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1. 发明申请

WO2010012672A3 METHOD FOR THE PRODUCTION OF DIAMINES FROM LACTAMS 审中-公开
标题翻译：用于制备二胺关内酰胺
公开(公告)号：WO2010012672A3
公开(公告)日：2010-07-15
申请号：PCT/EP2009059629
申请日：2009-07-27
申请人： BASF SE , ANDERS JOACHIM-THIERRY , STEIN BERND , HAUBNER MARTIN , MELDER JOHANN-PETER , BENISCH CHRISTOPH , HADERLEIN GERD
发明人： ANDERS JOACHIM-THIERRY , STEIN BERND , HAUBNER MARTIN , MELDER JOHANN-PETER , BENISCH CHRISTOPH , HADERLEIN GERD
IPC分类号： C07C209/50 , C07C211/09
CPC分类号： C07C209/50 , C07C211/09
摘要： The invention relates to a method for producing 1,?-diamines by reacting lactams having at least 7 C atoms with hydrogen and ammonia in the presence of a catalyst at temperatures ranging from 20 to 600°C and a pressure ranging from 1 to 500 bar. Said method is characterized in that the catalyst is obtained by reducing a catalyst precursor.
摘要翻译：本发明涉及一种用于为1的制备方法，？ - 通过具有在催化剂的存在下，在20的温度至600℃和1〜500巴的压力下与氢气和氨的至少7个碳原子的内酰胺的反应的二胺，其特征在于在于该催化剂是通过还原催化剂前体获得的。

2. 发明申请

WO2009030649A3 METHOD FOR PRODUCING TEDA DERIVATIVES 审中-公开
标题翻译：制备泰达衍生物的方法
公开(公告)号：WO2009030649A3
公开(公告)日：2009-10-01
申请号：PCT/EP2008061393
申请日：2008-08-29
申请人： BASF SE , CAUWENBERGE GUNTHER VAN , MELDER JOHANN-PETER , ANDERS JOACHIM-THIERRY , BENISCH CHRISTOPH , KLOPSCH RAINER , DAUN GREGOR , DULLY CHRISTIAN , BUSCHHAUS BORIS , BOECKEMEIER HENNING , POX EVELYN
发明人： CAUWENBERGE GUNTHER VAN , MELDER JOHANN-PETER , ANDERS JOACHIM-THIERRY , BENISCH CHRISTOPH , KLOPSCH RAINER , DAUN GREGOR , DULLY CHRISTIAN , BUSCHHAUS BORIS , BOECKEMEIER HENNING , POX EVELYN
IPC分类号： C07D487/08
CPC分类号： C07D487/08
摘要： The invention relates to a method for producing triethylenediamine (TEDA) derivatives, comprising the following steps: a) reaction of a dihydropyrazine with an olefin, b) optionally hydrogenation following step a). The invention also relates to novel TEDA derivatives as such and to the use thereof as built-in polyurethane catalysts.
摘要翻译：制备三亚乙基二胺（TEDA）衍生物的方法本发明涉及制备三亚乙基二胺（TEDA）衍生物的方法，其包括以下步骤：a）二氢吡嗪与烯烃的反应，b）步骤a）后的任选氢化。此外，本发明还涉及新颖的TEDA衍生物本身以及它们作为可安装的聚氨酯催化剂的用途。

3. 发明申请

WO2004013082A3 METHOD FOR PRODUCING AMINOALKOXY BENZYLAMINES AND AMINOALKOXY BENZONITRILES AS INTERMEDIATES 审中-公开
标题翻译：工艺用于生产和AMINOALKOXYBENZYLAMINEN AMINOALKOXYBENZONITRILEN中间产品
公开(公告)号：WO2004013082A3
公开(公告)日：2004-07-15
申请号：PCT/EP0307871
申请日：2003-07-18
申请人： BASF AG , LOEBER OLIVER , BENISCH CHRISTOPH , EBEL KLAUS , MELDER JOHANN-PETER
发明人： LOEBER OLIVER , BENISCH CHRISTOPH , EBEL KLAUS , MELDER JOHANN-PETER
IPC分类号： C07B61/00 , C07C213/02 , C07C217/58 , C07C253/30 , C07C255/54
CPC分类号： C07C213/02 , C07C253/30 , C07C217/58 , C07C255/54
摘要： The invention relates to methods for producing 4-[aminoalkoxy]benzylamines of general formula (I) by means of catalytic hydrogenation of 4-[aminoalkoxy]benzonitriles of general formula (II). In the compounds of general formulae (I) and (II), R represents C1-C8 alkylene, and R and R independently represent C1-C8 alkyl or are linked to form a ring which can also contain a heteroatom. The hydrogenation is carried out at increased pressure and increased temperatures. The invention also relates to a method for producing the intermediate (II).
摘要翻译：本发明涉及一种方法，通过4- [氨基烷氧基] -benzonitrilen通式（II），其中所述通式的化合物中的I和II [R <1的催化氢化制备通式（I）的4- [氨基烷氧基]苄 >代表C1-C8亚烷基，R <2>和R <3>独立地是C1-C8烷基或连接形成一个环，该环还可以含有杂原子，其中所述氢化在升高的压力和升高的温度下进行执行。此外，本发明涉及一种用于中间体（II）的制备方法。

4. 发明申请

WO03035250A8 IRON-CONTAINING MATERIAL SUITABLE FOR USE AS A HYDROGENATION CATALYST 审中-公开
标题翻译：作为一种液压催化剂含铁质量
公开(公告)号：WO03035250A8
公开(公告)日：2003-07-24
申请号：PCT/EP0211669
申请日：2002-10-18
申请人： BASF AG , ANSMANN ANDREAS , BENISCH CHRISTOPH , BASSLER PETER , FISCHER ROLF-HARTMUTH , MAIXNER STEFAN , MELDER JOHANN-PETER , LUYKEN HERMANN
发明人： ANSMANN ANDREAS , BENISCH CHRISTOPH , BASSLER PETER , FISCHER ROLF-HARTMUTH , MAIXNER STEFAN , MELDER JOHANN-PETER , LUYKEN HERMANN
IPC分类号： B01J37/18 , B01J23/745 , B01J23/889 , C07B61/00 , C07C209/48 , C07C211/12 , C07C253/30 , C07C255/24
CPC分类号： C07C253/30 , B01J23/745 , B01J23/8892 , C07C209/48 , C07C211/12 , C07C255/24
摘要： The iron-containing catalyst suitable for use as a catalyst contains a) iron or a mixture containing iron and an iron-based compound. The iron has an average crystallite size ranging from 1-35 nm measured by X-ray diffraction.
摘要翻译：适合的催化剂，其包含a）铁或含有铁和基于铁的化合物的混合物，其中通过X射线衍射测量，所述铁的平均平均微晶尺寸为1至35nm。

5. 发明申请

WO03035249A8 IRON-CONTAINING OXIDIC MATERIAL SUITABLE FOR USE AS A HYDROGENATION CATALYST PRECURSOR 审中-公开
标题翻译： AS APPROPRIATE HYDRIERKATALYSATORVORSTUFE含氧化铁MASS
公开(公告)号：WO03035249A8
公开(公告)日：2003-07-24
申请号：PCT/EP0211667
申请日：2002-10-18
申请人： BASF AG , ANSMANN ANDREAS , BENISCH CHRISTOPH , BASSLER PETER , FISCHER ROLF-HARTMUTH , MAIXNER STEFAN , MELDER JOHANN-PETER , LUYKEN HERMANN
发明人： ANSMANN ANDREAS , BENISCH CHRISTOPH , BASSLER PETER , FISCHER ROLF-HARTMUTH , MAIXNER STEFAN , MELDER JOHANN-PETER , LUYKEN HERMANN
IPC分类号： B01J37/18 , B01J23/745 , B01J23/889 , C07B61/00 , C07C209/48 , C07C211/12
CPC分类号： B01J23/745
摘要： The oxidic material suitable for use as a hydrogenation catalyst contains a) bivalent and trivalent iron, the atomic ratio of bivalent iron to trivalent iron ranging from more than 0.5 to 5.5, and b) oxygen as a counter ion to the bivalent and trivalent iron.
摘要翻译：作为催化剂前体合适的氧化性组合物包含：a）二价铁和三价铁，其特征在于，三价铁在大于0.5的范围内的二价铁的原子比高达5.5是，和b）氧作为抗衡离子的二价铁和铁三价。

6. 发明申请

WO2010054988A2 PROCESS FOR PREPARING CYCLIC DIAMINES 审中-公开
标题翻译：制备环状二胺的方法
公开(公告)号：WO2010054988A2
公开(公告)日：2010-05-20
申请号：PCT/EP2009064751
申请日：2009-11-06
申请人： BASF SE , DAHMEN KIRSTEN , ERNST MARTIN , LIMBACH MICHAEL , MELDER JOHANN-PETER , ROESLER-FEIGEL BEATRICE , TELES JOAQUIM HENRIQUE
发明人： DAHMEN KIRSTEN , ERNST MARTIN , LIMBACH MICHAEL , MELDER JOHANN-PETER , ROESLER-FEIGEL BEATRICE , TELES JOAQUIM HENRIQUE
IPC分类号： C07C209/16 , C07C209/26 , C07C209/48 , C07C211/36 , C07C253/30 , C07C255/46
CPC分类号： C07C209/48 , C07C209/16 , C07C209/26 , C07C253/30 , C07C2601/14 , C07C211/36 , C07C255/46
摘要： The present invention relates to a process for preparing a cyclic diamine, comprising the reaction of at least one cyclic alkene with a gas mixture (G) comprising dinitrogen monoxide to give at least one cyclic ketone and the subsequent conversion of the at least one cyclic ketone to a cyclic diamine. The invention also relates to the use of a cyclic diamine with primary and secondary amine functions thus obtained to prepare polyamides and polyurethanes.
摘要翻译：本发明涉及一种制备环状二胺的方法，该方法包括使至少一种环烯烃与包含一氧化二氮的气体混合物（G）反应以得到至少一种环酮并随后转化所述至少一种环酮转化为环状二胺。本发明还涉及由此获得的具有伯胺和仲胺官能团的环状二胺用于制备聚酰胺和聚氨酯。

7. 发明申请

WO2009027249A3 METHOD FOR PRODUCING AMINES FROM SUGAR ALCOHOLS 审中-公开
标题翻译：从糖醇制备胺的方法
公开(公告)号：WO2009027249A3
公开(公告)日：2009-06-18
申请号：PCT/EP2008060742
申请日：2008-08-15
申请人： BASF SE , ERNST MARTIN , HOFFER BRAM WILLEM , MELDER JOHANN-PETER
发明人： ERNST MARTIN , HOFFER BRAM WILLEM , MELDER JOHANN-PETER
IPC分类号： C07C209/16 , C07C211/10 , C07C211/11 , C07D241/02 , C07D295/00
CPC分类号： C07C209/16 , C04B24/122 , C04B28/02 , C07C213/02 , C07D241/04 , C07D295/02 , C07D295/023 , C07C211/09 , C07C211/10 , C07C211/11 , C07C215/08
摘要： The invention relates to a method for producing amines by reacting sugar alcohols with hydrogen and an amination agent, selected from the group containing ammonia, primary and secondary amines, in the presence of a catalyst at a temperature of between 100°C and 400°C and at a pressure of between 1 and 40 MPa (10 to 400 bar). The catalyst preferably contains a metal or several metals or one or more oxygen-containing compounds of metals in groups 8 and/or 9 and/or 10 and/or 11 of the periodic table of elements. Preferably, the sugar alcohol is obtained by the hydrogenation of the corresponding sugars. The invention also relates to the use of the reaction product as an additive in cement or concrete production and in other application areas.
摘要翻译：本发明涉及一种通过糖醇与氢气和选自氨，伯和仲胺中选择的胺化剂反应制备胺的方法，在催化剂的存在下，在100℃的温度至400℃和压力 1至40MPa（10至400巴）。催化剂优选含有一种或多种金属或一种或多种元素周期表第8和/或9族和/或10和/或11族金属的含氧化合物。糖醇优选通过相应糖的氢化获得。本发明还涉及反应产物作为水泥或混凝土生产和其它应用中的添加剂的用途。

8. 发明申请

WO2010052181A3 METHOD FOR PRODUCING N,N-SUBSTITUTED-3-AMINOPROPAN-1-OLS 审中-公开
标题翻译：用于生产N，N-二取代-3-氨基-1- OLAND
公开(公告)号：WO2010052181A3
公开(公告)日：2010-09-30
申请号：PCT/EP2009064438
申请日：2009-11-02
申请人： BASF SE , WIGBERS CHRISTOF WILHELM , MELDER JOHANN-PETER , ERNST MARTIN
发明人： WIGBERS CHRISTOF WILHELM , MELDER JOHANN-PETER , ERNST MARTIN
IPC分类号： C07C213/00 , C07C215/08
CPC分类号： C07C213/02 , C07C227/08 , Y02P20/582 , C07C215/08 , C07C229/12
摘要： The present invention relates to a method for producing N,N-substituted-3-aminopropan-1-ols by a) converting secondary amine with acrolein at a temperature of (-50) to 100°C and a pressure of 0.01 to 300 bar, and b) converting the reaction mixture obtained in step a) with hydrogen and ammonia in the presence of a hydrogenation catalyst at a pressure of 1 to 400 bar, characterized in that in step a) the molar ratio of secondary amine to acrolein is 1:1 or more and the temperature in step b) is in the range of (-50) to 70°C. In a preferred embodiment, an acrolein that was obtained from glycerine based on renewable raw materials is used. The invention further relates to the use of an N,N-dimethyl-3-aminopropan-1-ol (DMAPOL) based on renewable raw materials as a catalyst for producing polyurethane, as a scrubbing liquid in gas scrubbing, in the field of electronics chemicals and electroplating, as a feed material in organic synthesis, and as an intermediate product in the production of pharmaceuticals and plant protection agents.
摘要翻译：本发明涉及一种方法，用于制备的N，N-取代的3-氨基丙-1-醇通过a）在（-50的温度下与丙烯醛仲胺的反应）至100℃和0.01的压力至300巴，和b））在1至400巴的压力下在步骤a）与氢气和氨在氢化催化剂的存在下反应混合物中得到的产物，其特征在于，在阶段的仲胺为丙烯醛1的摩尔比反应： 1以上且在步骤b的范围为（-50）至70℃的温度）在一个优选的实施方案中，丙烯醛被用于已经从甘油基于可再生资源获得的。此外，本发明涉及使用一个N，基于可再生原料的N-二甲基-3-氨基丙烷-1-醇（DMAPOL）的，作为用于聚氨酯生产的催化剂，如在气体洗涤器中的洗涤液，在电子化学品和电镀领域中，如在起始原料有机合成并作为医药和农药的制造中间体。

9. 发明申请

WO2009138377A2 METHOD FOR PRODUCING N,N-SUBSTITUTED-1,3-PROPANDIAMINES 审中-公开
标题翻译：用于生产N，N-取代的1,3-丙二胺
公开(公告)号：WO2009138377A2
公开(公告)日：2009-11-19
申请号：PCT/EP2009055655
申请日：2009-05-11
申请人： BASF SE , ERNST MARTIN , MELDER JOHANN-PETER
发明人： ERNST MARTIN , MELDER JOHANN-PETER
IPC分类号： C07C209/26 , C07C209/60
CPC分类号： C07C211/11 , C07C209/60 , Y02P20/582
摘要： The invention relates to a method for producing N,N-substituted- 1,3-propandiamine by a) reacting secondary amines with acrolein at a temperature between (-50) - 100°C and at a pressure between 0,01 - 300 bar, and b) reacting the reaction mixture obtained in step a) with hydrogen and ammonia in the presence of a hydrogenation catalyst at a temperature between 40 - 400°C and at a pressure of 1 - 400 bar. The invention is characterised in that in step a) the molar ratio of secondary amines to acrolein is 2:1 or more and the hydrogenation catalyst used in step b) contains cobalt. In a preferred embodiment, acrolein that is obtained from glycerin based on renewable raw material is used. The invention also relates to the use of a N,N-dimethyl-1,3-propandiamine (DMAPA) based on renewable raw material as charge material for soft soaps and other detergents, coagulation agents, polymers and comb polymers. In another preferred embodiment, step b) takes place in the presence of water.
摘要翻译：本发明涉及一种方法，用于制备的N，N-甲基-1,3-丙二胺substiuierten-通过用丙烯醛仲胺的）反应在温度（-50）至100℃和0.01〜300的压力巴，和b）），在温度40〜400℃和1〜400巴的压力下在步骤a）与氢气和氨在氢化催化剂的存在下反应混合物中得到的产物，其特征在于，在阶段a的摩尔比反应仲胺为丙烯醛的是2：1或更大，并包含在步骤b中使用）氢化催化剂的钴。在一个优选的实施方案中，丙烯醛被用于已经从甘油基于可再生资源获得的。此外，本发明涉及基于可再生Rohstoffenals原料用于在存在一个进一步优选的实施方案中进行软皂和其它清洁剂，凝结剂聚合物和Kammpolymere.In中，阶段b）中使用的N，N-二甲基-1,3-丙二胺（DMAPA）的水。

10. 发明申请

WO2010089266A3 HYDROGENATING CATALYSTS, PRODUCTION AND USE THEREOF 审中-公开
标题翻译：加氢催化剂，生产和使用
公开(公告)号：WO2010089266A3
公开(公告)日：2010-12-23
申请号：PCT/EP2010051143
申请日：2010-02-01
申请人： BASF SE , WIGBERS CHRISTOF WILHELM , STEINER JOCHEN , ERNST MARTIN , HOFFER BRAM WILLEM , SCHWAB EKKEHARD , MELDER JOHANN-PETER
发明人： WIGBERS CHRISTOF WILHELM , STEINER JOCHEN , ERNST MARTIN , HOFFER BRAM WILLEM , SCHWAB EKKEHARD , MELDER JOHANN-PETER
IPC分类号： B01J23/78 , B01J23/83 , B01J27/18 , B01J27/185 , B01J35/04 , B01J37/02 , C07C209/48 , C07C211/11 , C07C211/12 , C07C211/36 , C07C253/30 , C07C255/24
CPC分类号： B01J23/78 , B01J23/83 , B01J27/1853 , B01J35/04 , B01J37/0201 , B01J37/0205 , B01J37/0215 , B01J37/0234 , C07C209/48 , C07C253/30 , C07C2601/14 , C07C211/11 , C07C211/12 , C07C211/36 , C07C255/24
摘要： The invention relates to a method for improving the catalytic properties of a catalyst that exists in the form of a structured monolith and comprises one or more elements selected from the group comprising cobalt, nickel and copper, wherein the catalyst is brought into contact with one or more base compounds selected from the group of alkali, earth alkali and rare earth metals. The invention further relates to a method for hydrogenating compounds comprising at least one unsaturated carbon-carbon, carbon-nitrogen or carbon-oxygen compound, in the presence of a catalyst comprising one or more elements selected from the group comprising cobalt, nickel and copper, wherein the catalyst exists in the form of a structured monolith, characterized in that the catalyst is brought into contact with one or more base compounds selected from the group of alkali, earth alkali and rare earth metals. In addition, the invention relates to the use of a base compound selected from the group of alkali, earth alkali and rare earth metals for improving the catalytic properties of a catalyst, comprising copper and/or cobalt and/or nickel, wherein the catalyst exists in the form of a structured monolith.
摘要翻译：本发明涉及一种用于改善的催化剂，其存在于结构化的整料和或多种元素的选自由钴，镍的含有基团和铜中选择的形式的催化性质，其中与所述催化剂的一种或多种基本选自碱金属，碱土金属和稀土金属的选择的化合物所接触。本发明还涉及一种方法，用于包含在催化剂的存在下对含至少一个不饱和碳 - 碳，碳 - 氮或碳 - 氧键的化合物的氢化的组中选择的一种或多种元素自由钴，镍和铜，其中，所述催化剂是在结构化的单块形式，其特征在于，所述催化剂与选自碱金属，碱土和在接触稀土金属中的一种或多种碱性化合物接触。此外，本发明是使用选自碱金属，碱土金属和稀土金属中选出的碱性化合物，以提高催化剂的催化性能而言，包含铜和/或钴和/或镍，其特征在于，以结构化的形式的催化剂整料是存在的。

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