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1. 发明申请

WO2015061522A1 SELF-HEALING AGENT FORMULATIONS CONTAINING LIQUID CORROSION INHIBITORS 审中-公开
标题翻译：含有液体腐蚀抑制剂的自我保护剂配方
公开(公告)号：WO2015061522A1
公开(公告)日：2015-04-30
申请号：PCT/US2014/061876
申请日：2014-10-23
申请人： AUTONOMIC MATERIALS, INC.
发明人： WILSON, Gerald, O.
IPC分类号： C23F11/00 , C23F11/04 , C23F11/08
CPC分类号： C08K9/10 , B29C73/22 , C09D5/08 , C09D5/086 , C09D7/63 , C09D7/65 , C09D7/70 , C08L83/04
摘要： Disclosed herein are self-healing systems that include corrosion inhibitors and self-healing materials that are capable of repairing themselves without any external intervention when they are damaged. The self-healing materials and corrosion inhibitors may be microencapsulated, and damage to a matrix containing the microcapsules may rupture the microcapsules and cause the self-healing materials and corrosion inhibitors to be released into the site of damage. The self- healing materials then may polymerize and restore the functional capabilities of the matrix, and the corrosion inhibitors may work in concert with the self healing materials to prevent corrosion at the site of damage.
摘要翻译：本文公开了包括腐蚀抑制剂和自修复材料的自修复系统，其能够在损坏时无需任何外部干预即可自行修复。自修复材料和腐蚀抑制剂可以被微胶囊化，并且对含有微胶囊的基质的损伤可能使微胶囊破裂并导致自修复材料和腐蚀抑制剂释放到损伤部位。然后，自愈材料可以聚合并恢复基质的功能性，并且腐蚀抑制剂可以与自愈材料协同工作，以防止损伤部位的腐蚀。

2. 发明申请

WO2019168551A1 ZINC-RICH COATINGS AND SYSTEMS WITH MICROENCAPSULATED HEALING AGENTS 审中-公开
公开(公告)号：WO2019168551A1
公开(公告)日：2019-09-06
申请号：PCT/US2018/026732
申请日：2018-04-09
申请人： AUTONOMIC MATERIALS, INC.
发明人： WILSON, Gerald, O. , KASISOMAYAJULA, Subramanyam, V. , DAYTON, Christopher, R. D.
IPC分类号： C09D7/65 , C08J3/12 , C09D163/00 , B05D5/10 , B05D7/14 , B05D7/00
摘要： Microencapsulated healing agents that, upon incorporation into a zinc-rich coating or coating system, improve the coating or coating system's ability to maintain its adhesion and corrosion resistance after damage that exposes the underlying substrate. These microencapsulated healing agent formulations are uniquely synergistic with zinc-rich coatings, and/or with zinc particles in a zinc rich coating, improving both adhesion maintenance and corrosion resistance following damage that exposes the substrate.

3. 发明申请

WO2015006727A1 DISPERSION OF MICROCAPSULES FOR SELF-HEALING APPLICATIONS 审中-公开
标题翻译：自我治疗应用微阵列的分散
公开(公告)号：WO2015006727A1
公开(公告)日：2015-01-15
申请号：PCT/US2014/046407
申请日：2014-07-11
申请人： AUTONOMIC MATERIALS, INC.
发明人： WILSON, Gerald, O. , KASISOMAYAJULA, Subramanyam, V. , BLANCHETTE, Ryan, T.
IPC分类号： B01J13/02 , B01J13/18 , B01F17/14
CPC分类号： C08L71/02 , C08L61/24 , C09D5/00 , C09D161/24
摘要： Disclosed herein are compositions and methods for increasing microcapsule dispersion in self-healing paint and coating applications, and more particularly for non-covalent functionalization of polymeric microcapsule shell walls for improved dispersion in polymeric material formulations. Some embodiments are methods of forming a microcapsule dispersion, the methods including providing a polymeric material capable of forming a plurality of microcapsules; initiating polymerization of the polymeric material under reaction conditions sufficient to permit formation of the plurality of microcapsules; and adding an ethoxy-functionalized dispersant to the polymeric material before formation of the plurality of microcapsules is complete, thereby forming the microcapsule dispersion.
摘要翻译：本文公开了用于增加自修复涂料和涂料应用中的微胶囊分散体的组合物和方法，更具体地涉及聚合物微胶囊壳壁的非共价官能化以改善聚合物材料配方中的分散体。一些实施方案是形成微胶囊分散体的方法，所述方法包括提供能够形成多个微胶囊的聚合物材料; 在足以允许形成多个微胶囊的反应条件下引发聚合物材料的聚合; 并且在形成多个微胶囊之前，向聚合物材料中加入乙氧基官能化的分散剂，从而形成微胶囊分散体。

4. 发明申请

WO2020243441A1 SILICONE-BASED PROTECTIVE FORMULATIONS 审中-公开
公开(公告)号：WO2020243441A1
公开(公告)日：2020-12-03
申请号：PCT/US2020/035138
申请日：2020-05-29
申请人： AUTONOMIC MATERIALS, INC.
发明人： WILSON, Gerald, O. , NAVARRO, Aidnel, Geister R. , KASISOMAYAJULA, Subramanyam, V.
IPC分类号： C08K9/10 , C08K5/5415 , C08L83/04 , C08G77/20 , C08G77/08 , B29C73/16 , C09D183/04 , C09D7/40 , C09D5/00
摘要： Self-healing compositions, method of preparation and uses thereof are disclosed. In an example, a self-healing composition includes a first microcapsule and a second microcapsule. The first microcapsule includes a first polydimethylsiloxane resin, a first silicone fluid, a first functionalized alkoxysilane, and a catalyst capable of catalyzing hydrosilylation reactions, and the second microcapsule includes a second polydimethylsiloxane resin, a second silicone fluid, a second functionalized alkoxysilane, and a hydrogen-terminated dimethyl siloxane resin. In this way, the self- healing composition releases and mixes contents of the first microcapsule and the second microcapsule upon the rupture thereof, imparting a passively initiated repair process to the self-healing composition.

5. 发明申请

WO2018031511A1 BIOCIDAL PROTECTIVE FORMULATIONS 审中-公开
标题翻译：生物防护配方
公开(公告)号：WO2018031511A1
公开(公告)日：2018-02-15
申请号：PCT/US2017/045831
申请日：2017-08-08
申请人： AUTONOMIC MATERIALS, INC.
发明人： WILSON, Gerald, O. , EBBERT, Byron, R.
IPC分类号： A01N25/28 , A01N43/80 , C08L67/00 , C08L33/12 , C08L63/00
摘要： Disclosed are biocidal self-healing protective materials, including coatings, stains, sealants, and adhesives. The biocidal protective materials may include a first microcapsule that includes a hydrophobic film-forming agent and a hydrophobic biocidal agent. Upon rupture of the first microcapsule, the hydrophobic film-forming agent may form a polymerized film that includes the hydrophobic biocidal agent. The biocidal protective materials may include a second microcapsule that may include a curing agent. Upon rupture of the first and second microcapsules, the curing agent may cause the hydrophobic film-forming agent to form a polymerized film that includes the hydrophobic biocidal agent. Also disclosed are protective materials that include a polymeric material matrix and the first and/or second microcapsules, as well as methods of increasing the biocidal activity of a protective material and methods of increasing a biocidal activity of a porous substrate.
摘要翻译：公开了生物灭杀自愈保护材料，包括涂料，污渍，密封剂和粘合剂。杀生物保护材料可以包括包含疏水性成膜剂和疏水性杀生物剂的第一微胶囊。在第一微胶囊破裂时，疏水性成膜剂可形成包含疏水性杀生物剂的聚合膜。杀生物保护材料可以包括可以包含固化剂的第二微胶囊。当第一和第二微胶囊破裂时，固化剂可以使疏水性成膜剂形成包含疏水性杀生物剂的聚合膜。还公开了包含聚合物材料基质和第一和/或第二微胶囊的保护性材料，以及增加保护性材料的杀生物活性的方法和增加多孔基质的杀生物活性的方法。

6. 发明申请

WO2018018014A3 PEEL-RESISTANT SELF-HEALING COATINGS AND STAINS FOR POROUS SUBRTATES 审中-公开
公开(公告)号：WO2018018014A3
公开(公告)日：2018-01-25
申请号：PCT/US2017/043390
申请日：2017-07-21
申请人： AUTONOMIC MATERIALS, INC.
发明人： WILSON, Gerald, O. , EBBERT, Byron, R.
IPC分类号： B05D5/00 , C09D167/06 , C09D167/08 , C09D191/00 , C09D183/04 , B05D7/24
摘要： Disclosed are methods of protecting porous substrates and/or increasing the peel-resistance of coatings and stains for porous substrates. The methods may include providing a stain or coating comprising a microencapsulated self-healing material; and applying the stain or coating to a porous substrate. Damage to the stain or coating may release the self-healing material at a site of damage, such as a crack or scratch in the stain or coating. The self-healing material may be a polymeric precursor,.an unsaturated polyester resin or alkyd, a fatty acid-based natural oil or derivative thereof, or a cross-linkable silane or siloxane monomer or resin. The microencapsulated self-healing material may include a microcapsule having a shell wall that includes a thermosetting polymer or a thermoplastic polymer; the thermosetting polymer may include urea-formaldehyde, melamine formaldehyde, polyurethane, polyurea, or polyacrylate; and the thermoplastic polymer comprises poly(methyl methacrylate), poly(lactic acid), or poly(glycolic acid).

7. 发明申请

WO2018018014A2 PEEL-RESISTANT SELF-HEALING COATINGS AND STAINS FOR POROUS SUBRTATES 审中-公开
标题翻译：用于多孔微孔板的抗剥离自修复涂层和染色剂
公开(公告)号：WO2018018014A2
公开(公告)日：2018-01-25
申请号：PCT/US2017/043390
申请日：2017-07-21
申请人： AUTONOMIC MATERIALS, INC.
发明人： WILSON, Gerald, O. , EBBERT, Byron, R.
摘要： Disclosed are methods of protecting porous substrates and/or increasing the peel-resistance of coatings and stains for porous substrates. The methods may include providing a stain or coating comprising a microencapsulated self-healing material; and applying the stain or coating to a porous substrate. Damage to the stain or coating may release the self-healing material at a site of damage, such as a crack or scratch in the stain or coating. The self-healing material may be a polymeric precursor,.an unsaturated polyester resin or alkyd, a fatty acid-based natural oil or derivative thereof, or a cross-linkable silane or siloxane monomer or resin. The microencapsulated self-healing material may include a microcapsule having a shell wall that includes a thermosetting polymer or a thermoplastic polymer; the thermosetting polymer may include urea-formaldehyde, melamine formaldehyde, polyurethane, polyurea, or polyacrylate; and the thermoplastic polymer comprises poly(methyl methacrylate), poly(lactic acid), or poly(glycolic acid).
摘要翻译：公开了保护多孔基材和/或增加多孔基材的涂料和着色剂的抗剥离性的方法。该方法可以包括提供包含微胶囊化自修复材料的污渍或涂层; 并将该污渍或涂层施加到多孔基材上。对污渍或涂层的损坏可能会在损坏部位释放自修复材料，例如污迹或涂层中的裂缝或划痕。自我修复材料可以是聚合物前体，不饱和聚酯树脂或醇酸树脂，基于脂肪酸的天然油或其衍生物或可交联硅烷或硅氧烷单体或树脂。微胶囊化自修复材料可以包括具有包含热固性聚合物或热塑性聚合物的壳壁的微胶囊; 热固性聚合物可以包括脲醛，三聚氰胺甲醛，聚氨酯，聚脲或聚丙烯酸酯; 并且热塑性聚合物包含聚（甲基丙烯酸甲酯），聚（乳酸）或聚（乙醇酸）。

8. 发明申请

WO2014201290A1 SELF-HEALING POLYMERIC MATERIALS VIA UNSATURATED POLYESTERS 审中-公开
标题翻译：通过不饱和聚酯的自愈聚合材料
公开(公告)号：WO2014201290A1
公开(公告)日：2014-12-18
申请号：PCT/US2014/042184
申请日：2014-06-12
申请人： AUTONOMIC MATERIALS, INC.
发明人： WILSON, Gerald, O.
IPC分类号： A61K47/32 , C08L67/02 , C09D167/02
CPC分类号： C08L75/04 , B29C73/16 , B29C73/22 , C08J3/241 , C08J2367/02 , C08J2367/08 , C08K9/10 , C08L33/00 , C08L61/24 , C08L61/28 , C08L67/08 , C09D167/08 , C09D175/04 , C09J133/066 , C09J133/08 , C09J167/08 , C09J175/00
摘要： Disclosed herein are self-healing materials, which are smart materials that are capable of repairing themselves without any external intervention when they are damaged. The self-healing materials may be microencapsulated, for example in a one-capsule system or a two-capsule system, and damage to a matrix containing the microcapsules may rupture the microcapsules and cause the healing materials to be released into the site of damage, where it may polymerize and restore the functional capabilities of the matrix. The self-healing materials may be based on unsaturated multi-functional resins capable of oxygen-initiated cross-linking, and may include alkyd resins, such as alkyd resins that include one or more telechelic end groups.
摘要翻译：这里公开的是自修复材料，它们是能够在损坏时无需任何外部干预的情况下自行修复的智能材料。自修复材料可以例如在单胶囊系统或双胶囊系统中微胶囊化，并且对含有微胶囊的基质的损伤可能破裂微胶囊并导致愈合材料释放到损伤部位，在那里它可以聚合并恢复基体的功能性能。自修复材料可以基于能够引发氧的交联的不饱和多官能树脂，并且可以包括醇酸树脂，例如包含一个或多个遥爪端基的醇酸树脂。

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