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1. 发明申请

WO2010100256A2 BULK SULFIDIC MIXED METAL CATALYST AND METHODS FOR ITS MANUFACTURE AND USE IN CONVERTING SYNGAS TO ALCOHOL 审中-公开
标题翻译：大容量硫化金属催化剂及其制造方法及其在酒精转化中的应用
公开(公告)号：WO2010100256A2
公开(公告)日：2010-09-10
申请号：PCT/EP2010052822
申请日：2010-03-05
申请人： ALBEMARLE EUROPE SPRL , JANBROERS STEPHAN , OOGJEN BOB GERARDUS , PLANTENGA FRANS LODEWIJK , HOMAN FREE HARMANNUS WILLEM , EIJSBOUTS-SPICKOVA SONA , STEENWINKEL EDGAR EVERT , NUBERG EDWIN
发明人： JANBROERS STEPHAN , OOGJEN BOB GERARDUS , PLANTENGA FRANS LODEWIJK , HOMAN FREE HARMANNUS WILLEM , EIJSBOUTS-SPICKOVA SONA , STEENWINKEL EDGAR EVERT , NUBERG EDWIN
CPC分类号： B01J27/0515 , B01J23/8872 , B01J37/0009 , B01J37/20 , C07C29/1518 , Y02P20/52 , C07C31/08 , C07C31/04
摘要： A process for sulfiding a cobalt-molybdenum bulk catalyst precursor to form a bulk sulfided alcohol synthesis catalyst. The process steps include contacting an oxidic bulk cobalt- molybdenum catalyst precursor with an amount of a sulfur-containing compound which is in the range of about 1 to about 10 moles of sulfur per mole of metals, at one or more temperatures at or in excess of about 300°C in a medium which is substantially devoid of added hydrogen, so as to form a sulfided bulk cobalt-molybdenum catalyst product. Also described are processes for forming the catalyst precursor, processes for producing an alcohol using the catalyst product and the catalyst product itself.
摘要翻译：硫化钴 - 钼体积催化剂前体以形成本体硫化醇合成催化剂的方法。所述方法步骤包括使氧化体钴钴钼催化剂前体与一定量的含硫化合物接触，所述含硫化合物的量在约或约10摩尔硫/每摩尔金属的一个或多个温度下或过量在基本上没有添加氢的介质中约300℃，以形成硫化体积的钴 - 钼催化剂产物。还描述了形成催化剂前体的方法，使用催化剂产物和催化剂产物本身生产醇的方法。

2. 发明申请

WO2011023668A3 SOLUTIONS AND CATALYSTS COMPRISING GROUP VI METAL, GROUP VIII METAL, PHOSPHOROUS AND AN ADDITIVE 审中-公开
标题翻译：包含第VI组金属，第VIII族金属，磷和添加剂的溶液和催化剂
公开(公告)号：WO2011023668A3
公开(公告)日：2011-05-19
申请号：PCT/EP2010062282
申请日：2010-08-24
申请人： ALBEMARLE EUROPE SPRL , EIJSBOUTS-SPICKOVA SONA , JANSEN MARCEL ADRIAAN
发明人： EIJSBOUTS-SPICKOVA SONA , JANSEN MARCEL ADRIAAN
IPC分类号： B01J23/888 , B01J21/04 , B01J23/88 , B01J27/185 , B01J27/19 , B01J37/02 , B01J37/08
CPC分类号： B01J27/19 , B01J21/04 , B01J23/88 , B01J23/888 , B01J27/1853 , B01J37/0203 , B01J37/0213 , B01J37/0236 , B01J37/08 , C10G45/00 , C10G45/08 , C10G49/04
摘要： This invention provides a process for forming a solution composition, which process comprises forming a primary solution by bringing together, in an aqueous medium, i) at least one phosphorus compound, ii) at least one Group VI metal compound, iii) at least one Group VIII metal compound, and iv) an additive which is a) tetraethylene glycol, b) polyethylene glycol having an average molecular weight in the range of about 200 to about 400, c) a mixture of tetraethylene glycol and polyethylene glycol having an average molecular weight in the range of about 200 to about 400, or d) a mixture of (1) tetraethylene glycol and/or polyethylene glycol having an average molecular weight in the range of about 200 to about 400 and (2) one or more of monoethylene glycol, diethylene glycol, and triethylene glycol. The molar ratio of additive to the total moles of Group VI metal and Group VIII metal is above 0.30:1, and the atomic ratio of phosphorus to Group VI metal is at least about 0.33: 1. Optionally, the primary solution is heated at a temperature above about 40°C to form a heated solution. The heated solution is optionally cooled to form a cooled solution. Also provided are compositions formed by such processes, processes for forming catalyst compositions from these compositions, and catalyst compositions formed by these processes.
摘要翻译：本发明提供一种形成溶液组合物的方法，该方法包括通过在水性介质中聚合来形成初级溶液，i）至少一种磷化合物，ii）至少一种VI族金属化合物，iii）至少一种 VIII族金属化合物，和iv）a）四乙二醇，b）平均分子量在约200至约400范围内的聚乙二醇的添加剂，c）四甘醇和聚乙二醇的混合物，其平均分子量重量在约200至约400的范围内，或d）平均分子量在约200至约400范围内的（1）四甘醇和/或聚乙二醇的混合物，和（2）一种或多种单乙烯乙二醇，二甘醇和三甘醇。 VI族金属和VIII族金属的添加剂与总摩尔数的摩尔比高于0.30:1，磷与Ⅵ族金属的原子比为至少约0.33:1。任选地，将第一溶液加热至温度高于约40℃以形成加热溶液。加热的溶液任选地冷却以形成冷却的溶液。还提供了通过这些方法形成的组合物，由这些组合物形成催化剂组合物的方法，以及由这些方法形成的催化剂组合物。

3. 发明申请

WO2011029716A2 CONCENTRATED SOLUTIONS COMPRISING GROUP VI METAL, GROUP VIII METAL, AND PHOSPHORUS 审中-公开
标题翻译：包含第VI组金属，第VIII族金属和磷的浓缩溶液
公开(公告)号：WO2011029716A2
公开(公告)日：2011-03-17
申请号：PCT/EP2010062283
申请日：2010-08-24
申请人： ALBEMARLE EUROPE SPRL , EIJSBOUTS-SPICKOVA SONA , JANSEN MARCEL ADRIAAN
发明人： EIJSBOUTS-SPICKOVA SONA , JANSEN MARCEL ADRIAAN
IPC分类号： B01J23/88
CPC分类号： B01J23/888 , B01J23/88 , B01J27/1853 , B01J27/19 , B01J37/0203 , B01J37/0213 , B01J37/0236 , B01J37/08 , C10G45/04 , C10G45/08 , C10G49/04
摘要： This invention provides processes for forming solution compositions, which processes comprises bringing together, in an aqueous medium, i) at least one phosphorus compound; ii) at least one Group VI metal compound; and iii) at least one Group VIII metal compound, such that a solution having a Group VI metal concentration of more than about 5.6 mol/L is formed. Also provided are compositions formed by such processes, processes for forming catalyst compositions from these compositions, and catalyst compositions formed by these processes.
摘要翻译：本发明提供了形成溶液组合物的方法，该方法包括在水性介质中将i）至少一种磷化合物， ii）至少一种VI族金属化合物; 和iii）至少一种VIII族金属化合物，使得形成具有大于约5.6mol / L的VI族金属浓度的溶液。还提供了通过这些方法形成的组合物，由这些组合物形成催化剂组合物的方法，以及由这些方法形成的催化剂组合物。

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