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1. 发明申请

WO2012092006A3 HYDROPROCESSING CATALYSTS AND METHODS FOR MAKING THEREOF 审中-公开
标题翻译：氢化催化剂及其制备方法
公开(公告)号：WO2012092006A3
公开(公告)日：2013-01-17
申请号：PCT/US2011066016
申请日：2011-12-20
申请人： CHEVRON USA INC , KUPERMAN ALEXANDER E , BRAIT AXEL , KOU BO , REYNOLDS BRUCE EDWARD , DUNCKLEY CHRISTOPHER PAUL , MARIS ERIN P , NGUYEN JOSEPH V , CHABOT JULIE , KWIK KENNETH , JIAO LING , MIRONOV OLEG , BHADURI RAHUL SHANKAR , YANG SHUWU , KOTUN MODINAT
发明人： KUPERMAN ALEXANDER E , BRAIT AXEL , KOU BO , REYNOLDS BRUCE EDWARD , DUNCKLEY CHRISTOPHER PAUL , MARIS ERIN P , NGUYEN JOSEPH V , CHABOT JULIE , KWIK KENNETH , JIAO LING , MIRONOV OLEG , BHADURI RAHUL SHANKAR , YANG SHUWU , KOTUN MODINAT
IPC分类号： B01J23/28 , B01J19/24 , B01J23/30 , B01J23/755 , B01J35/10
CPC分类号： B01J23/883 , B01J23/24 , B01J23/85 , B01J23/8872 , B01J23/8873 , B01J27/051 , B01J27/0515 , B01J35/0073 , B01J35/1019 , B01J35/1023 , B01J35/1042 , B01J35/1047 , B01J35/1095 , B01J37/20 , C10G49/04 , C10G49/06 , C10G49/12 , C10G2300/107 , C10G2300/1077 , C10G2300/205 , C10G2300/301 , C10G2300/701 , C10G2300/703 , C10G2300/802
摘要： A process for preparing a slurry catalyst for the heavy oil upgrade is provided. The slurry catalyst has a BET total surface area of at least 100 m2/g, a total pore volume of at least 0.5 cc/g and a polymodal pore distribution with at least 80% of pore sizes from 5 to 2,000 Angstroms. In one embodiment, a polar aprotic solvent is mixed with the metal precursor feed to form an oil-dispersible precursor. In another embodiment, the precursor feedstock is selected from any of a pressure leach solution from metal recovery, a rework material, a double metal salt precursor, a single metal precursor. In one embodiment, high shear mixing is employed to generate an emulsion. In another embodiment, sulfiding is carried out at least twice for enhanced sulfiding. In another embodiment, at least a metal precursor feedstock is split into portions for addition in various stages of the process.
摘要翻译：提供了一种制备用于重油升级的浆料催化剂的方法。浆料催化剂的BET总表面积为至少100m 2 / g，总孔体积至少为0.5cc / g，多孔模数孔隙分布为至少80％孔径从5至2000埃。在一个实施方案中，将极性非质子溶剂与金属前体进料混合以形成油分散性前体。在另一个实施方案中，前体原料选自金属回收的压力浸出溶液，返修材料，双金属盐前体，单一金属前体中的任何一种。在一个实施方案中，采用高剪切混合来产生乳液。在另一个实施方案中，硫化进行至少两次以增强硫化。在另一个实施方案中，至少金属前体原料被分成用于在该方法的各个阶段中添加的部分。

2. 发明申请

WO2010033487A3 SYSTEMS AND METHODS FOR PRODUCING A CRUDE PRODUCT 审中-公开
标题翻译：用于生产原料产品的系统和方法
公开(公告)号：WO2010033487A3
公开(公告)日：2010-07-01
申请号：PCT/US2009056932
申请日：2009-09-15
申请人： CHEVRON USA INC , FARSHID DARUSH , REYNOLDS BRUCE , CHABOT JULIE , KOU BO , BRENNAN VIVION ANDREW , MARIS ERIN , YANG SHUWU , BISWAS GOUTAM , CHEN KAIDONG , NGUYEN JOSEPH V , BRAIT AXEL , BHADURI RAHUL S , KUPERMAN ALEXANDER E
发明人： FARSHID DARUSH , REYNOLDS BRUCE , CHABOT JULIE , KOU BO , BRENNAN VIVION ANDREW , MARIS ERIN , YANG SHUWU , BISWAS GOUTAM , CHEN KAIDONG , NGUYEN JOSEPH V , BRAIT AXEL , BHADURI RAHUL S , KUPERMAN ALEXANDER E
IPC分类号： C10G65/02 , C10G45/02
CPC分类号： C10G65/10 , C10G65/00 , C10G65/12 , C10G65/18 , C10G2300/1044 , C10G2300/107 , C10G2300/1074 , C10G2300/1077 , C10G2300/202 , C10G2300/203 , C10G2300/205 , C10G2300/206 , C10G2300/208 , C10G2300/302 , C10G2300/308 , C10G2300/4018 , C10G2300/44 , C10G2300/80 , C10G2300/805 , C10G2300/807 , C10G2400/02 , C10G2400/04 , C10G2400/08 , C10G2400/28
摘要： A flexible once-through process for hydroprocessing heavy oil feedstock is disclosed. The process employs a plurality of contacting zones and at least a separation zone to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products. The contacting zones operate under hydrocracking conditions, employing a slurry catalyst which comprises an active metal catalyst having an average particle size of at least 1 micron in a hydrocarbon oil diluent, at a concentration of greater than 500 wppm of active metal catalyst to heavy oil feedstock. The plurality of contacting zones and separation zones are configured in a permutable fashion allowing the once-through process to be flexible operating in various modes: a sequential mode; a parallel mode; a combination of parallel and sequential mode; all online; some online and some on stand-by; some online and some off-line; a parallel mode with the effluent stream from the contacting zone being sent to at least a separation zone in series with the contacting zone; a parallel mode with the effluent stream from the contacting zone being combined with an effluent stream from at least another contacting zone and sent to the separation zone; and combinations thereof. In one embodiment, the effluent from a contacting zone is sent to the next contacting zone in series for further upgrade, with the next contacting zone having a pressure drop of at most 100 psi, with the pressure drop is not due to a pressure reducing device as in the prior art. In one embodiment, at least an additive material selected from inhibitor additives, anti-foam agents, stabilizers, metal scavengers, metal contaminant removers, metal passivators, and sacrificial materials, in an amount of less than 1 wt. % of the heavy oil feedstock, is added to at least one of the contacting zones.
摘要翻译：公开了用于加氢处理重油原料的灵活的一次通过工艺。该方法采用多个接触区和至少一个分离区将至少一部分重油原料转化为较低沸点的烃，形成升级产物。接触区在加氢裂化条件下操作，使用浆状催化剂，其包含活性金属催化剂与重油原料的浓度大于500wppm的烃油稀释剂中平均粒度至少1微米的活性金属催化剂。多个接触区域和分离区域以可置换的方式配置，允许直通过程灵活地以各种模式操作：顺序模式; 并行模式; 并行和顺序模式的组合; 全部在线; 一些在线和一些待命; 一些在线和一些离线; 与来自接触区的流出物流平行的方式被送至与接触区串联的至少一个分离区; 与来自接触区的流出物流平行的方式与来自至少另一个接触区的流出物流合并并送至分离区; 以及它们的组合。在一个实施方案中，来自接触区的流出物串联送入下一个接触区用于进一步升级，其中下一个接触区具有至多100psi的压降，其中压降不是由于减压装置如在现有技术中那样。在一个实施方案中，至少选自抑制剂添加剂，消泡剂，稳定剂，金属清除剂，金属污染物去除剂，金属钝化剂和牺牲材料的添加剂材料的量小于1wt。将重油原料的％重量添加到至少一个接触区中。

3. 发明申请

WO2010033487A2 SYSTEMS AND METHODS FOR PRODUCING A CRUDE PRODUCT 审中-公开
公开(公告)号：WO2010033487A2
公开(公告)日：2010-03-25
申请号：PCT/US2009056932
申请日：2009-09-15
申请人： CHEVRON USA INC , FARSHID DARUSH , REYNOLDS BRUCE , CHABOT JULIE , KOU BO , BRENNAN VIVION ANDREW , MARIS ERIN , YANG SHUWU , BISWAS GOUTAM , CHEN KAIDONG , NGUYEN JOSEPH V , BRAIT AXEL , BHADURI RAHUL S , KUPERMAN ALEXANDER E
发明人： FARSHID DARUSH , REYNOLDS BRUCE , CHABOT JULIE , KOU BO , BRENNAN VIVION ANDREW , MARIS ERIN , YANG SHUWU , BISWAS GOUTAM , CHEN KAIDONG , NGUYEN JOSEPH V , BRAIT AXEL , BHADURI RAHUL S , KUPERMAN ALEXANDER E
IPC分类号： C10G65/02 , C10G45/02
CPC分类号： C10G65/10 , C10G65/00 , C10G65/12 , C10G65/18 , C10G2300/1044 , C10G2300/107 , C10G2300/1074 , C10G2300/1077 , C10G2300/202 , C10G2300/203 , C10G2300/205 , C10G2300/206 , C10G2300/208 , C10G2300/302 , C10G2300/308 , C10G2300/4018 , C10G2300/44 , C10G2300/80 , C10G2300/805 , C10G2300/807 , C10G2400/02 , C10G2400/04 , C10G2400/08 , C10G2400/28
摘要： A flexible once-through process for hydroprocessing heavy oil feedstock is disclosed. The process employs a plurality of contacting zones and at least a separation zone to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products. The contacting zones operate under hydrocracking conditions, employing a slurry catalyst which comprises an active metal catalyst having an average particle size of at least 1 micron in a hydrocarbon oil diluent, at a concentration of greater than 500 wppm of active metal catalyst to heavy oil feedstock. The plurality of contacting zones and separation zones are configured in a permutable fashion allowing the once-through process to be flexible operating in various modes: a sequential mode; a parallel mode; a combination of parallel and sequential mode; all online; some online and some on stand-by; some online and some off-line; a parallel mode with the effluent stream from the contacting zone being sent to at least a separation zone in series with the contacting zone; a parallel mode with the effluent stream from the contacting zone being combined with an effluent stream from at least another contacting zone and sent to the separation zone; and combinations thereof. In one embodiment, the effluent from a contacting zone is sent to the next contacting zone in series for further upgrade, with the next contacting zone having a pressure drop of at most 100 psi, with the pressure drop is not due to a pressure reducing device as in the prior art. In one embodiment, at least an additive material selected from inhibitor additives, anti-foam agents, stabilizers, metal scavengers, metal contaminant removers, metal passivators, and sacrificial materials, in an amount of less than 1 wt. % of the heavy oil feedstock, is added to at least one of the contacting zones.

4. 发明申请

WO2010033487A9 SYSTEMS AND METHODS FOR PRODUCING A CRUDE PRODUCT 审中-公开
标题翻译：用于生产原料产品的系统和方法
公开(公告)号：WO2010033487A9
公开(公告)日：2010-09-16
申请号：PCT/US2009056932
申请日：2009-09-15
申请人： CHEVRON USA INC , FARSHID DARUSH , REYNOLDS BRUCE , CHABOT JULIE , KOU BO , BRENNAN VIVION ANDREW , MARIS ERIN , YANG SHUWU , BISWAS GOUTAM , CHEN KAIDONG , NGUYEN JOSEPH V , BRAIT AXEL , BHADURI RAHUL S , KUPERMAN ALEXANDER E
发明人： FARSHID DARUSH , REYNOLDS BRUCE , CHABOT JULIE , KOU BO , BRENNAN VIVION ANDREW , MARIS ERIN , YANG SHUWU , BISWAS GOUTAM , CHEN KAIDONG , NGUYEN JOSEPH V , BRAIT AXEL , BHADURI RAHUL S , KUPERMAN ALEXANDER E
IPC分类号： C10G65/02 , C10G45/02
CPC分类号： C10G65/10 , C10G65/00 , C10G65/12 , C10G65/18 , C10G2300/1044 , C10G2300/107 , C10G2300/1074 , C10G2300/1077 , C10G2300/202 , C10G2300/203 , C10G2300/205 , C10G2300/206 , C10G2300/208 , C10G2300/302 , C10G2300/308 , C10G2300/4018 , C10G2300/44 , C10G2300/80 , C10G2300/805 , C10G2300/807 , C10G2400/02 , C10G2400/04 , C10G2400/08 , C10G2400/28
摘要： A flexible once-through process for hydroprocessing heavy oil feedstock is disclosed. The process employs a plurality of contacting zones and at least a separation zone to convert at least a portion of the heavy oil feedstock to lower boiling hydrocarbons, forming upgraded products. The contacting zones operate under hydrocracking conditions, employing a slurry catalyst which comprises an active metal catalyst having an average particle size of at least 1 micron in a hydrocarbon oil diluent, at a concentration of greater than 500 wppm of active metal catalyst to heavy oil feedstock. The plurality of contacting zones and separation zones are configured in a permutable fashion allowing the once-through process to be flexible operating in various modes: a sequential mode; a parallel mode; a combination of parallel and sequential mode; all online; some online and some on stand-by; some online and some off-line; a parallel mode with the effluent stream from the contacting zone being sent to at least a separation zone in series with the contacting zone; a parallel mode with the effluent stream from the contacting zone being combined with an effluent stream from at least another contacting zone and sent to the separation zone; and combinations thereof. In one embodiment, the effluent from a contacting zone is sent to the next contacting zone in series for further upgrade, with the next contacting zone having a pressure drop of at most 100 psi, with the pressure drop is not due to a pressure reducing device as in the prior art. In one embodiment, at least an additive material selected from inhibitor additives, anti-foam agents, stabilizers, metal scavengers, metal contaminant removers, metal passivators, and sacrificial materials, in an amount of less than 1 wt. % of the heavy oil feedstock, is added to at least one of the contacting zones.
摘要翻译：公开了用于加氢处理重油原料的灵活的一次性方法。该方法采用多个接触区和至少一个分离区，将至少一部分重油原料转化成低沸点烃，形成升级产物。接触区在加氢裂化条件下操作，使用浆料催化剂，其在烃油稀释剂中包含平均粒度至少为1微米的活性金属催化剂，其浓度大于500wppm的活性金属催化剂与重油原料。多个接触区域和分离区域被配置成可替换的方式，使得直通过程能够以各种模式灵活地操作：顺序模式; 并行模式; 并行和顺序模式的组合; 所有在线一些在线和一些待机; 一些在线和一些离线; 与来自接触区的流出物流的并行模式被传送到与接触区串联的至少一个分离区; 来自接触区域的流出物流与来自至少另一个接触区域的流出物流的并行模式组合并被送至分离区域; 及其组合。在一个实施方案中，将来自接触区域的流出物串联送入下一个接触区域以进一步升级，下一个接触区域的压力降至多为100psi，压降不是由于减压装置如现有技术中那样。在一个实施方案中，至少一种选自抑制剂添加剂，消泡剂，稳定剂，金属清除剂，金属污染物去除剂，金属钝化剂和牺牲材料的添加剂材料的量小于1wt。％的重油原料加入到至少一个接触区中。

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