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1. 发明申请

WO2011121181A1 SEPARATION PROCESS 审中-公开
标题翻译：分离过程
公开(公告)号：WO2011121181A1
公开(公告)日：2011-10-06
申请号：PCT/FI2011/050264
申请日：2011-03-29
申请人： DANISCO A/S , AIRAKSINEN, Jyrki , PAANANEN, Hannu , LEWANDOWSKI, Jari , LAIHO, Kari
发明人： AIRAKSINEN, Jyrki , PAANANEN, Hannu , LEWANDOWSKI, Jari , LAIHO, Kari
IPC分类号： B01D15/18 , C13K13/00 , C13B35/06 , C07C229/12
CPC分类号： C13B20/148 , B01D15/185 , C07C227/40 , C13K13/00 , C07C229/12
摘要： The invention relates to a three-profile chromatographic sequential SMB process of separating and recovering products such as sugars and betaine from multicomponent feed solutions. In the process of the invention, product fractions and optionally recycle fractions are collected from several positions of the chromatographic separation system. The process of the invention may be applied to the separation of sucrose and betaine from sugar beet based solutions and to the separation of sugars, e.g. xylose, from plant-based hydrolysates, for example.
摘要翻译：本发明涉及从多组分进料溶液中分离和回收产物如糖和甜菜碱的三色谱色谱顺序SMB方法。在本发明的方法中，从色谱分离系统的几个位置收集产物级分和任选的再循环级分。本发明的方法可以应用于从甜菜基溶液中分离蔗糖和甜菜碱以及分离糖，例如蔗糖和甜菜碱。木糖，例如来自植物的水解产物。

2. 发明申请

WO2007138167A1 SEPARATION PROCESS 审中-公开
标题翻译：分离过程
公开(公告)号：WO2007138167A1
公开(公告)日：2007-12-06
申请号：PCT/FI2007/050306
申请日：2007-05-29
申请人： DANISCO A/S , HEIKKILÄ, Heikki , KOIVIKKO, Hannu , LEWANDOWSKI, Jari , MÄNTTÄRI, Mika , MATTILA, Jari
发明人： HEIKKILÄ, Heikki , KOIVIKKO, Hannu , LEWANDOWSKI, Jari , MÄNTTÄRI, Mika , MATTILA, Jari
IPC分类号： C13D3/16 , B01D61/00 , B01D61/02 , C13K13/00
CPC分类号： C13B35/08 , B01D61/027 , B01D2315/14 , C13B20/165
摘要： The invention relates to an improved nanofiltration process for separating and recovering components, such as sug ars and sugar alcohols from multicomponent mixtures. The process of the invention is characterized by collecting the nanofiltration retentate/permeate in several fractions with different purity, optional recycling of at least one of the collected nanofiltration retentate/permeate fractions to the nanofiltration and recovering the desired component from the nanofiltration permeate/retentate fractions by dif ferent methods. In one embodiment of the invention, the process comprises a combination of nanofiltration and chromatography.
摘要翻译：本发明涉及用于从多组分混合物中分离和回收组分如糖和糖醇的改进的纳滤方法。本发明的方法的特征在于以不同纯度的几个级分收集纳滤过滤滞留物/渗透物，任选地将收集的纳滤渗余物/渗透物部分中的至少一种再循环到纳滤中，并从纳滤过滤渗透物/渗余物馏分中回收所需组分通过不同的方法。在本发明的一个实施方案中，该方法包括纳滤和层析的组合。

3. 发明申请

WO2005040430A1 SEPARATION OF SUGARS 审中-公开
标题翻译：糖的分离
公开(公告)号：WO2005040430A1
公开(公告)日：2005-05-06
申请号：PCT/FI2004/000557
申请日：2004-09-22
申请人： DANISCO SWEETENERS OY , JUMPPANEN, Juho , RAVANKO, Vili , HEIKKILÄ, Heikki , NURMI, Juha , NURMI, Nina , SAARI, Pia , HÄKKÄ, Katja , LEWANDOWSKI, Jari
发明人： JUMPPANEN, Juho , RAVANKO, Vili , HEIKKILÄ, Heikki , NURMI, Juha , NURMI, Nina , SAARI, Pia , HÄKKÄ, Katja , LEWANDOWSKI, Jari
IPC分类号： C13K13/00
CPC分类号： C13B20/142 , C13K13/00
摘要： The invention relates to the recovery of deoxy sugars, such as fucose from biomass-derived solutions, such as spent liquors obtained from pulping processes. The invention also relates to the recovery of glycosides from biomass. The invention is based on the use of chromatographic fractionation with specific column packing materials and combinations thereof using water as the eluent. The deoxy sugar product obtained from the chromatographic fractionation may be further purified by crystallization. The invention also provides a novel crystalline L-fucose product and a novel process for the crystallization of fucose.
摘要翻译：本发明涉及从生物质衍生的溶液中回收脱氧糖，例如岩藻糖，例如从制浆方法获得的废液。本发明还涉及从生物质中回收糖苷。本发明基于使用具有特定柱填充材料的色谱分离和使用水作为洗脱液的组合。从色谱分离得到的脱氧糖产品可通过结晶进一步纯化。本发明还提供了一种新型的结晶L-岩藻糖产物和岩藻糖结晶的新方法。

4. 发明申请

WO2002022228A3 METHOD FOR FRACTIONATING LIQUID MIXTURES 审中-公开
公开(公告)号：WO2002022228A3
公开(公告)日：2002-03-21
申请号：PCT/EP2001/010035
申请日：2001-08-30
申请人： DANISCO SWEETENERS OY , HEIKKILÄ, Heikki , KUISMA, Jarmo , LEWANDOWSKI, Jari , PAANANEN, Hannu , RAVANKO, Vili , RINNE, Jukka
发明人： HEIKKILÄ, Heikki , KUISMA, Jarmo , LEWANDOWSKI, Jari , PAANANEN, Hannu , RAVANKO, Vili , RINNE, Jukka
IPC分类号： B01D15/02
摘要： The present invention relates to a method of fractionating liquid mixtures or solutions, comprising the steps of subjecting a feed in the form of a liquid mixture or solution to a first chromatographic separation, thereby recovering at least a fraction (A) and a fraction (B) both containing a first component or product, subjecting a mixture or solution derived from or comprising said fraction (A) to a second chromatographic separation, thereby recovering at least a fraction (C) rich in said first component or product and subjecting a mixture or solution derived from or comprising said fraction (B) to a third chromatographic separation, thereby recovering at least a fraction (D) also rich in said first component or product, and whereby at least two fractions are recovered from the second and third chromatographic separations.

5. 发明申请

WO0222228A2 METHOD FOR FRACTIONATING LIQUID MIXTURES 审中-公开
标题翻译：分离液体混合物的方法
公开(公告)号：WO0222228A2
公开(公告)日：2002-03-21
申请号：PCT/EP0110035
申请日：2001-08-30
申请人： XYROFIN OY , HEIKKILAE HEIKKI , KUISMA JARMO , LEWANDOWSKI JARI , PAANANEN HANNU , RAVANKO VILI , RINNE JUKKA
发明人： HEIKKILAE HEIKKI , KUISMA JARMO , LEWANDOWSKI JARI , PAANANEN HANNU , RAVANKO VILI , RINNE JUKKA
IPC分类号： B01D15/18 , G01N30/82 , B01D15/08
CPC分类号： G01N30/82 , B01D15/1821
摘要： The present invention relates to a method of fractionating liquid mixtures or solutions, comprising the steps of subjecting a feed in the form of a liquid mixture or solution to a first chromatographic separation, thereby recovering at least a fraction (A) and a fraction (B) both containing a first component or product, subjecting a mixture or solution derived from or comprising said fraction (A) to a second chromatographic separation, thereby recovering at least a fraction (C) rich in said first component or product and subjecting a mixture or solution derived from or comprising said fraction (B) to a third chromatographic separation, thereby recovering at least a fraction (D) also rich in said first component or product, and whereby at least two fractions are recovered from the second and third chromatographic separations.
摘要翻译：本发明涉及一种分离液体混合物或溶液的方法，包括以液体混合物或溶液形式的进料进行第一次色谱分离，从而回收至少一个馏分（A）和馏分（B ），其含有第一组分或产物，使来自或包含所述级分（A）的混合物或溶液进行第二层析分离，从而回收至少一种富含所述第一组分或产物的级分（C），并使混合物或衍生自或包含所述级分（B）的溶液进行第三色谱分离，由此回收至少一种还富含所述第一组分或产物的级分（D），并且从第二和第三色谱分离中回收至少两个级分。

6. 发明申请

WO2010097511A1 SEPARATION PROCESS 审中-公开
标题翻译：分离过程
公开(公告)号：WO2010097511A1
公开(公告)日：2010-09-02
申请号：PCT/FI2010/050127
申请日：2010-02-24
申请人： DANISCO A/S , AIRAKSINEN, Jyrki , HEIKKILÄ, Heikki , LEWANDOWSKI, Jari , LAIHO, Kari
发明人： AIRAKSINEN, Jyrki , HEIKKILÄ, Heikki , LEWANDOWSKI, Jari , LAIHO, Kari
IPC分类号： B01D15/10 , B01D15/18 , C13D3/14
CPC分类号： C13B20/14 , B01D15/185 , B01D15/362 , B01D15/363 , C07H1/06 , C13K13/00
摘要： The present invention relates to a chromatographic separation process for fractionating betaine-containing solutions by utilizing fractions comprising parts of the separation profile as a substituent of the eluent in a novel and inventive manner. The process provides improved separation capacity and separation efficiency without affecting the yield or purity of betaine or other products. The process can especially be applied to sequential SMB separation systems.
摘要翻译：本发明涉及一种色谱分离方法，用于通过以新颖和创新的方式利用包含部分分离分布作为洗脱液的取代基的级分来分馏含甜菜碱的溶液。该方法提供了改善的分离能力和分离效率，而不影响甜菜碱或其他产品的产率或纯度。该过程可以特别适用于连续的SMB分离系统。

7. 发明申请

WO2010097510A1 SEPARATION PROCESS 审中-公开
标题翻译：分离过程
公开(公告)号：WO2010097510A1
公开(公告)日：2010-09-02
申请号：PCT/FI2010/050126
申请日：2010-02-24
申请人： DANISCO A/S , AIRAKSINEN, Jyrki , HEIKKILÄ, Heikki , LEWANDOWSKI, Jari , LAIHO, Kari , SARMALA, Päivi
发明人： AIRAKSINEN, Jyrki , HEIKKILÄ, Heikki , LEWANDOWSKI, Jari , LAIHO, Kari , SARMALA, Päivi
IPC分类号： B01D15/10 , B01D15/18 , C13D3/14
CPC分类号： C13B20/14 , B01D15/185 , B01D15/362 , B01D15/363 , C07H1/06 , C13K13/00
摘要： The present invention relates to a chromatographic separation process for fractionating solutions containing sugars, sugar alcohols, sugar acids and/or betaine by utilizing fractions comprising parts of the separation profile as a substituent of the eluent in a novel and inventive manner. The starting solutions are typically multicomponent plant- based extracts and hydrolysates, stillages, and fermentation products and derivatives thereof. The process provides improved separation capacity and separation efficiency without affecting the yield or purity of product components, such as sugars, sugar alcohols, sugar acids, and betaine. The process can especially be applied to sequential SMB separation systems.
摘要翻译：本发明涉及一种色谱分离方法，其通过以新颖和创造性方式利用包含部分分离分布作为洗脱液的取代基的级分来分馏含有糖，糖醇，糖酸和/或甜菜碱的溶液。起始溶液通常是多组分植物为基础的提取物和水解产物，水解产物及其发酵产物及其衍生物。该方法提供了提高的分离能力和分离效率，而不影响产物组分如糖，糖醇，糖酸和甜菜碱的产率或纯度。该过程可以特别适用于连续的SMB分离系统。

8. 发明申请

WO2009155982A1 PROCESS FOR SEPARATION OF CA- OR MG-SULFITE SPENT LIQUOR TO YIELD CRYSTALLINE XYLOSE 审中-公开
标题翻译：将CA-或MG-硫酸酯液体分离成晶体晶体的方法
公开(公告)号：WO2009155982A1
公开(公告)日：2009-12-30
申请号：PCT/EP2008/058172
申请日：2008-06-26
申请人： DANISCO A/S , HEIKKILÄ, Heikki , LEWANDOWSKI, Jari
发明人： HEIKKILÄ, Heikki , LEWANDOWSKI, Jari
IPC分类号： C13D3/14 , C13K13/00 , C13J1/06 , B01D15/36 , B01D15/38 , B01J39/04 , B01J39/26 , C08H5/02
CPC分类号： C13K13/002 , B01D15/362 , C08H6/00 , C13B20/144 , C13B35/06
摘要： A process for the separation of a xylose-containing, lignosulphonate-containing Ca-sulfite spent liquor is provided. The process comprises a first step of : (A) chromatographic separation of the Ca- or Mg-sulfite spent liquor using a single pass through a batch- type long resin bed chromatography column having a strong acid cation exchange resin as a separation medium. The ratio of the bed length: mean resin bead diameter of the column is 10,000- 40,000. This step yields •a first xylose-rich fraction having a xylose content 50- 70 wt. % based on dry solids and • a lignosulphonate-rich fraction. The process further comprises a step of : (B) crystallizing xylose from the first xylose rich fraction by using a crystallization method comprising (i) boiling crystallization; (ii) cooling crystallization or (iii) a combination of (i) and (ii) to obtain a first batch of crystalline xylose and a first xylose run-off. The process provides a simplification of existing methods, and at the same time allows advantages such as improved xylose yield and improved xylose purity.
摘要翻译：提供了一种用于分离含木糖的含木质素磺酸盐的亚硫酸钙废液的方法。该方法包括以下步骤：（A）使用单次通过具有强酸性阳离子交换树脂作为分离介质的间歇型长树脂床色谱柱对Ca-或Mg-亚硫酸盐废液进行色谱分离。床长的比例：柱的平均树脂珠粒直径为10,000-40,000。该步骤产生具有木糖含量为50-70重量％的第一富含木糖的级分。基于干固体和富含木素磺酸盐的级分。该方法还包括以下步骤：（B）通过使用包含（i）沸腾结晶的结晶方法从第一富含木糖的级分结晶木糖; （ii）冷却结晶或（iii）（i）和（ii）的组合以获得第一批结晶木糖和第一木糖流出物。该方法提供了现有方法的简化，并且同时可以获得诸如改善木糖产量和改善木糖纯度的优点。

9. 发明申请

WO2005042788A1 SEPARATION PROCESS 审中-公开
标题翻译：分离过程
公开(公告)号：WO2005042788A1
公开(公告)日：2005-05-12
申请号：PCT/FI2004/000641
申请日：2004-10-29
申请人： DANISCO SWEETENERS OY , HEIKKILÄ, Heikki , KOIVIKKO, Hannu , NURMI, Juha , MATTILA, Jari , SAARI, Pia , NURMI, Nina , SARMALA, Päivi , LINDROOS, Mirja , LEWANDOWSKI, Jari
发明人： HEIKKILÄ, Heikki , KOIVIKKO, Hannu , NURMI, Juha , MATTILA, Jari , SAARI, Pia , NURMI, Nina , SARMALA, Päivi , LINDROOS, Mirja , LEWANDOWSKI, Jari
IPC分类号： C13K13/00
CPC分类号： C07H1/08 , C13K13/00 , C13K13/007
摘要： The invention relates to a process of recovering arabinose and optionally other monosaccharides from vegetable fiber rich in heteropolymeric arabinose, such as gum arabic. Said other monosaccharides are typically selected from galactose and rhamnose. The process of the invention comprises controlled hydrolysis of the arabinose-rich vegetable fiber and fractionation of the hydrolysis product to obtain a fraction enriched in arabinose and optionally other product fractions followed by crystallization of arabinose. The invention also relates to a novel method of crystallizing arabinose from biomass-derived material. Furthermore, the invention relates to novel crystalline L-arabinose.
摘要翻译：本发明涉及从富含异聚阿拉伯糖的植物纤维如阿拉伯树胶中回收阿拉伯糖和任选的其它单糖的方法。所述其它单糖通常选自半乳糖和鼠李糖。本发明的方法包括控制富含阿拉伯糖的植物纤维的水解和水解产物的分级，以获得富含阿拉伯糖和任选的其它产物级分的级分，然后结晶阿拉伯糖。本发明还涉及从生物质衍生的材料中结晶阿拉伯糖的新方法。此外，本发明涉及新的结晶L-阿拉伯糖。

10. 发明申请

WO2004060526A1 DISTRIBUTING OR COLLECTING DEVICE 审中-公开
标题翻译：分销或收集设备
公开(公告)号：WO2004060526A1
公开(公告)日：2004-07-22
申请号：PCT/FI2003/000989
申请日：2003-12-30
申请人： FINNFEEDS FINLAND OY , PAANANEN, Hannu , HEIKKILÄ, Heikki , LEWANDOWSKI, Jari , VARTEVA, Esko
发明人： PAANANEN, Hannu , HEIKKILÄ, Heikki , LEWANDOWSKI, Jari , VARTEVA, Esko
IPC分类号： B01D15/08
CPC分类号： B01D15/14 , G01N30/6017
摘要： The present invention relates to a fluid distributing device for distributing fluid into a column and to a fluid collecting device for collecting fluid from a column. The invention relates also to methods of using the devices of the present invention. The distributing device and/or the collecting device of the present invention can be used in fixed or fluidized bed reactors or columns, such as chromatographic separation columns, ion exchange columns, adsorption columns etc. A fluid distributing device comprises a) a first fluid conveying system; and b) a distributing plate, which comprises i) first means for fluid transfer for dividing the fluid flow coming from the delivering points into several partial fluid flows and for distributing the partial fluid flows into the column; and ii) first means for controlling of the partial fluid flows by differential pressure in the first means for fluid transfer.
摘要翻译：本发明涉及用于将流体分配到塔中的流体分配装置和用于从塔收集流体的流体收集装置。本发明还涉及使用本发明的装置的方法。本发明的分配装置和/或收集装置可用于固定或流化床反应器或色谱柱，例如色谱分离柱，离子交换柱，吸附柱等。流体分配装置包括：a）第一流体输送系统; 和b）分配板，其包括i）用于流体转移的第一装置，用于将来自所述输送点的流体流分成几个部分流体流，并将所述部分流体流分配到所述塔中; 以及ii）第一装置，用于在第一流体传递装置中通过差压来控制部分流体流动。

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