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1. 发明申请

WO2010139755A1 PROCESS TO PREPARE A CHELATING AGENT OR PRECURSOR THEREOF USING A CYANIDE SALT 审中-公开
标题翻译：使用氰化物盐制备螯合剂或其前体的方法
公开(公告)号：WO2010139755A1
公开(公告)日：2010-12-09
申请号：PCT/EP2010/057776
申请日：2010-06-03
申请人： AKZO NOBEL CHEMICALS INTERNATIONAL B.V. , LAMMERS, Hans , HEUS, Martin , BOONSTRA, Tjerk Oedse , REICHWEIN, Adrianus Maria
发明人： LAMMERS, Hans , HEUS, Martin , BOONSTRA, Tjerk Oedse , REICHWEIN, Adrianus Maria
IPC分类号： C07C253/08 , C07C255/25 , C07C227/28 , C07C229/24
CPC分类号： C07C253/08 , C07C229/24 , C07C255/25
摘要： The present invention relates to a process comprising the reaction of a cyanide with an amino acid and an aldehyde, characterized in that the cyanide is a cyanide salt, the amino acid is aspartic acid and/or glutamic acid in the acidic form, and the process is performed under acidic pH by the addition of between 0 and 1 equivalent of an acid based on the amount of aspartic or glutamic acid.
摘要翻译：本发明涉及氰化物与氨基酸和醛的反应的方法，其特征在于氰化物是氰化物盐，氨基酸是酸性形式的天冬氨酸和/或谷氨酸，该方法通过加入基于天冬氨酸或谷氨酸的量的0至1当量的酸在酸性pH下进行。

2. 发明申请

WO2010139763A1 AN ELECTROCHEMICAL PROCESS TO PREPARE CHEMICALS USING A CYANIDE SALT 审中-公开
标题翻译：使用氰化物盐制备化学品的电化学工艺
公开(公告)号：WO2010139763A1
公开(公告)日：2010-12-09
申请号：PCT/EP2010/057788
申请日：2010-06-03
申请人： AKZO NOBEL CHEMICALS INTERNATIONAL B.V. , APPELMAN, Wilhelmus Joannes Theodorus Maria , LAMMERS, Hans , VOLMER, Arie , BOONSTRA, Tjerk Oedse , REICHWEIN, Adrianus Maria
发明人： APPELMAN, Wilhelmus Joannes Theodorus Maria , LAMMERS, Hans , VOLMER, Arie , BOONSTRA, Tjerk Oedse , REICHWEIN, Adrianus Maria
IPC分类号： C25B1/22 , C25B3/00 , B01D61/44 , B01D61/04 , C07C253/30
CPC分类号： C07C227/18 , B01D61/44 , C07C229/16
摘要： The present invention relates to a process comprising the reaction of a cyanide with a hydrogen cyanide-reactive compound, characterized in that the cyanide is a cyanide salt and the process is an electrochemical process involving the transporting of a reaction mixture to which cyanide salt has been added through an electrochemical cell, in which process the cyanide salt reacts with the hydrogen cyanide-reactive compound while at least partly under the influence of an electric current the cyanide salt is acidified and the salt cation content is reduced.
摘要翻译：本发明涉及一种包括氰化物与氰化氢反应性化合物的反应的方法，其特征在于氰化物是氰化物盐，该方法是一种电化学方法，涉及运输已经将氰化物盐的反应混合物通过电化学电池添加，其中氰化物盐与氰化氢反应性化合物反应，同时至少部分地在电流的影响下，氰化物盐被酸化并且盐阳离子含量降低。

3. 发明申请

WO2008065109A1 PROCESS TO PREPARE AMINO ACID-N, N-DIACETIC ACID COMPOUNDS 审中-公开
标题翻译：制备氨基酸-N，N-二酸化合物的方法
公开(公告)号：WO2008065109A1
公开(公告)日：2008-06-05
申请号：PCT/EP2007/062881
申请日：2007-11-27
申请人： Akzo Nobel N.V. , HEUS, Martin , LAMMERS, Hans , VOLMER, Arie
发明人： HEUS, Martin , LAMMERS, Hans , VOLMER, Arie
IPC分类号： C07C227/40 , C07C229/16 , C07C229/24 , B01D61/44
CPC分类号： C07C227/40 , B01D61/44 , C07C229/16 , C07C229/24
摘要： The invention relates to a process for the production of an amino acid having at least one secondary or tertiary amino group and three or more carboxyl groups or its salt with less than an equivalent of alkaline metal based on the number of carboxyl groups, said process comprising reducing alkali metal ions from an aqueous solution of an alkali metal salt of an amino acid having at least one secondary or tertiary amino group and three or more carboxyl groups and acidifying the amino carboxylate starting material by first performing a chemical acidification step using an organic or inorganic acid to get a compound in which at least one of the groups is protonated, and in a subsequent step further acidifying the amino carboxylate starting material and reducing alkali metal ions from an aqueous solution of the partially acidified alkali metal salt of the amino acid having at least one secondary or tertiary amino group and three or more carboxyl groups by electrodialysis, wherein the electrodialysis is performed using a hydrogen ion permselective membrane on the anode side and a cation-permeable membrane on the cathode side.
摘要翻译：本发明涉及一种制备具有至少一个仲氨基或叔氨基和三个或更多个羧基的氨基酸的方法或其盐，其基于羧基数目少于等于碱当量，所述方法包括从具有至少一个仲或叔氨基和三个或多个羧基的氨基酸的碱金属盐的水溶液中还原碱金属离子，并且通过首先使用有机或不饱和羧酸盐进行化学酸化步骤酸化氨基羧酸盐原料无机酸，得到其中至少一个基团被质子化的化合物，并且在随后的步骤中，进一步酸化氨基羧酸酯起始原料并从部分酸化的氨基酸的碱金属盐的水溶液中还原碱金属离子，其具有至少一个仲或叔氨基和三个或更多个羧基通过电渗析，其中选择使用阳极侧的氢离子选择性膜和阴极侧的阳离子透过膜进行透析。

4. 发明申请

WO2005014527A1 ANAQUEOUS SOLUTION OF A SODIUM SALT OF HEDTA 审中-公开
标题翻译： HEDTA钠盐的无效解决方案
公开(公告)号：WO2005014527A1
公开(公告)日：2005-02-17
申请号：PCT/EP2004/007841
申请日：2004-07-13
申请人： AKZO NOBEL N.V. , HEUS, Martin , LAMMERS, Hans , LEPAGE, Jim
发明人： HEUS, Martin , LAMMERS, Hans , LEPAGE, Jim
IPC分类号： C07C229/26
CPC分类号： B01D61/445 , C02F1/683 , C02F2101/203
摘要： The invention pertains to an aqueous solution of a sodium salt xNa + yH + of the chelating compound of formula (I): wherein x = 2.1 - 2.7, y = 0.9 - 0.3, and x + y = 3. The invention further pertains to a container comprising at least 0.5 kg of said aqueous solution and to a method of preparing an aqueous solution comprising at least 45wt% of the sodium salt xNa + yH + of the chelating compound of formula (I) from Na 3 -HEDTA, comprising the steps of electrodialysing an aqueous solution containing less than 42 wt% of Na 3 -HEDTA using a bipolar membrane, thereby converting the trisodium salt solution to the solution of the sodium salt of formula (I) with x = 2.1 - 2.7, y = 0.9 - 0.3, and x + y = 3.
摘要翻译：本发明涉及式（I）螯合化合物的钠盐x Na + yH +的水溶液：其中x = 2.1-2.7，y = 0.9-0.3，x + y = 3。本发明还涉及包含至少0.5kg所述水溶液的容器和制备包含至少45wt％的式（I）螯合化合物的钠盐x Na + yH +的水溶液的方法，包括以下步骤：使用双极膜电渗析含有少于42重量％的Na 3 -HEDTA的水溶液，由此将三钠盐溶液转化为式（I）的钠盐溶液，其中x = 2.1 -2.7，y = 0.9-0.3，x + y = 3。

5. 发明申请

WO2013144175A1 STABILIZATION OF AN AQUEOUS SOLUTION OF AN ORGANIC IRON SALT 审中-公开
标题翻译：有机铁盐水溶液的稳定性
公开(公告)号：WO2013144175A1
公开(公告)日：2013-10-03
申请号：PCT/EP2013/056459
申请日：2013-03-27
申请人： AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
发明人： LAMMERS, Hans , MEIJER, Johannes Albertus Maria
IPC分类号： C25B1/00 , C01D3/26
CPC分类号： C09K15/06 , C01D3/26 , C25B1/00 , C25B3/02 , C25B9/08
摘要： Process and station for stabilizing an aqueous solution of an iron salt of an organic acid with a ferric component and a ferrous component of less solubility than the ferric component, such as the aqueous solution based on the Fe 3+ salt of meso-tartaric acid. To stabilize the content of the dissolved ferric salt, the solution is at least partly subjected to electrolytic oxidation.
摘要翻译：稳定有机酸的铁盐水溶液的方法和工作站，其中含铁组分和比铁组分溶解度低的铁组分，例如基于内消旋酒石酸的Fe 3+盐的水溶液。为了稳定溶解的铁盐的含量，溶液至少部分地进行电解氧化。

6. 发明申请

WO2007131969A3 AN ELECTROCHEMICAL PROCESS TO PREPARE A HALOGENATED CARBONYL GROUP-CONTAINING COMPOUND 审中-公开
公开(公告)号：WO2007131969A3
公开(公告)日：2007-11-22
申请号：PCT/EP2007/054599
申请日：2007-05-11
申请人： AKZO NOBEL N.V. , LAMMERS, Hans , KOELEWIJN, Willem , SEETZ, Johannes Wilhelmus Franciscus Lucas , FABER, Joldert
发明人： LAMMERS, Hans , KOELEWIJN, Willem , SEETZ, Johannes Wilhelmus Franciscus Lucas , FABER, Joldert
IPC分类号： C25B3/06
摘要： The present invention provides a process to prepare a halogenated carbonyl group-containing compound by electrochemically reacting the corresponding carbonyl group-containing compound with a hydrogen halide H-X, an organic halide R'-X and/or a halide salt M n+ -X n - under substantially water-free conditions, wherein X is a chlorine, bromine or iodine atom, R' is an alkyl or aryl group that may be linear or branched, optionally containing one or more heteroatoms such as oxygen, nitrogen, chloride, bromide, fluoride or iodide of which the halogen atom X can be electrochemically split off, M n+ is a quaternary ammonium, alkaline earth metal, alkali metal or metal cation, and n is an integer of 1 to 5, depending on the valency of the metal cation M n+ .

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