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1. 发明申请

WO9318005A3 PROCESSES FOR PRODUCING 2-HALO-NICOTINIC ACID DERIVATIVES AND PRECURSORS THERETO 审中-公开
标题翻译：生产2-羟基丁酸酸衍生物及其前体的方法
公开(公告)号：WO9318005A3
公开(公告)日：1993-10-28
申请号：PCT/US9302117
申请日：1993-03-08
申请人： REILLY IND INC
发明人： ZHANG TONY Y , SCRIVEN ERIC F V
IPC分类号： C07B61/00 , C07C253/30 , C07C255/21 , C07D213/73 , C07D213/79 , C07D213/80 , C07D213/82
CPC分类号： C07D213/73 , C07D213/79 , C07D213/80 , C07D213/82
摘要： Disclosed are preferred processes for the preparation of 2-halo-nicotinic acid derivatives of formula (IV) by cyclocondensation of a 4-halo-4-cyanocarbonyl compound of formula (III) wherein X is Cl or Br; Y is a carbonyl group and R?1, R2 and R3¿ are each, independently, H, Cl, Br or an organic radical. Further preferred aspects include the preparation of the above-noted 4-halo-4-cyanocarbonyl compound via Michael addition of a 2-halonitrile with an α,β-unsaturated aldehyde or ketone, and the preparation of the 2-halonitrile by redistribution of halogen between a 2,2-dihalonitrile and a parent nitrile.

2. 发明申请

WO9207648A3 ELECTRO-SYNTHESIS OF ALCOHOLS AND CARBOXYLIC ACIDS FROM CORRESPONDING METAL SALTS 审中-公开
标题翻译：从相应的金属盐中电化学合成醇和羧酸
公开(公告)号：WO9207648A3
公开(公告)日：1992-11-26
申请号：PCT/US9107960
申请日：1991-10-28
申请人： REILLY IND INC
发明人： TOOMEY JOSEPH E
IPC分类号： B01D61/44 , C07C29/88 , C07C51/02 , C25B3/00
CPC分类号： C25B3/00 , B01D61/44 , C07C29/88 , C07C51/02 , Y02A20/134 , C07C31/22 , C07C31/245
摘要： A preferred electrochemical process for producing an alcohol or carboxylic acid from a corresponding metal salt while also recovering metal cation residues is described. The preferred process does not require a three-compartment desalination cell but rather can be performed in a standard two-compartment cell divided by a cation-permeable membrane. The process comprises the step of electrolyzing an aqueous medium containing the metal salt in the anolyte of the cell to thereby yield alcohol or carboxylic acid in the anolyte and pass the metal cation into the catholyte. In one particularly preferred mode, the process provides a highly effective recovery of valuable materials from byproduct streams of base-catalyzed syntheses of polyols such as such as trimethylolpropane or pentaerythritol from aldehydes, and in another provides an efficient recovery of phenol.
摘要翻译：描述了从相应金属盐生产醇或羧酸同时还回收金属阳离子残基的优选电化学方法。优选的方法不需要三室脱盐池，而是可以在由阳离子渗透膜分开的标准二室室中进行。该方法包括电解在电解池的阳极电解液中含有金属盐的含水介质，从而在阳极电解液中产生醇或羧酸并将金属阳离子送入阴极电解液的步骤。在一个特别优选的方式中，该方法从多元醇如三羟甲基丙烷或季戊四醇的碱催化合成的副产物流中从醛中高效回收有价值的物质，并且另一种方法提供苯酚的有效回收。

3. 发明申请

WO9003367A3 4-(N-BENZYL-N-METHYLAMINO)PYRIDINE ACID SALTS AND USE IN PREPARATION OF POLYMER-SUPPORTED CATALYSTS 审中-公开
标题翻译： 4-（N-苄基-N-甲基氨基）吡啶酸盐及其在制备聚合物载体催化剂中的应用
公开(公告)号：WO9003367A3
公开(公告)日：1990-05-17
申请号：PCT/US8904122
申请日：1989-09-21
申请人： REILLY IND INC
发明人： MCQUIGG DONALD W , SOWERS EDWARD E , GOE GERALD L , SCRIVEN ERIC F V , KEAY JAMES G
IPC分类号： B01J31/06 , C07D213/74 , C08F12/00 , C08F12/26 , C08F26/06 , C08F212/14 , C08F226/06 , C08F212/08
CPC分类号： C07D213/74 , C08F12/26
摘要： A cross-linked polymer-supported 4-(N-benzyl-N-methylamino)pyridine material and process for its preparation in high yield and having effective physical and catalytic properties. The polymer-supported catalyst is characterized by the suspension copolymerization of an organic phase containing the corresponding vinyl-substituted pyridine monomer, a styrene monomer, and a suitable cross-linking agent and free radical-generating catalyst in the presence of an aqueous phase containing a cellulose ether derivative as the stabilizing agent. A purified acid salt of the vinyl-substituted pyridine monomer useful in polymerizations and stable for storage as either a solid or an aqueous solution.
摘要翻译：一种交联聚合物负载的4-（N-苄基-N-甲基氨基）吡啶物质及其制备方法，其产率高，具有有效的物理和催化性能。聚合物负载型催化剂的特征在于含有相应的乙烯基取代的吡啶单体的有机相，苯乙烯单体和合适的交联剂和自由基生成催化剂的悬浮共聚合在含有纤维素醚衍生物作为稳定剂。用于聚合的乙烯基取代吡啶单体的纯化酸盐，作为固体或水溶液贮存稳定。

4. 发明申请

WO2006086602A2 IMPROVED PROCESS FOR THE PREPARATION OF 3,5-DIETHYL-1,2-DIHYDRO-1-PHENYL-2-PROPYLPYRIDINE 审中-公开
标题翻译：制备3,5-二乙基-1,2-二氢-1-苯基-2-丙酰基吡啶的改进方法
公开(公告)号：WO2006086602A2
公开(公告)日：2006-08-17
申请号：PCT/US2006004668
申请日：2006-02-10
申请人： REILLY IND INC , GRENDZE MARTIN , MURUGAN RAMIAH , HUCKSTEP L MARK , HOPPER CHARLES R
发明人： GRENDZE MARTIN , MURUGAN RAMIAH , HUCKSTEP L MARK , HOPPER CHARLES R
IPC分类号： C07D213/06
CPC分类号： C07D211/82
摘要： Methods are provided for improving production of 3,5-diethyl-l,2-dihydro-l-phenyl-2- propylpyridine (DHP). In one illustrative embodiment, the methods involve controlling the rate of reaction and temperature of the reaction during formation of DHP. In another illustrative embodiment, the methods involve neutralizing the acid catalyst subsequent to DHP formation.
摘要翻译：提供了用于改善3,5-二乙基-1,2-二氢-1-苯基-2-丙基吡啶（DHP）的生产的方法。在一个说明性实施方案中，所述方法包括在形成DHP期间控制反应速率和反应温度。在另一说明性实施方案中，所述方法包括在DHP形成之后中和酸催化剂。

5. 发明申请

WO9219596A3 PROCESSES FOR PRODUCING (ALPHA)-PYRIDYL CARBINOLS 审中-公开
标题翻译：生产（ALPHA） - 吡啶羧酸的方法
公开(公告)号：WO9219596A3
公开(公告)日：1993-04-29
申请号：PCT/US9203596
申请日：1992-04-29
申请人： GOE MARY ELLEN & LF , REILLY IND INC
发明人： MURUGAN RAMIAH , SCRIVEN ERIC F V , GOE GERALD L
IPC分类号： B01J23/44 , C07B61/00 , C07D211/22 , C07D213/30 , C07D213/38
CPC分类号： C07D213/30 , C07D211/22
摘要： Disclosed are preferred processes for producing α-2-pyridyl α-aryl carbinol or α-4-pyridyl α-aryl carbinol compounds.

6. 发明申请

WO9003368A3 POLYMER-SUPPORTED 4-(N-BENZYL-N-METHYLAMINO)PYRIDINE CATALYST AND PROCESS FOR SAME 审中-公开
标题翻译：聚合物支持的4-（N-苄基-N-甲基氨基）吡啶催化剂及其方法
公开(公告)号：WO9003368A3
公开(公告)日：1990-05-03
申请号：PCT/US8904131
申请日：1989-09-21
申请人： REILLY IND INC
发明人： MCQUIGG DONALD WAYNE , WEBB HEATHER KAY , SOWERS EDWARD E
IPC分类号： B01J31/06 , C07D213/74 , C08F2/08 , C08F12/00 , C08F26/06 , C08F212/14 , C08F226/06
CPC分类号： C07D213/74
摘要： A cross-linked polymer-supported 4-(N-benzyl-N-methylamino)pyridine material and process for its preparation in high yield and having effective physical and catalytic properties. The polymer-supported catalyst is characterized by the suspension copolymerization of an organic phase containing the corresponding vinyl-substituted pyridine monomer, a styrene monomer, and a suitable cross-linking agent and free radical-generating catalyst in the presence of an aqueous phase containing a cellulose ether derivative as the stabilizing agent. The catalyst is further characterized by its yield in excess of 90 % by weight and by its predominant and generally spherical and smooth bead form and substantially uniform size that is efficiently hard and durable and possesses sufficient catalytic activity for effective use in acylation, alkylation or other related reactions.

7. 发明申请

WO0012476A9 PROCESSES FOR PREPARING 2-PIPERIDINEETHANOL COMPOUNDS 审中-公开
标题翻译：制备2-哌啶乙醇化合物的方法
公开(公告)号：WO0012476A9
公开(公告)日：2000-10-05
申请号：PCT/US9919867
申请日：1999-08-27
申请人： REILLY IND INC , MEAGHER TIMOTHY P
发明人： MEAGHER TIMOTHY P
IPC分类号： C07D211/02 , C07D211/22
CPC分类号： C07D211/22 , C07D211/02
摘要： Described are preferred processes for producing 2-piperidineethanol compounds by hydrogenation of corresponding 2-pyridineethanol compounds. The preferred processes are conducted in the presence of an amine other than said reactant or product, and a hydrogenation catalyst preferably comprising a noble metal catalyst such as ruthenium or palladium or oxides thereof. The catalyst is preferably provided on a heterogeneous support, and most preferred processes are conducted using controlled temperature conditions and high levels of catalyst to minimize the formation of deleterious byproducts.
摘要翻译：描述了通过氢化相应的2-吡啶乙醇化合物生产2-哌啶乙醇化合物的优选方法。优选的方法在除所述反应物或产物以外的胺存在下进行，以及氢化催化剂优选包含贵金属催化剂如钌或钯或其氧化物。催化剂优选提供在非均相载体上，并且最优选的方法使用受控的温度条件和高水平的催化剂进行以使有害副产物的形成最小化。

8. 发明申请

WO2005016505A3 METHOD FOR THE MANUFACTURE OF CYANOPYRIDINES AND CATALYSTS SUITABLE THEREFOR 审中-公开
标题翻译：氰基吡啶的制备方法及其适用的催化剂
公开(公告)号：WO2005016505A3
公开(公告)日：2005-06-09
申请号：PCT/US2004024939
申请日：2004-07-30
申请人： REILLY IND INC , FISCHER ACHIM , MARTIN ANDREAS , LUCKE BERNHARD , KALEVARU VENKATA , WECKBECKER CHRISTOPH , HUTHMACHER KLAUS
发明人： FISCHER ACHIM , MARTIN ANDREAS , LUCKE BERNHARD , KALEVARU VENKATA , WECKBECKER CHRISTOPH , HUTHMACHER KLAUS
IPC分类号： B01J20060101 , B01J21/06 , B01J27/198 , B01J37/00 , C07D213/57 , C07D213/85
CPC分类号： C07D213/84 , B01J21/06 , B01J21/063 , B01J23/002 , B01J27/198 , B01J37/0009 , B01J37/0036 , B01J2523/00 , B01J2523/31 , B01J2523/51 , B01J2523/55
摘要： The invention relates to a method for the manufacture of cyanopyridines from methylpyridines by their conversion with ammonia and oxygen and catalysts suitable therefor which contain further transition metals in addition to vanadium and phosphorus.
摘要翻译：本发明涉及一种由甲基吡啶通过氨和氧转化而制备氰基吡啶的方法及其适用的催化剂，其中还含有除钒和磷之外的其它过渡金属。

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