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1. 发明申请

WO2004081149A3 SELECTIVE HYDROGENATION OF ACETYLENES AND DIENES IN A HYDROCARBON STREAM 审中-公开
标题翻译：乙烯和二氧化碳在氢气流中的选择性加氢
公开(公告)号：WO2004081149A3
公开(公告)日：2005-01-13
申请号：PCT/US2004006535
申请日：2004-03-04
申请人： CATALYTIC DISTILLATION TECH
发明人： GELBEIN ABRAHAM P , SMITH LAWRENCE A JR
IPC分类号： C07C5/05 , C07C5/09 , C07C7/163 , C07C7/167 , C07C5/03
CPC分类号： C07C5/09 , C07C5/05 , C07C7/163 , C07C7/167 , C07C2523/44
摘要： Acetylenes and dienes in a stream containing hydrogen, methane, C2-C6 olefins and paraffins, C2-C6 acetylenes and dienes, benzene, toluene, xylenes, and other C6+ components are hydrogenated in a downflow boiling point reactor wherein the heat of reaction is absorbed by the liquid in the reactor which produces a vapor. Besides the feed to the reactor there is a recirculating stream which is fed at a rate sufficient to ensure that the catalyst particles within the reactor are wetted. A third stream, which is taken from a downstream distillation column, is fed to provide the make up mass corresponding to the mass evaporated in the reactor. The composition of the this third stream controls the steady state composition of the liquid flowing through the reactor.
摘要翻译：在含有氢，甲烷，C 2 -C 6烯烃和链烷烃，C 2 -C 6炔烃和二烯，苯，甲苯，二甲苯和其它C 6+组分的物流中的乙炔和二烯在其中反应热被吸收的下流沸点反应器中氢化通过反应器中产生蒸汽的液体。除了进料到反应器之外还有一个再循环流，其进料量足以确保反应器内的催化剂颗粒被润湿。进料从下游蒸馏塔获得的第三料流，以提供与在反应器中蒸发的物质相应的补充质量。该第三流的组成控制流过反应器的液体的稳态组成。

2. 发明申请

WO2007061480A3 PROCESS FOR MAKING DIARYL CARBONATE 审中-公开
标题翻译：制备二氧化碳的方法
公开(公告)号：WO2007061480A3
公开(公告)日：2007-11-01
申请号：PCT/US2006033882
申请日：2006-08-30
申请人： CATALYTIC DISTILLATION TECH
发明人： GELBEIN ABRAHAM P , RYU J YONG
IPC分类号： C07C69/96
CPC分类号： C07C68/06 , C07C68/08 , C07C69/96
摘要： Diphenyl carbonate is produced by reacting phenol with diethyl carbonate in a series of fixed bed reactors each of which is connected at different position on a distillation column via side draw and return streams. The composition of material in a distillation column varies along the length of the column, which is predictable under a given set of conditions of temperature and pressure, thus withdrawing streams at different stages in the column, allows the reactor receiving the feed from a particular stage to be operated under conditions to maximize the desired reaction, while allowing the unreacted or byproduct to go back into the distillation and be sent to a stage (by the equilibrium of the distillation) where they are favorably treated in a reactor.
摘要翻译：碳酸二苯酯是通过在一系列固定床反应器中使苯酚与碳酸二乙酯反应制备的，每个固定床反应器通过侧馏分和回流在蒸馏塔上的不同位置连接。蒸馏塔中材料的组成随着柱长度而变化，这在一定温度和压力条件下是可预测的，因此在塔中的不同阶段取出料流，允许反应器从特定阶段接收进料在使所需反应最大化的条件下运行，同时使未反应或副产物回到蒸馏中并送入阶段（通过蒸馏的平衡），在反应器中有利地处理它们。

3. 发明申请

WO2006110201A3 METHOD OF OPERATING DOWNFLOW BOILING POINT REACTORS IN THE SELECTIVE HYDROGENATION OF ACETYLENES AND DIENES 审中-公开
标题翻译：在乙烯和二氧化碳的选择性加氢中操作下游沸点沸点反应器的方法
公开(公告)号：WO2006110201A3
公开(公告)日：2007-11-01
申请号：PCT/US2006003083
申请日：2006-01-30
申请人： CATALYTIC DISTILLATION TECH
发明人： SMITH LAWRENCE A , GELBEIN ABRAHAM P
IPC分类号： C07C7/167
CPC分类号： C07C7/167 , C07C7/163 , C10G45/34 , C10G49/002
摘要： Acetylenes and dienes in a stream containing hydrogen, methane, C 2 -C 6 olefins and paraffins, C 2 -C 6 acetylenes and dienes, benzene, toluene, xylenes, and other C 6 + components are hydrogenated in a downflow boiling point reactor wherein the heat of reaction is absorbed by the liquid in the reactor which produces a vapor. Besides the feed to the reactor there is a recirculating stream which is fed at a rate sufficient to ensure that the catalyst particles within the reactor are wetted. A third stream, which is provided from a second downstream liquid/vapor separator from partially condensed vapor from the first downstream liquid/vapor separator corresponding to the mass evaporated in the reactor, is fed to the reactor. The composition of the third stream controls the steady state composition of the liquid flowing through the reactor.
摘要翻译：含有氢，甲烷，C 2 -C 6烯烃和链烷烃，C 2 -C 6烯烃的物流中的乙炔和二烯，乙炔和二烯，苯，甲苯，二甲苯和其它C 6+组分在下流沸点反应器中氢化，其中反应热被反应器中的液体吸收，产生汽。除了进料到反应器之外还有一个再循环流，其进料量足以确保反应器内的催化剂颗粒被润湿。从第二下游液体/蒸汽分离器提供的第三流体，其与来自在反应器中蒸发的物质相对应的来自第一下游液体/蒸气分离器的部分冷凝的蒸气供给到反应器。第三流的组成控制流过反应器的液体的稳态组成。

4. 发明申请

WO2004016342A3 CONTACT STRUCTURES 审中-公开
标题翻译：接触结构
公开(公告)号：WO2004016342A3
公开(公告)日：2005-02-24
申请号：PCT/US0323132
申请日：2003-07-24
申请人： CATALYTIC DISTILLATION TECH
发明人： SMITH LAWRENCE A JR , GELBEIN ABRAHAM P , ADAMS JOHN R
IPC分类号： B01D47/00 , B01D53/14 , B01F20060101 , B01F5/06 , B01J8/00 , B01J8/02 , B01J19/24 , B01J19/32 , C10G29/20 , C10G50/00
CPC分类号： B01J19/2495 , B01D3/009 , B01J19/32 , B01J35/04 , B01J2219/00006 , B01J2219/32213 , B01J2219/32227 , B01J2219/32231 , B01J2219/32286 , B01J2219/32289 , B01J2219/32408 , B01J2219/32416 , B01J2219/32441 , B01J2219/32466 , B01J2219/32483 , B01J2219/32491 , B01J2219/3306 , B01J2219/3322 , C10G29/205 , C10G50/00
摘要： An internal static mixing system (40) such as a disperser of mesh wire or expanded metal co-knit with a multi filament material selected from inert polymers, catalytic polymers, catalytic metals or mixtures in combination with a vertical reactor (10) having a reaction zone and the disperser (40) disposed in said reaction zone (10), particularly for carrying out paraffin alkylation using acid catalyst is disclosed. The wire mesh provides the structural integrity of the system as well as the open space required in reactors for the movement of vapors and liquids though the system. The disperser (40) may be in sheets, bundles or bales or positioned within a frame.
摘要翻译：一种内部静态混合系统（40），例如网状丝网或多孔金属分散机，其与选自惰性聚合物，催化聚合物，催化金属或混合物的多丝材料与具有反应的立式反应器（10）组合公开了设置在所述反应区（10）中的分散器（40），特别是用于使用酸催化剂进行烷烃烷基化。丝网提供了系统的结构完整性以及反应器中通过系统运动蒸汽和液体所需的开放空间。分散器（40）可以是片材，束或捆或者定位在框架内。

5. 发明申请

WO2007086942A2 ISOMERIZATION OF N-HEPTANE IN NAPHTHA CUTS 审中-公开
标题翻译： N-HEPTANE在NAPHTHA CUTS中的异构化
公开(公告)号：WO2007086942A2
公开(公告)日：2007-08-02
申请号：PCT/US2006033883
申请日：2006-08-30
申请人： CATALYTIC DISTILLATION TECH
发明人： BOYER CHRISTOPHER C , GELBEIN ABRAHAM P
IPC分类号： C07C5/13
CPC分类号： C10L1/06 , C07C5/2791 , C07C2523/08 , C07C2523/14 , C07C2523/42 , C07C2523/44 , C07C2523/46 , C07C2523/75 , C07C2523/755 , C10G49/002 , C07C9/16
摘要： A process for the isomerization of normal heptane contained within a naphtha stream, such as a C 6 -C 8 naphtha, in which the naphtha stream is fractionated into a fraction substantially free of normal heptane and a fraction containing normal heptane. The fraction containing normal heptane is contacted with an isomerization catalyst in an isomerization zone operated as a singe pass fixed bed reactor having a single effluent to isomerize a portion of said normal heptane to branched heptane. The effluent is recovered from said isomerization zone and the effluent is fractionated to recover said branched heptane. The unconverted normal heptane is recovered and returned to the isomerization since it can be separated from the branded heptanes by fractionation.
摘要翻译：包含在石脑油流（例如C 6 -C 8）石脑油内的常规庚烷异构化的方法，其中将石脑油流分馏成基本上不含的正庚烷和含有正庚烷的级分。含有正庚烷的馏分与异构化催化剂接触，异构化区域作为具有单一流出物的单通道固定床反应器操作，将一部分所述正庚烷异构化成支化庚烷。从所述异构化区回收流出物，并将流出物分馏以回收所述支化庚烷。未转化的正庚烷被回收并返回到异构化，因为它可以通过分馏从品牌的庚烷中分离出来。

6. 发明申请

WO2006023022A3 ENERGY EFFICIENT METHOD AND APPARATUS FOR EXOTHERMIC REACTIONS 审中-公开
标题翻译：能源有效方法和装置用于灭菌反应
公开(公告)号：WO2006023022A3
公开(公告)日：2007-08-02
申请号：PCT/US2005021456
申请日：2005-06-17
申请人： CATALYTIC DISTILLATION TECH
发明人： JUDZIS ARVIDS JR , GELBEIN ABRAHAM P , ADAMS JOHN R , BOYER CHRISTOPHER C
IPC分类号： B01D3/34 , B01D1/00 , B01D7/00 , C07C7/04
CPC分类号： B01D3/14 , B01D3/007 , B01D3/009 , B01D3/322 , B01D3/4261 , C10G2400/30
摘要： An energy efficient process scheme for a highly exothermic reactiondistillation system in which the reactor is external to the distillation column and the feed to the reactor comprises a mixture of at least one liquid product stream from the distillation column with or without other liquid/vapor reactants. The reactor is operated under adiabatic and boiling point conditions and at a pressure that results in vaporizing a portion of the liquid flow through the reactor due to the heat of reaction. Under these conditions, reaction temperature is controlled by reactor pressure. The pressure (and hence the temperature) is maintained at a sufficiently high level such that the reactor effluent can be efficiently used to provide reboil heat for the distillation column.
摘要翻译：用于高放热反应蒸馏系统的能量有效的方法方案，其中反应器在蒸馏塔外部和反应器的进料包括来自蒸馏塔的至少一种液体产物流与有或没有其它液体/蒸气反应物的混合物。反应器在绝热和沸点条件下运行，并且在由于反应热导致部分液体流过反应器的压力下运行。在这些条件下，反应温度由反应器压力控制。压力（因此温度）保持在足够高的水平，使得反应器流出物可以有效地用于为蒸馏塔提供再沸腾热。

7. 发明申请

WO2007070085A2 PROCESS FOR REGENERATING SPENT SULFURIC ACID 审中-公开
标题翻译：再生硫酸的方法
公开(公告)号：WO2007070085A2
公开(公告)日：2007-06-21
申请号：PCT/US2006018692
申请日：2006-05-16
申请人： CATALYTIC DISTILLATION TECH
发明人： GELBEIN ABRAHAM P , SMITH LAWRENCE A JR
IPC分类号： C01B17/90
CPC分类号： C01B17/905 , C01B17/79 , C01B17/92
摘要： A process for the regeneration of sulfuric acid contaminated with hydrocarbons and water to produce pure concentration acid comprising: contacting sulfuric acid contaminated with hydrocarbons and water with oxygen and elemental sulfur in the presence of a vanadium containing catalyst in a reaction zone, maintaining at least a portion of the acid in the liquid phase, converting hydrocarbon to carbon oxides and water, and converting sulfur and sulfur dioxide to sulfur trioxide, (4) separating the reactor effluent into a vapor stream and a liquid stream and cooling and partially condensing of the vapor stream to concentrate clean acid.
摘要翻译： 1.一种再生被烃和水污染的硫酸以产生纯浓酸的方法，包括：在含钒催化剂存在下，在反应区中使被烃和水污染的硫酸与氧和元素硫接触，至少保持部分酸在液相中，将烃转化成碳氧化物和水，并将硫和二氧化硫转化成三氧化硫，（4）将反应器流出物分离成蒸汽流和液体流并冷却和部分冷凝蒸气小溪浓缩干净的酸。

8. 发明申请

WO2005102986A2 PROCESS FOR MAKING DIALKYL CARBONATES 审中-公开
标题翻译：制备二烷基碳酸酯的方法
公开(公告)号：WO2005102986A2
公开(公告)日：2005-11-03
申请号：PCT/US2005004087
申请日：2005-02-10
申请人： CATALYTIC DISTILLATION TECH
发明人： RYU J YONG , GELBEIN ABRAHAM P
IPC分类号： C07C68/00 , C07C69/96
CPC分类号： C07C68/00 , C07C69/96
摘要： A process for the production of dialkyl carbonates from the reaction of alcohol, for example C1-C3 alcohols, with urea is disclosed wherein the water and ammonium carbamates impurities in the feed are removed in a prereactor. The water is reacted with urea in the feed to produce ammonium carbamate which is decomposed along with the ammonium carbamates originally in the feed to ammonia and carbon dioxide. In addition some of the urea is reacted with the alcohol in the first reactor to produce alkyl carbamate which is a precursor to dialkyl carbonate. Dialkyl carbonates are produced in the second reaction zone. The undesired by-product N-alkyl alkyl carbamates are continuously distilled off from the second reaction zone along with ammonia, alcohol and dialkyl carbonates under the steady state reactor operation. N-alkyl alkyl carbamates can be converted to heterocyclic compounds in a third reaction zone to remove as solids from the system.
摘要翻译：公开了一种由醇（例如C 1 -C 3醇）与脲的反应制备碳酸二烷基酯的方法，其中在预反应器中将进料中的水和氨基甲酸铵杂质除去。水与进料中的尿素反应生成氨基甲酸铵，氨基甲酸铵与原料在氨和二氧化碳中的氨基甲酸铵一起分解。此外，一些尿素与第一反应器中的醇反应以产生作为碳酸二烷基酯的前体的氨基甲酸烷基酯。在第二反应区产生碳酸二烷基酯。在稳态反应器操作下，不需要的副产物N-烷基烷基氨基甲酸酯与第二反应区连同蒸馏出氨，醇和碳酸二烷基酯。 N-烷基烷基氨基甲酸烷基酯可以在第三反应区转化成杂环化合物，以从系统中除去固体。

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