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1. 发明申请

WO2010046532A1 PROCESS OF PRODUCING XYLOSE AND DISSOLVING PULP 审中-公开
标题翻译：生产木糖和溶解浆的方法
公开(公告)号：WO2010046532A1
公开(公告)日：2010-04-29
申请号：PCT/FI2009/050840
申请日：2009-10-20
申请人： DANISCO A/S , HEIKKILÄ, Heikki , LEWANDOWSKI, Jari , LINDROOS, Mirja , SAARI, Pia
发明人： HEIKKILÄ, Heikki , LEWANDOWSKI, Jari , LINDROOS, Mirja , SAARI, Pia
IPC分类号： C13K13/00 , D21C1/04 , D21C3/02
CPC分类号： C13K13/002 , C13B20/148 , C13B20/165 , C13B30/02 , C13K1/04 , D21C1/04 , D21C3/02 , D21C11/0007
摘要： The present invention relates to a process for the production of xylose and dissolving pulp from xylan-containing biomass, such as hardwood. The invention is based on prehydrolysis of the xylan-containing biomass with SO 2 in specified conditions, followed by chromatographic fractionation, nanofiltration or precipitation crystallization of the xylose-containing prehydrolyzate to obtain a xylose product having a xylose content of at least 55% on DS. The dissolving pulp obtained from the process can be used for example for the production of viscose.
摘要翻译：本发明涉及由含木聚糖的生物质如硬木生产木糖和溶解纸浆的方法。本发明基于在特定条件下含SO 2的含木聚糖生物质的预水解，然后进行色谱分级，含木糖的预水解产物的纳滤或沉淀结晶，得到DS上木糖含量至少为55％的木糖产物。从该方法获得的溶解纸浆可用于例如粘胶纤维的生产。

2. 发明申请

WO2005042788A1 SEPARATION PROCESS 审中-公开
标题翻译：分离过程
公开(公告)号：WO2005042788A1
公开(公告)日：2005-05-12
申请号：PCT/FI2004/000641
申请日：2004-10-29
申请人： DANISCO SWEETENERS OY , HEIKKILÄ, Heikki , KOIVIKKO, Hannu , NURMI, Juha , MATTILA, Jari , SAARI, Pia , NURMI, Nina , SARMALA, Päivi , LINDROOS, Mirja , LEWANDOWSKI, Jari
发明人： HEIKKILÄ, Heikki , KOIVIKKO, Hannu , NURMI, Juha , MATTILA, Jari , SAARI, Pia , NURMI, Nina , SARMALA, Päivi , LINDROOS, Mirja , LEWANDOWSKI, Jari
IPC分类号： C13K13/00
CPC分类号： C07H1/08 , C13K13/00 , C13K13/007
摘要： The invention relates to a process of recovering arabinose and optionally other monosaccharides from vegetable fiber rich in heteropolymeric arabinose, such as gum arabic. Said other monosaccharides are typically selected from galactose and rhamnose. The process of the invention comprises controlled hydrolysis of the arabinose-rich vegetable fiber and fractionation of the hydrolysis product to obtain a fraction enriched in arabinose and optionally other product fractions followed by crystallization of arabinose. The invention also relates to a novel method of crystallizing arabinose from biomass-derived material. Furthermore, the invention relates to novel crystalline L-arabinose.
摘要翻译：本发明涉及从富含异聚阿拉伯糖的植物纤维如阿拉伯树胶中回收阿拉伯糖和任选的其它单糖的方法。所述其它单糖通常选自半乳糖和鼠李糖。本发明的方法包括控制富含阿拉伯糖的植物纤维的水解和水解产物的分级，以获得富含阿拉伯糖和任选的其它产物级分的级分，然后结晶阿拉伯糖。本发明还涉及从生物质衍生的材料中结晶阿拉伯糖的新方法。此外，本发明涉及新的结晶L-阿拉伯糖。

3. 发明申请

WO2005040430A1 SEPARATION OF SUGARS 审中-公开
标题翻译：糖的分离
公开(公告)号：WO2005040430A1
公开(公告)日：2005-05-06
申请号：PCT/FI2004/000557
申请日：2004-09-22
申请人： DANISCO SWEETENERS OY , JUMPPANEN, Juho , RAVANKO, Vili , HEIKKILÄ, Heikki , NURMI, Juha , NURMI, Nina , SAARI, Pia , HÄKKÄ, Katja , LEWANDOWSKI, Jari
发明人： JUMPPANEN, Juho , RAVANKO, Vili , HEIKKILÄ, Heikki , NURMI, Juha , NURMI, Nina , SAARI, Pia , HÄKKÄ, Katja , LEWANDOWSKI, Jari
IPC分类号： C13K13/00
CPC分类号： C13B20/142 , C13K13/00
摘要： The invention relates to the recovery of deoxy sugars, such as fucose from biomass-derived solutions, such as spent liquors obtained from pulping processes. The invention also relates to the recovery of glycosides from biomass. The invention is based on the use of chromatographic fractionation with specific column packing materials and combinations thereof using water as the eluent. The deoxy sugar product obtained from the chromatographic fractionation may be further purified by crystallization. The invention also provides a novel crystalline L-fucose product and a novel process for the crystallization of fucose.
摘要翻译：本发明涉及从生物质衍生的溶液中回收脱氧糖，例如岩藻糖，例如从制浆方法获得的废液。本发明还涉及从生物质中回收糖苷。本发明基于使用具有特定柱填充材料的色谱分离和使用水作为洗脱液的组合。从色谱分离得到的脱氧糖产品可通过结晶进一步纯化。本发明还提供了一种新型的结晶L-岩藻糖产物和岩藻糖结晶的新方法。

4. 发明申请

WO2007138167A1 SEPARATION PROCESS 审中-公开
标题翻译：分离过程
公开(公告)号：WO2007138167A1
公开(公告)日：2007-12-06
申请号：PCT/FI2007/050306
申请日：2007-05-29
申请人： DANISCO A/S , HEIKKILÄ, Heikki , KOIVIKKO, Hannu , LEWANDOWSKI, Jari , MÄNTTÄRI, Mika , MATTILA, Jari
发明人： HEIKKILÄ, Heikki , KOIVIKKO, Hannu , LEWANDOWSKI, Jari , MÄNTTÄRI, Mika , MATTILA, Jari
IPC分类号： C13D3/16 , B01D61/00 , B01D61/02 , C13K13/00
CPC分类号： C13B35/08 , B01D61/027 , B01D2315/14 , C13B20/165
摘要： The invention relates to an improved nanofiltration process for separating and recovering components, such as sug ars and sugar alcohols from multicomponent mixtures. The process of the invention is characterized by collecting the nanofiltration retentate/permeate in several fractions with different purity, optional recycling of at least one of the collected nanofiltration retentate/permeate fractions to the nanofiltration and recovering the desired component from the nanofiltration permeate/retentate fractions by dif ferent methods. In one embodiment of the invention, the process comprises a combination of nanofiltration and chromatography.
摘要翻译：本发明涉及用于从多组分混合物中分离和回收组分如糖和糖醇的改进的纳滤方法。本发明的方法的特征在于以不同纯度的几个级分收集纳滤过滤滞留物/渗透物，任选地将收集的纳滤渗余物/渗透物部分中的至少一种再循环到纳滤中，并从纳滤过滤渗透物/渗余物馏分中回收所需组分通过不同的方法。在本发明的一个实施方案中，该方法包括纳滤和层析的组合。

5. 发明申请

WO2010097511A1 SEPARATION PROCESS 审中-公开
标题翻译：分离过程
公开(公告)号：WO2010097511A1
公开(公告)日：2010-09-02
申请号：PCT/FI2010/050127
申请日：2010-02-24
申请人： DANISCO A/S , AIRAKSINEN, Jyrki , HEIKKILÄ, Heikki , LEWANDOWSKI, Jari , LAIHO, Kari
发明人： AIRAKSINEN, Jyrki , HEIKKILÄ, Heikki , LEWANDOWSKI, Jari , LAIHO, Kari
IPC分类号： B01D15/10 , B01D15/18 , C13D3/14
CPC分类号： C13B20/14 , B01D15/185 , B01D15/362 , B01D15/363 , C07H1/06 , C13K13/00
摘要： The present invention relates to a chromatographic separation process for fractionating betaine-containing solutions by utilizing fractions comprising parts of the separation profile as a substituent of the eluent in a novel and inventive manner. The process provides improved separation capacity and separation efficiency without affecting the yield or purity of betaine or other products. The process can especially be applied to sequential SMB separation systems.
摘要翻译：本发明涉及一种色谱分离方法，用于通过以新颖和创新的方式利用包含部分分离分布作为洗脱液的取代基的级分来分馏含甜菜碱的溶液。该方法提供了改善的分离能力和分离效率，而不影响甜菜碱或其他产品的产率或纯度。该过程可以特别适用于连续的SMB分离系统。

6. 发明申请

WO2010097510A1 SEPARATION PROCESS 审中-公开
标题翻译：分离过程
公开(公告)号：WO2010097510A1
公开(公告)日：2010-09-02
申请号：PCT/FI2010/050126
申请日：2010-02-24
申请人： DANISCO A/S , AIRAKSINEN, Jyrki , HEIKKILÄ, Heikki , LEWANDOWSKI, Jari , LAIHO, Kari , SARMALA, Päivi
发明人： AIRAKSINEN, Jyrki , HEIKKILÄ, Heikki , LEWANDOWSKI, Jari , LAIHO, Kari , SARMALA, Päivi
IPC分类号： B01D15/10 , B01D15/18 , C13D3/14
CPC分类号： C13B20/14 , B01D15/185 , B01D15/362 , B01D15/363 , C07H1/06 , C13K13/00
摘要： The present invention relates to a chromatographic separation process for fractionating solutions containing sugars, sugar alcohols, sugar acids and/or betaine by utilizing fractions comprising parts of the separation profile as a substituent of the eluent in a novel and inventive manner. The starting solutions are typically multicomponent plant- based extracts and hydrolysates, stillages, and fermentation products and derivatives thereof. The process provides improved separation capacity and separation efficiency without affecting the yield or purity of product components, such as sugars, sugar alcohols, sugar acids, and betaine. The process can especially be applied to sequential SMB separation systems.
摘要翻译：本发明涉及一种色谱分离方法，其通过以新颖和创造性方式利用包含部分分离分布作为洗脱液的取代基的级分来分馏含有糖，糖醇，糖酸和/或甜菜碱的溶液。起始溶液通常是多组分植物为基础的提取物和水解产物，水解产物及其发酵产物及其衍生物。该方法提供了提高的分离能力和分离效率，而不影响产物组分如糖，糖醇，糖酸和甜菜碱的产率或纯度。该过程可以特别适用于连续的SMB分离系统。

7. 发明申请

WO2009155982A1 PROCESS FOR SEPARATION OF CA- OR MG-SULFITE SPENT LIQUOR TO YIELD CRYSTALLINE XYLOSE 审中-公开
标题翻译：将CA-或MG-硫酸酯液体分离成晶体晶体的方法
公开(公告)号：WO2009155982A1
公开(公告)日：2009-12-30
申请号：PCT/EP2008/058172
申请日：2008-06-26
申请人： DANISCO A/S , HEIKKILÄ, Heikki , LEWANDOWSKI, Jari
发明人： HEIKKILÄ, Heikki , LEWANDOWSKI, Jari
IPC分类号： C13D3/14 , C13K13/00 , C13J1/06 , B01D15/36 , B01D15/38 , B01J39/04 , B01J39/26 , C08H5/02
CPC分类号： C13K13/002 , B01D15/362 , C08H6/00 , C13B20/144 , C13B35/06
摘要： A process for the separation of a xylose-containing, lignosulphonate-containing Ca-sulfite spent liquor is provided. The process comprises a first step of : (A) chromatographic separation of the Ca- or Mg-sulfite spent liquor using a single pass through a batch- type long resin bed chromatography column having a strong acid cation exchange resin as a separation medium. The ratio of the bed length: mean resin bead diameter of the column is 10,000- 40,000. This step yields •a first xylose-rich fraction having a xylose content 50- 70 wt. % based on dry solids and • a lignosulphonate-rich fraction. The process further comprises a step of : (B) crystallizing xylose from the first xylose rich fraction by using a crystallization method comprising (i) boiling crystallization; (ii) cooling crystallization or (iii) a combination of (i) and (ii) to obtain a first batch of crystalline xylose and a first xylose run-off. The process provides a simplification of existing methods, and at the same time allows advantages such as improved xylose yield and improved xylose purity.
摘要翻译：提供了一种用于分离含木糖的含木质素磺酸盐的亚硫酸钙废液的方法。该方法包括以下步骤：（A）使用单次通过具有强酸性阳离子交换树脂作为分离介质的间歇型长树脂床色谱柱对Ca-或Mg-亚硫酸盐废液进行色谱分离。床长的比例：柱的平均树脂珠粒直径为10,000-40,000。该步骤产生具有木糖含量为50-70重量％的第一富含木糖的级分。基于干固体和富含木素磺酸盐的级分。该方法还包括以下步骤：（B）通过使用包含（i）沸腾结晶的结晶方法从第一富含木糖的级分结晶木糖; （ii）冷却结晶或（iii）（i）和（ii）的组合以获得第一批结晶木糖和第一木糖流出物。该方法提供了现有方法的简化，并且同时可以获得诸如改善木糖产量和改善木糖纯度的优点。

8. 发明申请

WO2004003236A1 CRYSTALLIZATION OF SUGARS 审中-公开
标题翻译：糖的结晶
公开(公告)号：WO2004003236A1
公开(公告)日：2004-01-08
申请号：PCT/FI2003/000521
申请日：2003-06-26
申请人： DANISCO SWEETENERS OY , KOIVIKKO, Hannu , KAARTO, Minna , HEIKKILÄ, Heikki , LINDROOS, Mirja , NURMI, Juha
发明人： KOIVIKKO, Hannu , KAARTO, Minna , HEIKKILÄ, Heikki , LINDROOS, Mirja , NURMI, Juha
IPC分类号： C13D3/16
CPC分类号： C13B30/02 , B01D15/362 , B01D15/363 , C13B20/12 , C13B20/165 , C13K11/00 , C13K13/002
摘要： The invention relates to removing crystallization inhibitors from a solution comprising one or more reducing sugars by nanofiltration, hydrolysis and/or chromatography.The reducing sugars are typically selected from fructose and xylose.
摘要翻译：本发明涉及通过纳滤，水解和/或色谱从包含一种或多种还原糖的溶液中除去结晶抑制剂。还原糖通常选自果糖和木糖。

9. 发明申请

WO2005001145A1 A METHOD FOR RECOVERING GALACTOSE FROM A SOLUTION DERIVED FROM PLANT-BASE BIOMASS USING CHROMATOGRAPHIC FRACTIONATION STEPS AND CRYSTALLISATION 审中-公开
标题翻译：从使用色谱分离步骤和晶体结构的植物生物量衍生的溶液中回收角质醇的方法
公开(公告)号：WO2005001145A1
公开(公告)日：2005-01-06
申请号：PCT/FI2004/000388
申请日：2004-06-24
申请人： DANISCO SWEETENERS OY , HEIKKILÄ, Heikki , HÄKKÄ, Katja , JUMPPANEN, Juho , SAARI, Pia , NURMI, Nina , RAVANKO, Vili
发明人： HEIKKILÄ, Heikki , HÄKKÄ, Katja , JUMPPANEN, Juho , SAARI, Pia , NURMI, Nina , RAVANKO, Vili
IPC分类号： C13K13/00
CPC分类号： B01J20/288 , B01D15/362 , B01D15/363 , B01J39/26 , B01J41/20 , C13B20/144 , C13B20/146 , C13K13/00
摘要： The invention relates to a process of recovering galactose from a solution derived from plant-based biomass. In the process of the invention, the starting solution is subjected to one or more chromatographic fractionation steps, which may carried out with a strongly basic anion exchange resin and optionally with a strongly acid cation exchange resin, in any desired sequence, followed by recovering at least one fraction enriched in galactose. The galactose fraction thus obtained is further purified by crystallization to obtain crystalline galactose. The invention also relates to non-animal derived crystalline D-galactose.
摘要翻译：本发明涉及从源自植物的生物质的溶液中回收半乳糖的方法。在本发明的方法中，将起始溶液进行一个或多个色谱分离步骤，其可以用强碱性阴离子交换树脂和任选的强酸阳离子交换树脂以任何所需的顺序进行，随后在至少一份富含半乳糖。由此获得的半乳糖部分通过结晶进一步纯化，得到晶体半乳糖。本发明还涉及非动物衍生的结晶D-半乳糖。

10. 发明申请

WO2004076021A1 A SIMULATED MOVING BED SYSTEM AND PROCESS 审中-公开
标题翻译：模拟移动床系统和过程
公开(公告)号：WO2004076021A1
公开(公告)日：2004-09-10
申请号：PCT/FI2004/000099
申请日：2004-02-25
申请人： FINNFEEDS FINLAND OY , PAANANEN, Hannu , KUISMA, Jarmo , HEIKKILÄ, Heikki , RAVANKO, Vili , LEWANDOWSKI, Jari , KÄRKI, Ari
发明人： PAANANEN, Hannu , KUISMA, Jarmo , HEIKKILÄ, Heikki , RAVANKO, Vili , LEWANDOWSKI, Jari , KÄRKI, Ari
IPC分类号： B01D15/08
CPC分类号： B01D15/361 , B01D15/1842 , B01D15/362 , B01D15/363 , B01J20/28004 , B01J47/026 , B01J47/10 , C07C227/40 , C07H1/06 , C07H1/08 , C07H3/02 , C07H3/04 , C13B20/14 , C07C229/12
摘要： The invention relates to a system and a process for fractionating a solution into two or more fractions. The system of the invention comprises at least two compartments having a diameter of at least about one meter and including a uniform packing of a polymer-based ion exchange resin with a bead size in the range of about 50 to about 250 µm. The mixing volume of the fluid fronts in the system of the invention is not more than 5% of the volume of the compartment.
摘要翻译：本发明涉及一种将溶液分馏成两个或多个馏分的系统和方法。本发明的系统包括至少两个具有至少约一米的直径的隔室，并且包括具有约50至约250μm范围内的珠粒尺寸的基于聚合物的离子交换树脂的均匀包装。本发明系统中的流体前面的混合体积不超过隔室体积的5％。

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