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1. 发明申请

WO2008063731A3 PURIFICATION METHODS AND PURIFIED CONJUGATED POLYMERS 审中-公开
公开(公告)号：WO2008063731A3
公开(公告)日：2008-05-29
申请号：PCT/US2007/077456
申请日：2007-08-31
申请人： CARNEGIE MELLON UNIVERSITY , MCCULLOUGH, Richard, D. , IOVU, Mihaela, C.
发明人： MCCULLOUGH, Richard, D. , IOVU, Mihaela, C.
IPC分类号： H01B1/12 , C08G61/12 , H01L51/00
摘要： Metal complexing agents are used to purify polymers including conducting polymers to provide very low metal content. The process comprises precipitating the polymer in solution into a solvent system comprising the metal complexing agent. Very low levels including undetectable levels of metals such as nickel and magnesium can be achieved. High purity polymers are used in electronics and photovoltaic applications.

2. 发明申请

WO2008028166A1 UNIVERSAL GRIGNARD METATHESIS POLYMERIZATION 审中-公开
标题翻译：通用格氏硬脂酸聚合
公开(公告)号：WO2008028166A1
公开(公告)日：2008-03-06
申请号：PCT/US2007/077461
申请日：2007-08-31
申请人： CARNEGIE MELLON UNIVERSITY , MCCULLOUGH, Richard, D. , IOVU, Mihaela, C. , OSAKA, Itaru
发明人： MCCULLOUGH, Richard, D. , IOVU, Mihaela, C. , OSAKA, Itaru
IPC分类号： C08G61/00 , C07B49/00 , C07F3/02
CPC分类号： C08G61/00 , C07B49/00
摘要： Universal Grignard Metathesis (GRIM) reactions which provide access to conjugated polymers by GRTM methods are disclosed. Furthermore revealed is a method comprising: providing an unsaturated ring compound comprising at least two halogen ring substituents, providing an organomagnesium reagent comprising an organomagnesium component and a metal activation agent, combining the unsaturated ring compound with the reagent to form a second compound by metal-halogen exchange, wherein the metal activation agent activates the metal-halogen exchange, coupling the second compound to itself in an oligomerization or polymerization reaction. Metal activation agent can be lithium chloride. The process is commercially attractive and can be executed in good yields. Polyfluorenes, polypyrroles, and polythiophenes can be prepared for use in OLED, PLED, photovoltaic, transistor, antistatic coatings, and sensor applications.
摘要翻译：公开了通过GRTM方法提供对共轭聚合物的通用格利雅复分解（GRIM）反应。进一步揭示了一种方法，其包括：提供包含至少两个卤素环取代基的不饱和环化合物，提供包含有机镁组分和金属活化剂的有机镁试剂，将不饱和环化合物与试剂结合以通过金属 - 卤素交换，其中金属活化剂活化金属 - 卤素交换，在低聚或聚合反应中将第二化合物偶联到其自身。金属活化剂可以是氯化锂。该方法具有商业上的吸引力，可以以良好的产率进行。聚芴，聚吡咯和聚噻吩可以制备用于OLED，PLED，光伏，晶体管，抗静电涂层和传感器应用。

3. 发明申请

WO2006107740A3 LIVING SYNTHESIS OF CONDUCTING POLYMERS INCLUDING REGIOREGULAR POLYMERS, POLYTHIOPHENES, AND BLOCK COPOLYMERS 审中-公开
公开(公告)号：WO2006107740A3
公开(公告)日：2006-10-12
申请号：PCT/US2006/011840
申请日：2006-03-31
申请人： CARNEGIE MELLON UNIVERSITY , MCCULLOUGH, Richard, D. , IOVU, Mihaela, C. , SHEINA, Elena, E.
发明人： MCCULLOUGH, Richard, D. , IOVU, Mihaela, C. , SHEINA, Elena, E.
IPC分类号： C08G18/64
摘要： Regioregular poly(3-alkylthiophenes) and other polythiophenes can be prepared by living polymerization which have good solubility, processability and environmental stability. The polymerization method can afford regioregular poly(3-alkylthiophenes) in high yields. Kinetic study of polymerization revealed the living character of this process. The molecular weight of ρoly(3-alkylthiophenes) is a function of the molar ratio of the monomer to nickel initiator, and conducting polymers with relatively narrow molecular weight distribution (PDKl.5) are now readily available. Sequential monomer addition resulted in new block copolymers containing different poly(3-alkylthiophene) segments, which further confirms the "livingness" of this system. Other synthetic methods can be used as well to conduct living polymerization. Blends and electronic devices can be prepared.

4. 发明申请

WO2007025189A2 ELECTRICALLY CONDUCTIVE POLYMERS AND CONTROLLED RADICAL POLYMERZATION 审中-公开
标题翻译：电导电聚合物和控制放射性聚合
公开(公告)号：WO2007025189A2
公开(公告)日：2007-03-01
申请号：PCT/US2006/033324
申请日：2006-08-25
申请人： CARNEGIE MELLON UNIVERSITY , MCCULLOUGH, Richard, D. , IOVU, Michael, C.
发明人： MCCULLOUGH, Richard, D. , IOVU, Michael, C.
IPC分类号： H01B1/12 , H01L51/30
CPC分类号： H01L51/0036 , C08F293/005 , C08F2438/03 , C08G61/126 , H01B1/127 , H01L51/0043
摘要： Electrically conductive polymers including block copolymers, polythiophene copolymers, and regioregular polythiophene copolymers, prepared by controlled radical polymerization including RAPT and NMP polymerization methods. Polymers having low metal content can be prepared. Method of synthesizing polythiophene polymers and copolymers using RAFT and NMP polymerization are also provided. Regioregular polythiophenes are preferred. Blends with polythiophenes and non-conducting polymers can be prepared. Applications include PLEDs, sensors, and optoelectronics.
摘要翻译：包括嵌段共聚物，聚噻吩共聚物和区域定向聚噻吩共聚物的导电聚合物，其通过包括RAPT和NMP聚合方法的受控自由基聚合制备。可以制备具有低金属含量的聚合物。还提供了使用RAFT和NMP聚合合成聚噻吩聚合物和共聚物的方法。区域性聚噻吩是优选的。可以制备与聚噻吩和非导电聚合物的共混物。应用包括PLED，传感器和光电子。

5. 发明申请

WO2011057218A2 METAL INK COMPOSITIONS, CONDUCTIVE PATTERNS, METHODS, AND DEVICES 审中-公开
标题翻译：金属墨水组合物，导电图案，方法和装置
公开(公告)号：WO2011057218A2
公开(公告)日：2011-05-12
申请号：PCT/US2010/055874
申请日：2010-11-08
申请人： CARNEGIE MELLON UNIVERSITY , MCCULLOUGH, Richard, D. , BELOT, John, A. , JAVIER, Anna , POTASH, Rebecca
发明人： MCCULLOUGH, Richard, D. , BELOT, John, A. , JAVIER, Anna , POTASH, Rebecca
IPC分类号： C23C18/06
CPC分类号： C23C18/06 , C07F1/005 , C07F9/5045 , C09D11/101 , C09D11/322 , C09D11/52 , C23C18/08 , H05K3/105 , H05K3/125 , H05K2203/121
摘要： Metal complexes adapted to form conductive metal films and lines upon deposition and treatment. The metal complex can be a covalent complex and can comprise a first and second ligand. Low temperature treatment can be used to convert the complex to a metal. The metal films and lines can have low resistivity and work function similar to pure metal. Coinage metals can be used (e.g., Ag, Au, Cu). The ligands can be dative bonding ligands including amines, unsymmetrical amines, and carboxylate ligands. Sulfur complexes can be used. Carboxylate ligands can be used. The complexes can have a high concentration of metal and can be soluble in aromatic hydrocarbon solvent. The ligands can be adapted to volatilize well. Inkjet printing can be carried out. High yields of metal can be achieve with high conductivity.
摘要翻译：适于在沉积和处理时形成导电金属膜和管线的金属络合物。金属络合物可以是共价复合物，并且可以包含第一和第二配体。低温处理可用于将络合物转化为金属。金属膜和管线可以具有与纯金属相似的低电阻率和功函数。可以使用钴矿金属（例如Ag，Au，Cu）。配体可以是配位键配体，包括胺，不对称胺和羧酸盐配体。可以使用硫络合物。可以使用羧酸盐配体。络合物可以具有高浓度的金属，并且可溶于芳族烃溶剂。配体可适应于挥发良好。喷墨打印可以进行。金属的高产量可以实现高导电性。

6. 发明申请

WO2013130450A2 SELF-REDUCING METAL COMPLEX INKS SOLUBLE IN POLAR PROTIC SOLVENTS AND IMPROVED CURING METHODS 审中-公开
标题翻译：自由式金属复合油墨在极性溶剂中的溶解性和改进的固化方法
公开(公告)号：WO2013130450A2
公开(公告)日：2013-09-06
申请号：PCT/US2013/027768
申请日：2013-02-26
申请人： LIQUID X PRINTED METALS, INC. , MCCULLOUGH, Richard, D. , BELOT, John , POTASH, Rebecca , SEFTON, Elizabeth , COX, Christiana
发明人： MCCULLOUGH, Richard, D. , BELOT, John , POTASH, Rebecca , SEFTON, Elizabeth , COX, Christiana
IPC分类号： C09D11/00
CPC分类号： C09D11/52 , C07F1/10 , C09D11/322 , H05K1/092 , H05K1/16 , H05K3/105
摘要： Metal complexes adapted to form metallic conductive films upon deposition and treatment. The complexes can have a high concentration of metal and can be soluble in polar protic solvent including ethanol and water. The metal complex can be a covalent complex and can comprise a first and second ligand. Low temperature treatment can be used to convert the complex to a metal. The metallic conductive film can have low resistivity and work function close to pure metal. Coinage metals can be used (e.g., Ag). The ligands can be dative bonding ligands including amines and carboxylate ligands. The ligands can be adapted to volatilize well. High yields of metal can be achieve with high conductivity.
摘要翻译：适于在沉积和处理时形成金属导电膜的金属络合物。络合物可以具有高浓度的金属，并且可溶于包括乙醇和水在内的极性质子溶剂中。金属络合物可以是共价复合物，并且可以包含第一和第二配体。低温处理可用于将络合物转化为金属。金属导电膜可以具有接近纯金属的低电阻率和功函数。可以使用金银金属（例如Ag）。配体可以是配位键，包括胺和羧酸盐配体。配体可适应于挥发良好。金属的高产量可以实现高导电性。

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