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1. 发明申请

WO1997030120A1 AQUEOUS SILYLATED POLYMER CURABLE COMPOSITIONS 审中-公开
标题翻译：水性硅胶聚合物可固化组合物
公开(公告)号：WO1997030120A1
公开(公告)日：1997-08-21
申请号：PCT/US1996015733
申请日：1996-10-02
申请人： OSI SPECIALTIES, INC.
发明人： OSI SPECIALTIES, INC. , CHEN, Ming, J. , OSTERHOLTZ, Frederick, D.
IPC分类号： C08L83/04
CPC分类号： C09D143/04 , C08K5/57 , C08L101/10 , C09D201/10 , C08L43/04 , C08L2666/28
摘要： Curable composition comprising a stable, water dispersible, curable polymer containing a sterically hindered alkoxylated silane group at 0.1 to 75 weight percent of the total composition; a water dispersible or water soluble, hydrolytically stable organometallic catalyst, at 0.1 to 10 weight percent of the total composition; and water at 99.8 to 24.9 weight percent of the total composition are taught herein. These compositions are useful as adhesives, sealants and paints. The compositions have improved properties including solvent resistance, adhesion, hardness, abrasion resistance and mar resistance. Particular catalysts for use herein include dihydroxy bis [2-hydroxypropanato (2-)-O ,O ] titanate mixed titanium ortho ester complexes, acetylacetonate chelate, bis(ethyl-3-oxobutanolato-O ,O ) bis(2-propanolato) titanium, alkanolamine complex of titanium and mercaptoalcohol, mercaptide or sulfide forms of diorganotins having either a Sn-S or Sn=S bond.
摘要翻译：包含稳定的水分散性可固化聚合物的可固化组合物，其含有占总组合物重量百分比为0.1-75重量％的空间位阻烷氧基化硅烷基团; 水分散或水溶性，水解稳定的有机金属催化剂，占总组合物的0.1至10重量％并且在本文中教导了总组合物的99.8至24.9重量％的水。这些组合物可用作粘合剂，密封剂和油漆。该组合物具有改进的性能，包括耐溶剂性，粘合性，硬度，耐磨性和耐擦伤性。用于本文的具体催化剂包括二羟基双[2-羟基丙酸酯（2 - ） - O 1，O 2]钛酸酯混合的钛原酸酯络合物，乙酰丙酮化合物螯合物，双（乙基-3-氧代丁醇酯-O， O 3）双（2-丙醇）钛，钛和巯基醇的链烷醇胺络合物，巯基或硫化物形式的具有Sn-S或Sn = S键的二有机锡。

2. 发明申请

WO1997007165A1 STABLE SILANE COMPOSITIONS ON SILICA CARRIER 审中-公开
标题翻译：二氧化硅载体上稳定的硅烷组合物
公开(公告)号：WO1997007165A1
公开(公告)日：1997-02-27
申请号：PCT/US1996013250
申请日：1996-08-16
申请人： OSI SPECIALTIES, INC.
发明人： OSI SPECIALTIES, INC. , GUILLET, Antoine , GAUTHIER, Remy
IPC分类号： C08L83/16
CPC分类号： C08K9/06 , C08K3/36 , C08K5/5406 , C08K9/12 , C08L21/00
摘要： The present invention discloses blends of silanes and specific silicas, characterized in that when the blend is compounded into a rubber formulation even after 4 months of storage following formation of the blend, an unexpectedly high proportion of the silane present is available as a coupling and reinforcing agent for the rubber formulation. Over 80 % and even over 90 % of the silica can be extracted or desorbed from the blend even 4 months after formation of the blend, and rubber formulation properties indicate high availability of the silane for coupling and reinforcement.
摘要翻译：本发明公开了硅烷和特定二氧化硅的共混物，其特征在于，即使在共混物形成之后，即使在4个月的储存之后，当将共混物配混成橡胶配方时，出乎意料地高比例的硅烷可作为偶联和增强橡胶配方的代理。甚至在形成共混物后4个月，超过80％甚至超过90％的二氧化硅可以从共混物中萃取或解吸，而橡胶配方性能表明硅烷用于联结和增强的高可用性。

3. 发明申请

WO1995001412A1 EFFICIENT DIESEL FUEL ANTIFOAMS OF LOW SILICONE CONTENT 审中-公开
标题翻译：低硅含量的高效柴油燃料防腐
公开(公告)号：WO1995001412A1
公开(公告)日：1995-01-12
申请号：PCT/US1994006804
申请日：1994-06-15
申请人： OSI SPECIALTIES, INC.
发明人： OSI SPECIALTIES, INC. , GRABOWSKI, Wojciech
IPC分类号： C10L01/28
CPC分类号： C10L1/285 , B01D19/0409 , C08G77/46 , C10L1/143 , F02B3/06 , B01D19/0436
摘要： The present invention is a class of organosilicone terpolymers which may be used to abate the foaming of diesel fuel at silicon levels below 1.2 ppm. Said silicone terpolymers are modified alkyl phenol derivatives and polyethers grafted on a polysiloxane copolymer. Said polysiloxane terpolymer has a structure of MDxD*yD**zM, where M is O.5Si(CH3)3, D is an OSi(CH3)2, D* is OSi(CH3)R, R is a polyether, D** is OSi(CH3)R', R' is a phenol derivative x+y+z is 35-350, x/(y+z) is 3 to 6 and y/z is 0.25 to about 9.0.

4. 发明申请

WO1998014511A1 COMPOSITIONS OF EPOXYSILANE EMULSION ADDITIVES IN WATERBASED REACTIVE POLYMER DISPERSIONS AND METHODS OF PREPARATION 审中-公开
标题翻译：环氧树脂乳液添加剂在水溶性反应聚合物分散体中的组成及其制备方法
公开(公告)号：WO1998014511A1
公开(公告)日：1998-04-09
申请号：PCT/US1996015732
申请日：1996-10-02
申请人： OSI SPECIALTIES, INC.
发明人： OSI SPECIALTIES, INC. , OSTERHOLTZ, Frederick, D. , POHL, Eric, R. , CHEN, Ming, J. , CHAVES, Antonio
IPC分类号： C08K05/15
CPC分类号： C08K5/5435 , C09D133/064 , C09D183/06 , C08L2666/28 , C08L2666/04
摘要： The present invention provides stable epoxy silane emulsions and methods for the preparation of a stable epoxy-silane emulsions comprising: (I) a water insoluble or slightly soluble epoxysilane; (II) an emulsifier; (III) water; and (IV) a water dispersible polymer containing a functional group with an active hydrogen. Also provided are two part systems such that an epoxysilane emulsion comprising components (I)-(III) are combined and the component (IV) may be added upon use of components (I) to (III). Moreover, additional components (V), such as catalysts and pH buffers may be added. Said compositions may be used for, among other things, coatings, adhesives and sealants. The water dispersible or slightly soluble epoxy functional silane for use herein are of the general structure R aR bSi(OR )4-a-b where R is an epoxy substituted alkyl or aralkyl group, where the alkyl may have from four to thirty carbon atoms, R is an alkyl or alkoxy-substituted alkyl, aryl or aralkyl group having from two to ten carbon atoms, R is an alkyl group or alkoxy substituted alkyl, aryl or aralkyl group having from one to ten carbon atoms, a is one to three, and b is zero to two, with the proviso that a+b is 1, 2, or 3. R , R , and R group may be cyclic, branched or linear.
摘要翻译：本发明提供稳定的环氧硅烷乳液和制备稳定的环氧硅烷乳液的方法，包括：（I）水不溶性或微溶环氧硅烷; （II）乳化剂; （三）水; 和（IV）含有具有活性氢的官能团的水分散性聚合物。还提供了两部分系统，使得包含组分（I） - （III）的环氧硅烷乳液组合，并且组分（IV）可以在使用组分（I）至（III）时加入。此外，可以加入另外的组分（V），例如催化剂和pH缓冲剂。除其他外，所述组合物可用于涂料，粘合剂和密封剂。用于本文的水分散性或微溶性环氧官能化硅烷具有通式结构R 1 a R bSi（OR 3）4-ab，其中R 1是环烷基取代的烷基或芳烷基，其中烷基可以具有4至30个碳原子，R 3是具有2至10个碳原子的烷基或烷氧基取代的烷基，芳基或芳烷基，R 2是烷基或烷氧基取代的烷基，芳基或具有1至10个碳原子的芳烷基，a为1至3，b为0至2，条件是a + b为1,2或3.R 1，R 2和 R 3基可以是环状，支链或直链。

5. 发明申请

WO1998003574A1 FLUORINATED ORGANOSILICON COMPOUNDS AND PROCESS FOR THE PREPARATION THEREOF 审中-公开
标题翻译：氟化有机硅化合物及其制备方法
公开(公告)号：WO1998003574A1
公开(公告)日：1998-01-29
申请号：PCT/JP1997002449
申请日：1997-07-15
申请人： ASAHI GLASS COMPANY LTD. , OSI SPECIALTIES, INC. , FURUKAWA, Yutaka , KOTERA, Mami , KUMAI, Seisaku , RUCKLE, Robert, E., Jr. , MURPHY, Gerald, J.
发明人： ASAHI GLASS COMPANY LTD. , OSI SPECIALTIES, INC.
IPC分类号： C08G77/16
CPC分类号： C08G77/385 , C08G77/24 , C08G77/46
摘要： Fluorinated organosilicon compounds of general formula (1), useful as water- and oil-repellent and other various industrial materials required to exhibit stain resistance, mold release properties or various other performances, or as raw materials thereof. In the general formula (1), A is a specific organic group having a polyfluorohydrocarbon group; R and R are each independently a divalent organic group; R to R are each independently a monovalent organic group; a is an integer of 1 or above; and b is an integer of 0 or above.
摘要翻译：作为防水防油剂和其它各种工业用材料，具有抗污染性，脱模性，各种其他性能的通式（1）的氟化有机硅化合物或其原料。在通式（1）中，A 是具有多氟烃基的特定的有机基团; R 1和R 2各自独立地为二价有机基团; R 3至R 9各自独立地为一价有机基团; a为1以上的整数; b为0以上的整数。

6. 发明申请

WO1997015624A1 AQUEOUS SILYLATED POLYMER CURABLE COMPOSITIONS 审中-公开
标题翻译：水性硅胶聚合物可固化组合物
公开(公告)号：WO1997015624A1
公开(公告)日：1997-05-01
申请号：PCT/US1996016776
申请日：1996-10-18
申请人： OSi SPECIALTIES, INC.
发明人： OSi SPECIALTIES, INC. , CHEN, Ming, J. , OSTERHOLTZ, Frederick, D.
IPC分类号： C08L43/04
CPC分类号： C08L101/10 , C08L43/04 , C09D201/10 , C08L2666/28
摘要： Curable compositions comprising stable, water dispersible, curable polymers containing sterically hindered alkoxylated silane groups and acid groups blocked by fugitive bases at 0.1 to 75 weight percent of the total composition and water at 99.9 to 25 weight percent of the total composition are taught herein, as well as methods for the use and manufacture thereof. Additional components, such as emulsifiers, buffers and thickeners are also taught. These compositions are useful as adhesives, sealants and paints. The compositions have improved properties including solvent resistance, adhesion, hardness, abrasion resistance and mar resistance.
摘要翻译：包含稳定的水分散性固化性聚合物，其含有空间位阻烷氧基化硅烷基团和酸性基团，以总组合物的0.1至75重量％和水为总组合物的99.9至25重量％以及其使用和制造方法。还教导了其它组分，如乳化剂，缓冲剂和增稠剂。这些组合物可用作粘合剂，密封剂和涂料。该组合物具有改进的性能，包括耐溶剂性，粘合性，硬度，耐磨性和耐擦伤性。

7. 发明申请

WO1997010277A1 SILICONE SURFACTANTS FOR USE IN INERT GAS BLOWN POLYURETHANE FOAMS 审中-公开
标题翻译：硅胶表面活性剂用于燃烧气体聚氨酯泡沫
公开(公告)号：WO1997010277A1
公开(公告)日：1997-03-20
申请号：PCT/US1996014683
申请日：1996-09-11
申请人： OSI SPECIALTIES, INC.
发明人： OSI SPECIALTIES, INC. , GERKIN, Richard, M. , HARAKAL, Mark, E. , LAWLER, Lee, F. , MILLER, Glenn, A.
IPC分类号： C08G18/61
CPC分类号： C08J9/122 , C08J9/0061 , C08J2375/04 , C08J2483/00
摘要： It has now been found that the use of inert gases as an auxiliary blowing agent in flexible polyurethane foams places unexpected requirements on the composition of the silicone surfactants used in such foams. Typical silicone polyalkylene oxide polyether copolymer comb-type surfactants containing greater than about 37 % ethylene oxide in the pendant polyether chains cause large cells when added inert gas is used as the blowing agent.
摘要翻译：现在已经发现，在柔性聚氨酯泡沫中使用惰性气体作为辅助发泡剂使得对这种泡沫体中使用的硅氧烷表面活性剂的组成有意想不到的要求。含有大于约37％环氧乙烷的典型的聚硅氧烷聚环氧烷聚醚共聚物梳型表面活性剂，当加入惰性气体作为发泡剂时，在侧链聚醚链中引起大量的细胞。

8. 发明申请

WO1996040613A1 PROCESS FOR THE PREPARATION OF TERTIARY AMINOCARBONATES AND AMINOETHERS 审中-公开
标题翻译：制备仲胺和氨基甲酸酯的方法
公开(公告)号：WO1996040613A1
公开(公告)日：1996-12-19
申请号：PCT/US1996008682
申请日：1996-06-07
申请人： OSi SPECIALTIES, INC.
发明人： OSi SPECIALTIES, INC. , BASTRON, Victor
IPC分类号： C07C68/06
CPC分类号： C07C213/06
摘要： The invention relates to processes for producing di-(tertiary aminoalkyl) carbonate including the step of reacting a tertiary alkanolamine with methyl alkyl carbonate in the presence of a transesterification catalyst to form tertiary aminoalkyl alkyl carbonate, wherein some of the tertiary alkanolamine reacts with the tertiary aminoalkyl alkyl carbonate to form di-(tertiary aminoalkyl) carbonate. The invention also relates to processes for producing di-(tertiary aminoalkyl) carbonate including the steps of (i) reacting dimethyl carbonate with an alcohol in the presence of a transesterification catalyst to form a methyl alkyl carbonate, and (ii) reacting a tertiary alkanolamine with the methyl alkyl carbonate formed in step (i) in the presence of a transesterification catalyst to form tertiary aminoalkylalkyl carbonate, wherein some of the tertiary alkanolamine reacts with the tertiary aminoalkyl alkyl carbonate to form di-(tertiary aminoalkyl) carbonate.
摘要翻译：本发明涉及生产碳酸二（叔氨基烷基）酯的方法，其包括在酯交换催化剂存在下使叔链烷醇胺与碳酸甲基烷基酯反应以形成叔氨基烷基碳酸烷基酯的步骤，其中一些叔链烷醇胺与三氨基烷基碳酸酯以形成碳酸二（叔氨基烷基）酯。本发明还涉及生产碳酸二（叔氨基烷基）酯的方法，包括以下步骤：（i）在酯交换催化剂存在下使碳酸二甲酯与醇反应，形成碳酸甲基烷基酯，和（ⅱ）使叔链烷醇胺与步骤（i）中形成的碳酸甲基烷基酯在酯交换催化剂的存在下形成叔氨基烷基烷基碳酸酯，其中一些叔链烷醇胺与碳酸叔氨基烷基酯反应形成碳酸二（叔氨基烷基）酯。

9. 发明申请

WO1994022311A1 SUPER-SPREADING, LOW-FOAM SURFACTANT FOR AGRICULTURAL SPRAY MIXTURES 审中-公开
标题翻译：超级膨胀，农用喷雾混合物的低泡表面活性剂
公开(公告)号：WO1994022311A1
公开(公告)日：1994-10-13
申请号：PCT/US1994003523
申请日：1994-03-30
申请人： OSI SPECIALTIES, INC. , MURPHY, Dennis, Stephen
发明人： OSI SPECIALTIES, INC.
IPC分类号： A01N55/00
CPC分类号： A01N25/30 , A01N55/00 , A01N57/20 , A01N45/00 , A01N43/40 , A01N2300/00
摘要： Methods for preparing and applying superspreading agricultural sprays without undue foaming of the spray mixture employ a superspread-promoting, low-foaming trisiloxane surfactant. Agricultural spray mixtures with superspread properties, but limited foaming, comprise (A) a superspreading, low-foaming trisiloxane surfactant and (B) an agricultural chemical spray mixture comprising water, an agricultural chemical (e.g., a pesticide), and optionally an organic surfactant, antifoam agent, and an organic solvent.
摘要翻译：制备和应用超喷涂农用喷雾剂的方法，其喷雾混合物没有不适当的起泡使用超广泛促进的低发泡三硅氧烷表面活性剂。具有超广泛性能但有限发泡的农业喷雾混合物包含（A）超扩展，低发泡三硅氧烷表面活性剂和（B）农药化学喷雾混合物，其包含水，农药（例如农药）和任选的有机表面活性剂，消泡剂和有机溶剂。

10. 发明申请

WO1997012940A1 AQUEOUS CURABLE SILANE/POLYMER COMPOSITIONS 审中-公开
标题翻译：水性可固化硅烷/聚合物组合物
公开(公告)号：WO1997012940A1
公开(公告)日：1997-04-10
申请号：PCT/US1996016064
申请日：1996-10-07
申请人： OSi SPECIALTIES, INC.
发明人： OSi SPECIALTIES, INC. , CHEN, Ming, J. , OSTERHOLTZ, Frederick, D. , POHL, Eric, R. , CHAVES, Antonio , RAMADATT, Phil, E.
IPC分类号： C08L83/04
CPC分类号： C09D143/04 , C08K5/5415 , C09D167/00 , C09D201/10 , C08L43/04 , C08L2666/44 , C08L2666/28
摘要： The present invention provides stable alkoxy silane containing compositions and methods for the preparation of a stable silane containing composition comprising: (I) a water insoluble or slightly soluble alkoxy silane; (II) emulsifier; (III) water; and (IV) water dispersible or emulsified polymer containing an alkoxy silane functional group. Also provided are two part systems such that an alkoxy silane emulsion comprising components (I)-(III) are combined and the component (IV) may be added upon use of components (I) to (III). Moreover, additional components (V) such as catalysts and pH buffers may be added. The compositions of the present invention are stable for at least about three to twelve months.
摘要翻译：本发明提供了稳定的含烷氧基硅烷的组合物和制备稳定的含硅烷的组合物的方法，包括：（I）水不溶性或微溶性烷氧基硅烷; （II）乳化剂; （三）水; 和（IV）含有烷氧基硅烷官能团的水分散性或乳化性聚合物。还提供了两部分体系，使得包含组分（I） - （III）的烷氧基硅烷乳液合并，并且组分（IV）可以在使用组分（I）至（III）时加入。此外，可以加入另外的组分（V）如催化剂和pH缓冲剂。本发明的组合物稳定至少约三至十二个月。

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