中，低沸点产物和维生素E的未指定异构体在该顶部（105a）处脱除第一精馏塔实际上不损失有用物质，并且在精馏塔（105）的一侧（105b）和/或底部（105c）处取出纯化的含维生素E的物流，至少一部分侧面起飞或底部起飞或至少部分侧面和底部起飞通过维生素E的乙酰化进入乙酰化阶段（111），至少部分产物流从乙酰化阶段出来的化合物进入第二精馏塔（115）或作为纯度为= 92重量％的有用产物脱去，在第二精馏塔中，获得VEA有用产物作为侧取纯度为97重量％。

4. 发明申请

WO2021214144A1 PROCESS FOR THE PREPARATION OF ALPHA,OMEGA-ALKANEDIOL MONONITRATE 审中-公开
公开(公告)号：WO2021214144A1
公开(公告)日：2021-10-28
申请号：PCT/EP2021/060405
申请日：2021-04-21
申请人： DSM IP ASSETS B.V.
发明人： RIEBEL, Peter Hans , WILDERMANN, Angela
IPC分类号： C07C201/02 , C07C67/08 , C07C69/16 , C07C203/04
摘要： The invention relates to a safe and efficient process for the hydrolysis of α,ω-C3-10alkanediol mononitrate monoacylates. The process is safer to operators and allows to obtain advantageous yields on industrial scale.

5. 发明申请

WO2014023848A1 PROTECTED TOCOPHEROL WITH REDUCED CONTENT OF FREE TOCOPHEROL 审中-公开
标题翻译：具有降低免费TOCOPHEROL含量的保护的TOCOPHEROL
公开(公告)号：WO2014023848A1
公开(公告)日：2014-02-13
申请号：PCT/EP2013/066819
申请日：2013-08-12
申请人： DSM IP ASSETS B.V.
发明人： WILDERMANN, Angela
IPC分类号： C07D311/72
CPC分类号： C07D311/72
摘要： The present invention relates to a method of preparing a protected tocopherol with a reduced content of free tocopherol, comprising the step of contacting the tocopherol used for the preparation of the protected tocopherol in neat or in the form of a highly concentrated solution with an acid activated bleaching earth. The method is rather efficient in removal of substantial amounts of this impurity.
摘要翻译：本发明涉及一种制备具有降低的游离生育酚含量的受保护的生育酚的方法，其包括使用于制备受保护的生育酚的生育酚以高浓缩溶液的形式与酸活化漂白土该方法相当有效地去除大量的这种杂质。

6. 发明申请

WO2007121826A1 TRANSPORT OF ETHYNE IN FORM OF α-ALKYNOLS AS ETHYNE PRECURSORS 审中-公开
标题翻译：乙烯在乙烯前驱物中的运输
公开(公告)号：WO2007121826A1
公开(公告)日：2007-11-01
申请号：PCT/EP2007/002885
申请日：2007-03-30
申请人： DSM IP ASSETS B.V. , WILDERMANN, Angela , BONRATH, Werner , HELLMANN, Gunther
发明人： WILDERMANN, Angela , BONRATH, Werner , HELLMANN, Gunther
IPC分类号： C07C11/24 , C07C1/20 , C07C7/20 , C10L3/02 , C07C29/42
CPC分类号： C07C29/42 , C07C1/20 , C07C7/20 , C07C11/24 , C10L3/02 , C07C33/042 , C07C33/048
摘要： The present invention relates to a new method for a safe transport of ethyne in form of α-alkynols as precursors for ethyne. The new method comprises three steps. In a first step the synthesis of the α-alkynol(s) is performed by reacting ethyne with (a) carbonyl compound(s). The second step comprises the transport of the resulting α-alkynol(s) in a safe manner, whereas the safety requirements for this transport are not as high as for ethyne because α-alkynol(s) are normally classified for transportation as hazardous class 3. In the third step the α-alkynol(s) can be cleaved and the ethyne and the carbonyl compound(s) can be obtained in the cleavage reaction and can be separated to yield pure products for further applications.
摘要翻译：本发明涉及一种安全运输乙炔形式的乙炔作为乙炔前体的新方法。新方法包括三个步骤。在第一步中，α-炔醇的合成通过使乙炔与（a）羰基化合物反应来进行。第二步包括以安全的方式运输所得的α-炔醇，而这种运输的安全要求不如乙炔那么高，因为α-炔醇通常被分类为危险品类3 在第三步中，α-炔醇可以被切割，并且可以在裂解反应中获得乙炔和羰基化合物，并且可以分离得到用于进一步应用的纯产物。

7. 发明申请

WO2021214145A1 PROCESS FOR NITRATE ESTER FORMATION OF AN ALPHA,OMEGA-ALKANEDIOL MONOACYLATE 审中-公开
公开(公告)号：WO2021214145A1
公开(公告)日：2021-10-28
申请号：PCT/EP2021/060406
申请日：2021-04-21
申请人： DSM IP ASSETS B.V.
发明人： RIEBEL, Peter Hans , WILDERMANN, Angela
IPC分类号： C07C201/02 , C07C67/08 , C07C69/16 , C07C203/04
摘要： The invention relates to a safe and efficient process for the nitrate ester formation of an α,ω-C3-10alkanediol monoacylate. The process is safer to operators and allows to obtain advantageous yields on industrial scale.

8. 发明申请

WO2019115503A1 PROPANEDIOL MONOACETATE MONONITRATE 审中-公开
公开(公告)号：WO2019115503A1
公开(公告)日：2019-06-20
申请号：PCT/EP2018/084299
申请日：2018-12-11
申请人： DSM IP ASSETS B.V.
发明人： MENDROK-EDINGER, Christine , RIEBEL, Peter , WILDERMANN, Angela
IPC分类号： A61K8/40 , A61Q5/00 , A61Q15/00 , A61Q17/00 , A61Q19/00 , A61P17/10 , A61P17/06 , A61P17/08
CPC分类号： A61K8/40 , A61P17/06 , A61P17/08 , A61P17/10 , A61Q5/006 , A61Q15/00 , A61Q17/005 , A61Q19/00
摘要： The present invention relates to propanediol monoacetate mononitrate as well as the use thereof as antimicrobial agent, in particular for cosmetic applications.

9. 发明申请

WO2014023845A1 TOCOPHEROLS WITH REDUCED CONTENT OF DEHYDROTOCOPHEROL 审中-公开
标题翻译：具有降低内含物含量的植物油
公开(公告)号：WO2014023845A1
公开(公告)日：2014-02-13
申请号：PCT/EP2013/066814
申请日：2013-08-12
申请人： DSM IP ASSETS B.V.
发明人： WILDERMANN, Angela , EBNER, Niklas , STAEUBLE, Viktor , WEYLAND, Andreas , DOORNENBAL, Otto
IPC分类号： C07D311/72
CPC分类号： C07D311/72
摘要： The present invention relates to a method of preparing a tocopherol or protected tocopherol with a reduced content of dehydrotocopherol or protected dehydrotocopherol comprising the step of contacting tocopherol or protected tocopherol in neat or in the form of a highly concentrated solution with an acid activated bleaching earth. This method is rather efficient in removal of substantial amounts of this impurity.
摘要翻译：本发明涉及一种制备具有降低的脱氢生育酚含量或受保护的脱氢生育酚含量的生育酚或保护的生育酚的方法，其包括以酸活化的漂白土与纯化或以高度浓缩的溶液形式接触生育酚或保护的生育酚的步骤。该方法相当有效地去除大量的这种杂质。

10. 发明申请

WO2013120808A1 NOVEL PROCESS FOR THE MANUFACTURE OF METHYL LIMONITRILE 审中-公开
标题翻译：用于制造甲基硫酸钠的新工艺
公开(公告)号：WO2013120808A1
公开(公告)日：2013-08-22
申请号：PCT/EP2013/052689
申请日：2013-02-11
申请人： DSM IP ASSETS B.V.
发明人： WILDERMANN, Angela , BONRATH, Werner , BEUMER, Raphael , DORN, Silke
IPC分类号： C07C253/30 , C07C255/07
CPC分类号： C07C253/10 , C07C253/30 , C07C253/34 , C07C255/07
摘要： The present invention is directed to a process for the manufacture of methyl limonitrile comprising a mixture of 3,7-dimethyl-2,6-nonadiene nitrile, 3,7-dimethyl-3,6-nonadiene nitrile and 7-methyl-3-methylene-6-nonene nitrile comprising the following steps: a) reacting 6-methyl-5-octen-2-one with cyano acetic acid and removing carbon dioxide and water, wherein the reaction and the removal of carbon dioxide and water are performed in the presence of a base and a co-base 1 in an organic solvent, and wherein the organic solvent is a solvent which forms a heteroazeotrop with water; b) removing the solvent and the base of the reaction mixture obtained after having performed step a) or step c) by distillation to obtain a reaction mixture, whereby this step may optionally be performed in the presence of a co-base 2; c) isomerizing the reaction mixture obtained after having performed step a) or step b) to obtain an isomerized reaction mixture in the presence of a co-base 2; whereby step b) can be performed before or after step c).
摘要翻译：本发明涉及一种制备甲基有限公司的方法，该方法包括3,7-二甲基-2,6-壬二烯腈，3,7-二甲基-3,6-壬二烯腈和7-甲基-3- 亚甲基-6-壬烯腈包括以下步骤：a）使6-甲基-5-辛烯-2-酮与氰基乙酸反应并除去二氧化碳和水，其中二氧化碳和水的反应和除去在在有机溶剂中存在碱和共碱1，其中有机溶剂是与水形成杂合性的溶剂; b）通过蒸馏除去在进行步骤a）或步骤c）之后获得的反应混合物的溶剂和碱，得到反应混合物，由此该步骤可任选地在共碱2存在下进行; c）使在步骤a）或步骤b）中获得的反应混合物异构化，以在共碱2存在下得到异构化反应混合物; 由此步骤b）可以在步骤c）之前或之后进行。

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