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1. 发明申请

WO2013169447A1 PURIFICATION OF SUCCINIC ACID 审中-公开
标题翻译：纯化酸
公开(公告)号：WO2013169447A1
公开(公告)日：2013-11-14
申请号：PCT/US2013/036858
申请日：2013-04-17
申请人： ARCHER DANIELS MIDLAND COMPANY
发明人： SOPER, John, G. , SCHULTZ, Mitchell , BINDER, Thomas P.
IPC分类号： C12P7/40 , C12P7/44 , C12P7/46 , C12P1/04 , C12N1/20
CPC分类号： C07C51/47 , B01D15/327 , B01D15/426 , C07C51/42 , C12P7/46 , C07C55/10
摘要： A process for purifying a filtered fermentation broth of succinic acid is described. The process involves separating succinic acid from the other organic acids and salts in. a raw filtered broth using a non- functionalized chromatographic resin. The operation can be run either as an isocratic elution to yield free succinic acid, or as a gradient or binary elution to produce succinate salt.
摘要翻译：描述了用于纯化过滤的琥珀酸发酵液的方法。该方法包括使用非官能化色谱树脂将琥珀酸与原始过滤的肉汤中的其它有机酸和盐分离。操作可以作为等度洗脱进行，以产生游离的琥珀酸，或者作为梯度或二元洗脱来产生琥珀酸盐。

2. 发明申请

WO2013106137A1 PROCESS FOR MAKING LEVULINIC ACID 审中-公开
标题翻译：制备维生素A的方法
公开(公告)号：WO2013106137A1
公开(公告)日：2013-07-18
申请号：PCT/US2012/066710
申请日：2012-11-28
申请人： ARCHER DANIELS MIDLAND COMPANY
发明人： SANBORN, Alexandra , BINDER, Thomas P.
IPC分类号： C07C51/12 , C07C53/126 , C07D307/44
CPC分类号： C07C51/31 , C07C51/00 , C07C59/185
摘要： A process is described wherein a feed of a six-carbon carbohydrate-containing material or of a furanic dehydration product from a six-carbon carbohydrate-containing material or of a combination of these is supplied to a reactor in a controlled manner over time up to a desired combined or total feed level, and the feed is acid-hydrolyzed to produce levulinic acid. In certain embodiments, derivatives of the levulinic acid are prepared.
摘要翻译：描述了一种方法，其中将含六碳碳水化合物的材料或来自含六碳碳水化合物的材料的呋喃脱水产物或它们的组合的进料以受控的方式随时间供应到反应器中，期望的组合或总进料水平，并且进料被酸水解以产生乙酰丙酸。在某些实施方案中，制备乙酰丙酸的衍生物。

3. 发明申请

WO2013043981A1 CELLULOLYTIC ENZYME COMPOSITIONS AND USES THEREOF 审中-公开
标题翻译：纤维素酶组合物及其用途
公开(公告)号：WO2013043981A1
公开(公告)日：2013-03-28
申请号：PCT/US2012/056502
申请日：2012-09-21
申请人： NOVOZYMES A/S , ARCHER DANIELS MIDLAND COMPANY
发明人： IYER, Prashant , GASPAR, Armindo Ribeiro , CROONENBERGHS, James , BINDER, Thomas P.
IPC分类号： C12N9/18 , C12P7/10 , C12N9/42 , C12P19/14
CPC分类号： C12N9/18 , C07K14/37 , C12N9/2402 , C12N9/2437 , C12N9/2445 , C12P7/10 , C12P7/14 , C12P19/02 , C12P19/14 , C12P2203/00 , C12Y301/01072 , Y02E50/16
摘要： The present invention relates enzyme composition comprising a cellulolytic preparation and an acetylxylan esterase (AXE); and the used of cellulolytic enzyme compositions for hydrolyzing acetylated cellulosic material. Finally the invention also relates to processes of producing fermentation products from acetylated cellulosic materials using a cellulolytic enzyme composition of the invention.
摘要翻译：本发明涉及包含纤维素分解制剂和乙酰木聚糖酯酶（AX）的酶组合物; 并使用纤维素分解酶组合物水解乙酰化纤维素材料。最后，本发明还涉及使用本发明的纤维素分解酶组合物从乙酰化纤维素材料生产发酵产物的方法。

4. 发明申请

WO2011097075A2 IMPROVED PROCESS FOR FRACTIONATION OF LIGNOCELLULOSIC BIOMASS 审中-公开
标题翻译：木质纤维素生物质分级的改进方法
公开(公告)号：WO2011097075A2
公开(公告)日：2011-08-11
申请号：PCT/US2011/022000
申请日：2011-01-21
申请人： ARCHER DANIELS MIDLAND COMPANY , BINDER, Thomas P. , BLOOM, Paul D. , DOANE, Perry H. , MA, Chicheng
发明人： BINDER, Thomas P. , BLOOM, Paul D. , DOANE, Perry H. , MA, Chicheng
IPC分类号： C08B1/00 , A23K1/12 , C12P5/02 , C12P7/10 , C12P13/04
CPC分类号： C12P7/10 , A23K10/32 , A23K40/10 , A23K50/10 , C07G1/00 , C08H8/00 , C12P2203/00 , Y02E50/10 , Y02E50/16 , Y02E50/30 , Y02P60/877 , Y02T50/678
摘要： Methods are provided for the efficient fractionation of lignocellulosic biomasses into cellulosic, hemicellulosic and lignin fractions, wherein concentrated organic acid vapors are applied to the biomass at elevated temperatures at the location(s) or near the location(s) where the biomass has been harvested and gathered, to at least partly depolymerize or substantially solubilize the hemicelluloses and lignins in the biomass. The organic acid-treated biomass is in either case then dried and pelletized for extended bulk storage and/or for shipment to a second facility some distance away. The organic acid-treated biomass may be processed into desired chemicals, fuels and/or fuel additives at the local processing site or at a second facility away from the local processing site, or the pelletized material may be used as a ruminant feed locally or at a feedlot some distance removed from the local processing site.
摘要翻译：提供了将木质纤维素生物质有效分馏成纤维素，半纤维素和木质素部分的方法，其中将浓缩的有机酸蒸气在升高的温度下施用于生物质的位置处或附近的位置（ s），其中收获和收集生物质，以至少部分解聚或基本上溶解生物质中的半纤维素和木质素。经过有机酸处理的生物质在任一情况下都经过干燥和造粒以延长大容量储存和/或运送到距离一定距离的第二设施。有机酸处理过的生物质可以在当地处理场所或远离当地处理场所的第二设施处理成期望的化学品，燃料和/或燃料添加剂，或者该粒状材料可以局部用作反刍动物饲料或一个距离本地处理站点一定距离的饲养场。

5. 发明申请

WO2016032923A1 METHOD FOR THE CHROMATOGRAPHIC SEPARATION OF SORBITOL FROM DEXTROSE 审中-公开
标题翻译：用于从酯类中分离SORBITOL的方法
公开(公告)号：WO2016032923A1
公开(公告)日：2016-03-03
申请号：PCT/US2015/046462
申请日：2015-08-24
申请人： ARCHER DANIELS MIDLAND COMPANY
发明人： BINDER, Thomas P. , SOPER, John G.
IPC分类号： C07C29/141
CPC分类号： C07C29/132 , C07C29/76 , C07C31/26
摘要： A method for the continuous production and separation of sorbitol from dextrose to produce a high purity sorbitol product is described. The method comprises hydrogenating a dextrose composition in a continuous reaction to produce a mixture of sorbitol and dextrose, and contacting the mixture with a matrix containing a strong acid cation exchange resin in a simulated moving bed chromatography apparatus. An extract stream comprising 99.5% or greater sorbitol and a raffinate stream depleted of sorbitol and enriched in dextrose relative to the mixture are recovered from the apparatus. The method can also be used to produce hydrogenated maltodextrins and hydrogenated isomaltodextrins.
摘要翻译：描述了从葡萄糖连续生产和分离山梨糖醇以产生高纯度山梨醇产品的方法。所述方法包括在连续反应中氢化葡萄糖组合物以产生山梨糖醇和葡萄糖的混合物，并在模拟的移动床层析装置中将混合物与含有强酸阳离子交换树脂的基质接触。从该装置回收包含99.5％或更高的山梨糖醇和贫饱和山梨糖醇并且相对于混合物富含葡萄糖的萃余液流的提取物流。该方法也可用于生产氢化麦芽糖糊精和氢化异麦芽糊精。

6. 发明申请

WO2015156806A1 SYNTHESIS OF R-GLUCOSIDES, SUGAR ALCOHOLS, REDUCED SUGAR ALCOHOLS, AND FURAN DERIVATIVES OF REDUCED SUGAR ALCOHOLS 审中-公开
标题翻译： R-GLUCOSIDES，糖酒精，还原糖酒精和还原糖酒精的糠醛衍生物的合成
公开(公告)号：WO2015156806A1
公开(公告)日：2015-10-15
申请号：PCT/US2014/033586
申请日：2014-04-10
申请人： ARCHER DANIELS MIDLAND COMPANY
发明人： SANBORN, Alexandra , BINDER, Thomas P.
IPC分类号： C13K1/02
CPC分类号： C07C29/132 , C07C29/60 , C07D307/12 , C07D307/20 , C07H1/00 , C07H15/04 , C07C31/26 , C07C31/24
摘要： Disclosed herein are methods for synthesizing 1,2,5,6-hexanetetrol (HTO), 1,6 hexanediol (HDO) and other reduced polyols from C5 and C6 sugar alcohols or R glycosides. The methods include contacting the sugar alcohol or R-glycoside with a copper catalyst, most desirably a Raney copper catalyst with hydrogen for a time, temperature and pressure sufficient to form reduced polyols having 2 to 3 fewer hydoxy groups than the starting material. When the starting compound is a C6 sugar alcohol such as sorbitol or R-glycoside of a C6 sugar such as methyl glucoside, the predominant product is HTO. The same catalyst can be used to further reduce the HTO to HDO.
摘要翻译：本文公开了用于从C5和C6糖醇或R糖苷合成1,2,5,6-己烷乙醇（HTO），1,6-己二醇（HDO）和其它还原的多元醇的方法。所述方法包括使糖醇或R-糖苷与铜催化剂接触，最理想的是具有氢气的拉尼铜催化剂一段时间，足以形成比起始原料少2-3个羟基的还原多元醇的温度和压力。当起始化合物是C6糖醇如C6糖如山梨糖醇或R-糖苷如甲基葡糖苷时，主要产物是HTO。可以使用相同的催化剂进一步将HTO还原成HDO。

7. 发明申请

WO2013106136A1 PROCESS FOR MAKING HMF AND HMF DERIVATIVES FROM SUGARS, WITH RECOVERY OF UNREACTED SUGARS SUITABLE FOR DIRECT FERMENTATION TO ETHANOL 审中-公开
标题翻译：用于制备HMF和HMF衍生物的方法，用于恢复适用于直接发酵至乙醇的无菌糖
公开(公告)号：WO2013106136A1
公开(公告)日：2013-07-18
申请号：PCT/US2012/066708
申请日：2012-11-28
申请人： ARCHER DANIELS MIDLAND COMPANY
发明人： SANBORN, Alexandra , BINDER, Thomas P. , HOFFART, April
IPC分类号： C07D307/48 , C12P7/06 , C12P7/56
CPC分类号： C07D307/46 , C07C29/14 , C07D307/48 , C07D307/50 , C12P7/06 , C12P7/18 , C12P7/56 , C12P13/08 , Y02E50/17
摘要： Hydroxymethylfurfural is made from an aqueous hexose sugar solution, especially from a high fructose corn syrup product. By rapidly heating the sugar solution to the elevated temperatures involved as well as rapidly cooling the resultant product mixture, a limited per-pass conversion to HMF is obtained; correspondingly, however, the overall exposure of the HMF that is formed to acidic, elevated temperature conditions is also limited, so that byproducts are reduced. Separation and recovery of the products is simplified, and levels of HMF and other hexose dehydration products known to inhibit ethanol production by fermentation are reduced in the residual sugars product, to an extent whereby the residual sugars product is suited to be directly fermented to ethanol or for other uses.
摘要翻译：羟甲基糠醛由己糖糖水溶液，特别是高果糖玉米糖浆产品制成。通过将糖溶液快速加热到所涉及的高温以及快速冷却所得产物混合物，获得对HMF的有限的通过转化率; 然而，相应地，形成在酸性，高温条件下的HMF的总体曝光也受到限制，从而减少了副产物。简化了产品的分离和回收，已知残留糖产物抑制乙醇生产已知的HMF和其它己糖脱水产物的水平在一定程度上降低到残留糖产物适合直接发酵成乙醇或用于其他用途。

8. 发明申请

WO2011097070A3 IMPROVED GRAIN MILLING PROCESS 审中-公开
公开(公告)号：WO2011097070A3
公开(公告)日：2011-08-11
申请号：PCT/US2011/021601
申请日：2011-01-19
申请人： ARCHER DANIELS MIDLAND COMPANY , BINDER, Thomas P.
发明人： BINDER, Thomas P.
IPC分类号： C12P7/10 , B02C4/06
摘要： A modification is described of a dry grind process for producing ethanol and other co-products from whole grain, whereby the mash is thermochemically treated by cooking the mash in the presence of an organic acid. The organic acid effectively hydrolyzes both the starch and hemicellulosic components in the milled corn to provide fermentable sugars from both the endosperm and other parts of the kernel, without, however, also producing fermentation-inhibiting levels of other known products of the acid hydrolysis of hemicellulosic materials, such as hydroxymethylfurfural (HMF) and furfural. Further, the organic acid is able to solubilize both the starch and the more recalcitrant hemicelluloses while only partially hydrolyzing the same, so that most of the starch and hemicelluloses are hydrolyzed to oligomers and the amount of chemically labile and reducing sugars is kept sufficiently low as to also not appreciably interfere with the fermentation to ethanol.

9. 发明申请

WO2016061037A1 METHOD FOR ADJUSTING THE COMPOSITION OF CHROMATOGRAPHY PRODUCTS 审中-公开
标题翻译：用于调节色谱产物组合物的方法
公开(公告)号：WO2016061037A1
公开(公告)日：2016-04-21
申请号：PCT/US2015/055224
申请日：2015-10-13
申请人： ARCHER DANIELS MIDLAND COMPANY
发明人： BINDER, Thomas P. , SCHULTZ, Mitchell J.
IPC分类号： B01D15/18
CPC分类号： B01D15/1828 , B01D15/362 , C13K1/08 , C13K3/00 , C13K11/00
摘要： Described herein is a method of adjusting the composition of a chromatography product to achieve a target enriched proportion of a desired component from an input feed having a lower proportion of the desired component using simulated moving bed ("SMB") chromatography wherein the eluent for the SMB apparatus may comprise the very input feed being enriched. The method is exemplified by enriching a high fructose corn syrup from a 42% fructose syrup to a 55% fructose syrup without substantially reducing the dissolved solids concentration of the 55% syrup relative to the input 42% syrup. The 42% syrup is also used as the eluent for the SMB apparatus and may be reconstituted from the raffinate stream by passing the raffinate stream over a glucose isomerase column alone or in combination with a dextrose feed. The method reduces water usage and saves energy by minimizing the need for evaporation to obtain a 55% fructose syrup with a high dissolved solids content.
摘要翻译：本文描述的是调节色谱产物的组成的方法，以使用模拟移动床（“SMB”）色谱法从具有较低比例的所需组分的输入进料中获得所需组分的目标富集比例，其中用于 SMB装置可以包括富含的非常输入的进料。该方法的例子是将高果糖玉米糖浆从42％果糖糖浆富集至55％果糖糖浆，而基本上不降低55％糖浆相对于输入的42％糖浆的溶解固体浓度。 42％的糖浆也用作SMB装置的洗脱剂，并且可以通过将残液流单独或与葡萄糖进料组合使用葡萄糖异构酶柱，从萃余液流中重构。该方法通过最小化蒸发的需要来获得具有高溶解固体含量的55％果糖糖浆来减少用水量并节省能量。

10. 发明申请

WO2014175989A1 CATALYTIC SYNTHESIS OF REDUCED FURAN DERIVATIVES 审中-公开
标题翻译：催化合成还原型呋喃衍生物
公开(公告)号：WO2014175989A1
公开(公告)日：2014-10-30
申请号：PCT/US2014/031933
申请日：2014-03-27
申请人： ARCHER DANIELS MIDLAND COMPANY
发明人： SANBORN, Alexandra , BINDER, Thomas P.
IPC分类号： C07D405/06
CPC分类号： C07D307/42 , C07D307/46
摘要： The present invention relates to catalytic synthesis of furan derivatives from alkoxymethylfurfural ethers or acyloxymethylfurfural esters. More particularly, the invention pertains to furan derivatives obtained by use of a multifunctional catalyst system to carry out both hydrogenation of furan starting material and hydrolysis of the reduced furan derivative in a single reaction. The process allows recovering and recycling of alcohol or acid from the reaction product.
摘要翻译：本发明涉及从烷氧基甲基糠醚或酰氧基甲基糠酯的呋喃衍生物的催化合成。更具体地，本发明涉及通过使用多官能催化剂体系获得的呋喃衍生物，以在单次反应中进行呋喃起始原料的氢化和还原呋喃衍生物的水解。该方法允许从反应产物中回收和再循环醇或酸。

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