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1. 发明申请

WO2015088867A2 BUTADIENE TELOMERIZATION CATALYST PRECURSOR PREPARATION 审中-公开
标题翻译：丁二烯催化剂前体制备
公开(公告)号：WO2015088867A2
公开(公告)日：2015-06-18
申请号：PCT/US2014/068483
申请日：2014-12-04
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： LAUNAY, Helene N. , KLINKENBERG, Jessica L. , BRIGGS, John R. , HOUSE, Sarah E. , VAN ENGELEN, Marcel C. , WRIGHT, Larry G. , BAR, Georg , HANSEN, Wilma , CABELLO FUERTES, Julia , LENGYEL, Istvan
IPC分类号： C07F15/00
CPC分类号： B01J31/2438 , B01J31/2404 , B01J2231/20 , B01J2531/824 , C07F15/006
摘要： Use a solvent blend that contains 1-methoxy-2,7-octadiene and an alkanols rather than the alkanols by itself to prepare a catalyst precursor suitable for use in butadiene telomerization.
摘要翻译：使用含有1-甲氧基-2,7-辛二烯和链烷醇而不是链烷醇的溶剂共混物，以制备适合用于丁二烯调聚的催化剂前体。

2. 发明申请

WO2020061151A1 METHODS FOR PREPARING ARYLPHOSPHINE-BORANE COMPLEXES 审中-公开
公开(公告)号：WO2020061151A1
公开(公告)日：2020-03-26
申请号：PCT/US2019/051662
申请日：2019-09-18
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： TU, Siyu , KLINKENBERG, Jessica L. , HE, Yiyong , CHEN, Xiaoyun , LI, Haoquan , REMY, Matthew S.
IPC分类号： C01B6/13
摘要： A method for preparing phosphine-borane complexes from aryldihalophosphine includes mixing sodium borohydride, a solvent having at least 50 vol% glycol ethers, and the aryldihalophosphine to obtain a solution. The solution is maintained at a reaction temperature for a duration of time to obtain the phosphine-borane complexes. The solvent may include 1,2-dimethoxyethane and tetrahydrofuran. A ratio of tetrahydrofuran to 1,2-dimethoxyethane in the solvent may be from 0.1:1.0 to 2.5:1.0.

3. 发明申请

WO2014205025A1 ARYL PHOSPHINES WITH FUSED RING ORTHO-ALKOXY SUBSTITUTION 审中-公开
标题翻译： ARYL磷酸盐与熔融的OROO-ALKOXY取代
公开(公告)号：WO2014205025A1
公开(公告)日：2014-12-24
申请号：PCT/US2014/042846
申请日：2014-06-18
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： CLARK, Thomas P. , SPINNEY, Heather A. , HOUSE, Sarah E. , BRIGGS, John R. , CUMMINS, Clark H. , KLINKENBERG, Jessica L.
IPC分类号： C07F9/50 , B01J31/24 , C07F15/00
CPC分类号： B01J31/2457 , B01J31/2404 , B01J31/2414 , B01J31/2433 , B01J2231/20 , B01J2531/824 , B01J2540/10 , C07F9/50 , C07F9/5045 , C07F9/65517 , C07F9/65522 , C07F9/65527 , C07F15/006 , C07F15/0073 , C07F15/008
摘要： An aryl phosphine with fused ring ortho-alkoxy substitution that includes an aryl monophosphine and an aryl bisphosphine.
摘要翻译：具有稠环邻位烷氧基取代的芳基膦，其包括芳基单膦和芳基双膦。

4. 发明申请

WO2016164258A1 BUTADIENE TELOMERIZATION CATALYST AND PREPARATION THEREOF 审中-公开
标题翻译：丁二烯催化剂及其制备方法
公开(公告)号：WO2016164258A1
公开(公告)日：2016-10-13
申请号：PCT/US2016/025472
申请日：2016-04-01
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： KLINKENBERG, Jessica L. , BRIGGS, John R.
IPC分类号： C07C2/40 , C07F15/00 , C07C41/06
CPC分类号： C07C2/406 , B01J31/2438 , B01J2231/20 , B01J2531/824 , C07C41/06 , C07C2531/24 , C07C43/15
摘要： Catalyst compositions are prepared by contacting a palladium source and 1,3,5,7-tetramethyl-6-(2,4-dimethoxyphenyl)-2,4,8-trioxa-6-phosphaadamantane and a methoxyocta-diene compound, in a primary aliphatic alcohol, under suitable conditions including a ratio of equivalents of palladium to equivalents of 1,3,5,7-tetramethyl-6-(2,4-dimethoxyphenyl)-2,4,8-trioxa-6-phosphaadamantane ranging from greater than 1:1 to 1:1.3. The result is a complex of palladium, a 1,3,5,7-tetramethyl-6-(2,4-dimethoxyphenyl)-2,4,8-trioxa-6-phosphaada-mantane ligand, and a ligand selected from a methoxyoctadiene ligand, an octadienyl ligand, or a protonated octadienyl. Such complexes may, in solution, exhibit surprising solubility and storage stability and are useful in the telomerization of butadiene, which is a step in the production of 1-octene.
摘要翻译：催化剂组合物通过使钯源和1,3,5,7-四甲基-6-（2,4-二甲氧基苯基）-2,4,8-三氧杂-6-磷杂金刚烷和甲氧基辛二烯化合物在脂肪醇，在适当的条件下，包括钯当量与1,3,5,7-四甲基-6-（2,4-二甲氧基苯基）-2,4,8-三氧杂-6-磷杂金刚烷的当量比例范围从大于1：1至1：1.3。其结果是钯，1,3,5,7-四甲基-6-（2,4-二甲氧基苯基）-2,4,8-三氧杂-6-磷杂 - 金刚烷配体和选自甲氧基辛二烯配体，辛二烯基配体或质子化的八苯基。这种络合物在溶液中可以表现出令人惊奇的溶解性和储存稳定性，并且可用于丁二烯的调聚，丁苯是生产1-辛烯的一个步骤。

5. 发明申请

WO2018175671A1 METHODS FOR FORMING 1,3,5,7-TETRAALKYL-6-(2,4-DIMETHOXYPHENYL)-2,4,8-TRIOXA-6-PHOSPHAADAMANTANE 审中-公开
公开(公告)号：WO2018175671A1
公开(公告)日：2018-09-27
申请号：PCT/US2018/023678
申请日：2018-03-22
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： KLINKENBERG, Jessica L. , BRIGGS, John R. , CAMELIO, Andrew M. , GRIGG, Robert David , TU, Siyu
IPC分类号： C07F9/6571
摘要： A method for forming 1,3,5,7-tetraalkyl-6-(2,4-dimethoxyphenyl)-2,4,8-trioxa-6-phosphaadamantane includes obtaining a solution comprising an ethereal solvent and an aluminum hydride, adding dichloro(2,4-dimethoxyphenyl)phosphine to the solution to produce 2,4-dimethoxyphenylphosphine, and reacting the 2,4-dimethoxyphenylphosphine with an acidic mixture comprising diones to produce 1,3,5,7-tetraalkyl-6-(2,4-dimethoxyphenyl)-2,4,8-trioxa-6-phosphaadamantane. The solution has a temperature from greater than -20 C to 50 C throughout the method. Another method for forming 1,3,5,7-tetraalkyl-6-(2,4-dimethoxyphenyl)-2,4,8-trioxa-6-phosphaadamantane includes obtaining dichloro(2,4-dimethoxyphenyl)phosphine, forming 2,4-dimethoxyphenylphosphine by adding the dichloro(2,4-dimethoxyphenyl)phosphine to a solution comprising at least one solvent and an aluminum hydride, reacting the 2,4-dimethoxyphenylphosphine with a mixture to produce 1,3,5,7-tetraalkyl-6-(2,4-dimethoxyphenyl)-2,4,8-trioxa-6-phosphaadamantane. The mixture includes an acid selected from the group consisting of Lewis acids, sulfonic Bronsted acids, and mixtures thereof, an aromatic or non-aromatic hydrocarbons; and acetylacetone.

6. 发明申请

WO2017173074A1 AN OLEFIN POLYMERIZATION CATALYST 审中-公开
标题翻译：一种烯烃聚合催化剂
公开(公告)号：WO2017173074A1
公开(公告)日：2017-10-05
申请号：PCT/US2017/025009
申请日：2017-03-30
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： BAILEY, Brad C. , CHRISTIANSON, Matthew D. , DAVIS, Anna V. , CAMELIO, Andrew M. , FROESE, Robert, D.J. , KLINKENBERG, Jessica L.
IPC分类号： C08F210/16 , C08F2/38 , C08F4/64
摘要： An olefin polymerization catalyst system comprising: a procatalyst component comprising a metal-ligand complex of Formula (I) wherein each X is independently a monodentate or polydentate ligand that is neutral, monoanionic, or dianionic, wherein n is an integer, and wherein X and n are chosen such that the metal-ligand complex of Formula (I) is overall neutral; wherein each R1 and R5 independently is selected from (C1-C40)hydrocarbyls, substituted (C1-C40)hydrocarbyls; (C1-C-40)heterohydrocarbyls and substituted (C1-C40)heterohydrocarbyls; wherein each R2 and R4 independently is selected from (C1-C40)hydrocarbyls andsubstituted (C1-C40)hydrocarbyls; wherein R3 is selected from the group consisting of a (C3-C40)hydrocarbylene, substituted (C3-C40)hydrocarbylene, [(C+Si)3-(C+Si)40]organosilylene, substituted [(C+Si)3-(C+Si)40]organosilylene, [(C+Ge)3-(C+Ge)40]organogermylene, or substituted [(C+Ge)3-(C+Ge)40]organogermylene; wherein each N independently is nitrogen; and optionally, two or more R1-5 groups each independently can combine together to form mono-aza ring structures, with such ring structures having from 5 to 16 atoms in the ring excluding any hydrogen atoms.
摘要翻译：烯烃聚合催化剂体系，其包含：包含式（I）的金属 - 配体络合物的前催化剂组分，其中每个X独立地为中性，单阴离子或双阴离子的单齿或多齿配体，其中n 是整数，并且其中选择X和n使得式（I）的金属 - 配体络合物总体上是中性的; 其中每个R 1和R 5独立地选自（C 1 -C 40）烃基，取代的（C 1 -C 40）烃基; （C1-C40）杂烃基和取代的（C1-C40）杂烃基; 其中每个R 2和R 4独立地选自（C 1 -C 40）烃基和取代的（C 1 -C 40）烃基; 其中R3选自（C3-C40）亚烃基，取代的（C3-C40）亚烃基，[（C + Si）3-（C + Si）40] （C + Si）40]有机亚甲硅烷基，[（C + Ge）3-（C + Ge）40]有机亚锗烷基或取代的[（C + Ge）3- 其中每个N独立地为氮; 并且任选地，两个或更多个R 1至R 5基团各自独立地可以结合在一起形成单氮杂环结构，其中这样的环结构在环中具有5至16个原子，排除任何氢原子。

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