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1. 发明申请

WO2013009553A3 POLYOLEFIN DRAG REDUCING AGENTS PRODUCED BY MULTIPLE NON-CRYOGENIC GRINDING STAGES 审中-公开
标题翻译：多元非球晶研磨生产的聚烯烃减少剂
公开(公告)号：WO2013009553A3
公开(公告)日：2013-04-04
申请号：PCT/US2012045490
申请日：2012-07-05
申请人： BAKER HUGHES INC , MATHEW THOMAS , KOMMAREDDI NAGESH S , WARD JACK BRADFORD
发明人： MATHEW THOMAS , KOMMAREDDI NAGESH S , WARD JACK BRADFORD
IPC分类号： C08J3/12 , C08F6/00 , C08F10/00 , C08J3/02 , C09K3/00
CPC分类号： F17D1/17
摘要： Fine particulate polymer drag reducing agents (DRAs) in bi-modal or multi-modal particle size distributions may be produced simply and efficiently without cryogenic temperatures. The grinding or pulverizing of polymer, e.g. non-porous poly(alpha-olefin) suitable for reducing drag in hydrocarbons may be achieved by the use of at least one liquid grinding aid and at least two grinding processors in series. The blades of the stators of the grinders are of different configuration so that granulated polymer fed to the first processor having relatively larger gaps between blades is ground to an intermediate size which is fed to the second processor having relatively smaller gaps between blades which grinds the polymer to a second, smaller size. A non-limiting example of a suitable liquid grinding aid includes a blend of propylene glycol, water and hexanol. Particulate DRA may be produced at a size of 300 microns or less in only two passes.
摘要翻译：双模态或多模式粒度分布的细颗粒聚合物减阻剂（DRAs）可以在没有低温的情况下简单有效地生产。聚合物的研磨或粉碎，例如适用于减少烃中的阻力的非多孔聚（α-烯烃）可以通过使用至少一种液体研磨助剂和至少两种串联研磨处理器来实现。研磨机的定子的叶片具有不同的构造，使得进料到具有相对较大的叶片之间间隙的第一处理器的成粒聚合物被研磨成中间尺寸，其被馈送到第二处理器，其具有在研磨聚合物的叶片之间具有相对更小的间隙到第二个，更小的尺寸。合适的液体研磨助剂的非限制性实例包括丙二醇，水和己醇的共混物。颗粒状DRA可以仅在两次通过时以300微米或更小的尺寸生产。

2. 发明申请

WO2006132995A3 PARTICLE SIZE, PERCENT DRAG EFFICIENCY AND MOLECULAR WEIGHT CONTROL OF BULK POLYMER POLYMERIZED POLYALPHAOLEFINS USING HIGH SHEAR MATERIAL PROCESSORS 审中-公开
标题翻译：使用高剪切材料处理器的聚合物聚合物聚合物的颗粒尺寸，百分比效率和分子量控制
公开(公告)号：WO2006132995A3
公开(公告)日：2007-03-29
申请号：PCT/US2006021521
申请日：2006-06-02
申请人： BAKER HUGHES INC
发明人： MATTHEW THOMAS , KOMMAREDDI NAGESH S , CHOU LU CHIEN , HARRIS JEFFERY R , TONG CHEE LING
IPC分类号： A61K9/16 , B01F5/04 , B05D5/08 , B29B9/06 , B29C47/00 , B60C1/00 , C08J3/00 , C08K3/00 , C08K3/20 , C08L23/06 , C08L23/12 , C08L23/18 , C09K3/00
CPC分类号： C08F10/02 , C08F210/16 , C08J3/11 , C08J2323/08 , C08F2/02 , C08F2/005 , C08F210/08
摘要： High shear materials processing produces polymer drag reducing agent (DRA) slurries without cryogenic temperatures or conventional grinding. The homogenizing or size reduction, as well as controlled molecular weight reduction, of polymer such as poly(alpha-olefins), is achieved by the use of pre-ground polymer and at least one liquid, non-solvent for the polymer DRA in a high shear materials processor such as a homogenizer. In one non- limiting embodiment of the invention, the homogenizing is conducted at ambient temperature. Examples of suitable non-solvents include water and non-aqueous non-solvents including, but not necessarily limited to, alcohols, glycols, glycol ethers, ketones, and esters, having from 2-6 carbon atoms, and combinations thereof. The polymeric DRA may be homogenized to an average particle size of 300 microns or less.
摘要翻译：高剪切材料加工生产无低温温度或常规研磨的聚合物减阻剂（DRA）浆料。通过使用预研磨聚合物和至少一种用于聚合物DRA的液体非溶剂来实现聚合物（例如聚（α-烯烃））的均化或尺寸减小以及受控的分子量降低，高剪切材料处理器如均化器。在本发明的一个非限制性实施方案中，均化在环境温度下进行。合适的非溶剂的实例包括水和非水性非溶剂，包括但不一定限于具有2-6个碳原子的醇，二醇，二醇醚，酮和酯及其组合。聚合物DRA可以均化至300微米或更小的平均粒度。

3. 发明申请

WO2006138113A3 COMBINATION OF POLYMER SLURRY TYPES FOR OPTIMUM PIPELINE DRAG REDUCTION 审中-公开
标题翻译：聚合物浆料类型的组合用于最佳管道拖尾减少
公开(公告)号：WO2006138113A3
公开(公告)日：2007-04-12
申请号：PCT/US2006021928
申请日：2006-06-06
申请人： BAKER HUGHES INC
发明人： MOTIER JOHN F , HARRIS JEFFREY R , CHOU LU CHIEN , KOMMAREDDI NAGESH S
IPC分类号： C08K9/00
CPC分类号： C08F10/02 , C08F210/16 , F17D1/17 , C08F2/005 , C08F2/02 , C08F2/14 , C08F210/08
摘要： A method of extending or broadening the effective time of drag reduction for a drag reducing agent in a pipeline may be custom-designed by combining two drag reducing slurries or other drag reducing products made by different or alternative techniques. For instance a precipitation polymer slurry derived from polymer precipitation where the polymer dissolves relatively quickly can be combined with a ground polymer slurry derived by grinding bulk polymer (ground at either cryogenic or non-cryogenic temperatures), or by using other size reduction techniques, where the latter polymer dissolves relatively slowly. In one non-limiting embodiment of the invention, bulk polymer may be ground directly into a precipitation polymer slurry to make the ground polymer slurry and blend the slurries simultaneously, where the precipitation polymer slurry serves as an anti- agglomeration agent.
摘要翻译：可以通过组合两种减阻浆料或通过不同或替代技术制造的其它减阻产品来定制延长或扩大管道中减阻剂减阻的有效时间的方法。例如，衍生自聚合物沉淀的沉淀聚合物淤浆，其中聚合物相对较快地溶解，可与通过研磨本体聚合物（在低温或非低温温度下研磨）衍生的研磨聚合物浆料组合，或通过使用其它尺寸减小技术，其中后一种聚合物相对缓慢地溶解。在本发明的一个非限制性实施方案中，本体聚合物可以直接研磨成沉淀聚合物浆料，以制备研磨聚合物浆料并同时混合浆料，其中沉淀聚合物浆料用作抗附聚剂。

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