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1. 发明申请

WO2004005402A1 GRAFT COPOLYMERS 审中-公开
标题翻译： GRAFT共聚物
公开(公告)号：WO2004005402A1
公开(公告)日：2004-01-15
申请号：PCT/US2003/020968
申请日：2003-07-03
申请人： MASSACHUSETTS INSTITUTE OF TECHNOLOGY , PARK, Jane, Y. , ACAR, Metin , AKTHAKUL, Ariya , MAYES, Anne, M.
发明人： PARK, Jane, Y. , ACAR, Metin , AKTHAKUL, Ariya , MAYES, Anne, M.
IPC分类号： C08L71/02
CPC分类号： C08L71/02 , C08F265/04 , C08F273/00 , C08F289/00 , C08F297/02 , C08G81/00 , C08J5/18 , C08J2381/06 , C08L51/003 , C08L51/08 , C08L81/06 , C08L81/00 , C08L2666/22 , C08L2666/02
摘要： This invention relates to methods of making graft copolymers, and articles having such graft copolymers. The methods may provide better control than in radicalization or photoinitiated polymerization techniques. For example, a graft copolymer can be prepared by reacting an alkoxide ion with a polymer. The alkoxide, in turn, can be provided by any suitable technique, for example, by reacting an alcohol with a base. In some embodiments of the invention, the graft copolymers may be a normally hydrophobic polymer, such as a polysulfone, that has been made more hydrophilic due to the attachment of hydrophilic side groups such as polyethylene glycol or polypropylene glycol. The copolymers of the invention have many uses, for example, in films or porous membranes.
摘要翻译：本发明涉及制备接枝共聚物的方法和具有这种接枝共聚物的制品。该方法可以提供比在自由基化或光引发聚合技术更好的控制。例如，可以通过使醇盐离子与聚合物反应来制备接枝共聚物。醇盐又可以通过任何合适的技术提供，例如通过使醇与碱反应。在本发明的一些实施方案中，接枝共聚物可以是通常疏水的聚合物，例如聚砜，由于亲水性侧基如聚乙二醇或聚丙二醇的附着而使其变得更亲水。本发明的共聚物在膜或多孔膜中具有许多用途。

2. 发明申请

WO1998016960A2 POLYMER ELECTROLYTE, INTERCALATION COMPOUNDS AND ELECTRODES FOR BATTERIES 审中-公开
标题翻译：聚合物电解质，电介质化合物和电极
公开(公告)号：WO1998016960A2
公开(公告)日：1998-04-23
申请号：PCT/US1997018839
申请日：1997-10-10
申请人： MASSACHUSETTS INSTITUTE OF TECHNOLOGY , MAYES, Anne, M. , CEDER, Gerbrand , CHIANG, Yet-Ming , SADOWAY, Donald, R. , AYDINOL, Mehmet, K. , SOO, Philip, P. , JANG, Young-Il , HUANG, Biying
发明人： MASSACHUSETTS INSTITUTE OF TECHNOLOGY
IPC分类号： H01M06/00
CPC分类号： H01M4/133 , C01B13/14 , C01D15/02 , C01G45/1228 , C01G51/42 , C01G53/42 , C01P2002/02 , C01P2002/08 , C01P2002/20 , C01P2002/30 , C01P2002/52 , C01P2002/54 , C01P2002/72 , C01P2004/04 , C01P2006/40 , C01P2006/80 , H01B1/122 , H01M4/13 , H01M4/131 , H01M4/362 , H01M4/382 , H01M4/485 , H01M4/505 , H01M4/525 , H01M4/624 , H01M10/052 , H01M10/0525 , H01M10/0565 , H01M2300/0085 , H01M2300/0091 , Y10T428/31 , Y10T428/31935
摘要： Solid battery components are provided. A block copolymeric electrolyte is non-cross-linked and non-glassy through the entire range of typical battery service temperatures, that is, through the entire range of at least from about 0 DEG C to about 70 DEG C. The chains of which the copolymer is made each include at least one ionically-conductive block and at least one second block immiscible with the ionically-conductive block. The chains form an amorphous association and are arranged in an ordered nanostructure including a continuous matrix of amorphous ionically-conductive domains and amorphous second domains that are immiscible with the ionically-conductive domains. A compound is provided that has a formula of LixMyNzO2. M and N are each metal atoms or a main group elements, and x, y, and z are each numbers from about 0 to about 1. y and z are chosen such that a formal charge on the My, Nz portion of the compound is (4-x). In certain embodiments, these compounds are used in the cathodes of rechargeable batteries. The present invention also includes methods of predicting the potential utility of metal dichalcogenide compounds for use in lithium intercalation compounds. It also provides methods for processing lithium intercalation oxides with the structure and compositional homogeneity necessary to realize the increased formation energies of said compounds. An article is made of a dimensionally-stable, interpenetrating microstructure of a first phase including a first component and a second phase, immiscible with the first phase, including a second component. The first and second phases define interphase boundaries between the, and at least one particle is positioned between a first phase and a second phase at an interphase boundary. When the first and second phases are electronically-conductive and ionically-conductive polymers, respectively, and the particles are ion host particles, the arrangement is an electrode of a battery.
摘要翻译：提供固体电池组件。嵌段共聚物电解质在典型的电池使用温度的整个范围内，即在至少约0℃至约70℃的整个范围内是非交联和非玻璃化的。共聚物各自包含至少一个离子导电嵌段和至少一个与离子导电嵌段不混溶的第二嵌段。链形成无定形关联并且被布置在有序纳米结构中，包括非晶离子导电畴的连续矩阵和与离子导电畴不混溶的无定形第二结构域。提供了具有式LixMyNzO2的化合物。 M和N分别是金属原子或主要元素，x，y和z各自为约0至约1的数，y和z被选择为使得化合物的My，Nz部分上的正电荷为（4-x）的。在某些实施方案中，这些化合物用于可再充电电池的阴极中。本发明还包括预测金属二硫属化合物在锂嵌入化合物中的潜在用途的方法。它还提供了处理锂嵌入氧化物的方法，其具有实现所述化合物的增加的形成能所必需的结构和组成均匀性。一种制品由包括第一组分和第二相的第一相的尺寸稳定的互穿微结构制成，该第一相与第一相不混溶，包括第二组分。第一阶段和第二阶段限定了相间边界，并且至少一个粒子位于相间边界处的第一阶段和第二阶段之间。当第一相和第二相分别是电子导电和离子导电聚合物，并且颗粒是离子主体颗粒时，排列是电池的电极。

3. 发明申请

WO9816960A3 POLYMER ELECTROLYTE, INTERCALATION COMPOUNDS AND ELECTRODES FOR BATTERIES 审中-公开
标题翻译：聚合物电解质，电介质化合物和电极
公开(公告)号：WO9816960A3
公开(公告)日：2001-06-28
申请号：PCT/US9718839
申请日：1997-10-10
申请人： MASSACHUSETTS INST TECHNOLOGY , MAYES ANNE M , CEDER GERBRAND , CHIANG YET MING , SADOWAY DONALD R , AYDINOL MEHMET K , SOO PHILIP P , JANG YOUNG IL , HUANG BIYING
发明人： MAYES ANNE M , CEDER GERBRAND , CHIANG YET-MING , SADOWAY DONALD R , AYDINOL MEHMET K , SOO PHILIP P , JANG YOUNG-IL , HUANG BIYING
IPC分类号： C01G53/00 , C01G45/00 , C01G51/00 , H01B1/12 , H01M4/13 , H01M4/133 , H01M4/48 , H01M4/485 , H01M4/50 , H01M4/505 , H01M4/52 , H01M4/525 , H01M6/00 , H01M10/052 , H01M10/0525 , H01M10/0565 , H01M10/36 , H01M4/02 , H01M6/18
CPC分类号： H01M4/133 , C01B13/14 , C01D15/02 , C01G45/1228 , C01G51/42 , C01G53/42 , C01P2002/02 , C01P2002/08 , C01P2002/20 , C01P2002/30 , C01P2002/52 , C01P2002/54 , C01P2002/72 , C01P2004/04 , C01P2006/40 , C01P2006/80 , H01B1/122 , H01M4/13 , H01M4/131 , H01M4/362 , H01M4/382 , H01M4/485 , H01M4/505 , H01M4/525 , H01M4/624 , H01M10/052 , H01M10/0525 , H01M10/0565 , H01M2300/0085 , H01M2300/0091 , Y10T428/31 , Y10T428/31935
摘要： Solid battery components are provided. A block copolymeric electrolyte is non-cross-linked and non-glassy through the entire range of typical battery service temperatures, that is, through the entire range of at least from about 0 DEG C to about 70 DEG C. The chains of which the copolymer is made each include at least one ionically-conductive block and at least one second block immiscible with the ionically-conductive block. The chains form an amorphous association and are arranged in an ordered nanostructure including a continuous matrix of amorphous ionically-conductive domains and amorphous second domains that are immiscible with the ionically-conductive domains. A compound is provided that has a formula of LixMyNzO2. M and N are each metal atoms or a main group elements, and x, y, and z are each numbers from about 0 to about 1. y and z are chosen such that a formal charge on the My, Nz portion of the compound is (4-x). In certain embodiments, these compounds are used in the cathodes of rechargeable batteries. The present invention also includes methods of predicting the potential utility of metal dichalcogenide compounds for use in lithium intercalation compounds. It also provides methods for processing lithium intercalation oxides with the structure and compositional homogeneity necessary to realize the increased formation energies of said compounds. An article is made of a dimensionally-stable, interpenetrating microstructure of a first phase including a first component and a second phase, immiscible with the first phase, including a second component. The first and second phases define interphase boundaries between the, and at least one particle is positioned between a first phase and a second phase at an interphase boundary. When the first and second phases are electronically-conductive and ionically-conductive polymers, respectively, and the particles are ion host particles, the arrangement is an electrode of a battery.
摘要翻译：提供固体电池组件。嵌段共聚物电解质在典型的电池使用温度的整个范围内，即在至少约0℃至约70℃的整个范围内是非交联和非玻璃化的。共聚物各自包含至少一个离子导电嵌段和至少一个与离子导电嵌段不混溶的第二嵌段。链形成无定形关联并且被布置在有序纳米结构中，包括非晶离子导电畴的连续矩阵和与离子导电畴不混溶的无定形第二结构域。提供了具有式LixMyNzO2的化合物。 M和N分别是金属原子或主要元素，x，y和z各自为约0至约1的数。y和z被选择为使得化合物的My，Nz部分上的正电荷为（4-x）的。在某些实施方案中，这些化合物用于可再充电电池的阴极中。本发明还包括预测金属二硫属化合物在锂嵌入化合物中的潜在用途的方法。它还提供了处理锂嵌入氧化物的方法，其具有实现所述化合物的增加的形成能所必需的结构和组成均匀性。制品由第一相的尺寸稳定的互穿微结构构成，第一相包括与第一相不混溶的第一组分和第二相，包括第二组分。第一和第二阶段限定了相间界限，并且至少一个粒子位于相间边界处的第一相和第二相之间。当第一相和第二相分别是电子导电和离子导电聚合物，并且颗粒是离子主体颗粒时，排列是电池的电极。

4. 发明申请

WO1998008595A2 POLYMERIC MEMBRANES AND POLYMER ARTICLES HAVING HYDROPHILIC SURFACE AND METHOD FOR THEIR PREPARATION 审中-公开
标题翻译：具有水解表面的聚合物膜和聚合物及其制备方法
公开(公告)号：WO1998008595A2
公开(公告)日：1998-03-05
申请号：PCT/US1997016488
申请日：1997-08-26
申请人： MASSACHUSETTS INSTITUTE OF TECHNOLOGY , MAYES, Anne, M. , WALTON, David, G. , HESTER, Jonathan, F.
发明人： MASSACHUSETTS INSTITUTE OF TECHNOLOGY
IPC分类号： B01D67/00
CPC分类号： C08J3/005 , B01D67/0011 , B01D69/141 , B01D71/34 , B01D71/40 , B01D71/82 , B01D2323/12 , B01D2323/30 , B01D2325/38 , B01J45/00 , Y10T428/24942 , Y10T428/249953 , Y10T428/249961 , Y10T428/249978 , Y10T428/31 , Y10T428/31928 , Y10T428/31935
摘要： Polymeric articles, including membranes, with surfaces having a desired chemical functionality are created by surface segregation of a branched component blended with a compatible, matrix base component, the branched component having the desired chemical functionality. In particular, hydrophilic surfaces are created via surface segregation of a branched hydrophilic copolymer blended into a polymer matrix. The use of branched molecular architecture provides a thermodynamic mechanism for the segregation of the hydrophilic species to the surface and a means for achieving a high surface coverage of the hydrophilic moiety. The branched hydrophilic copolymer can be defined by a random copolymer including two or more methacrylate or acrylate monomers, at least one of which features a short hydrophilic side chain, such as a polyethylene glycol side chain. The branched hydrophilic copolymer is compatible, and well-entangled, with the acrylate polymer matrix.
摘要翻译：通过与相容的基质基质组分共混的支化组分的表面分离产生具有所需化学官能度的表面的聚合制品，包括膜，所述支化组分具有所需的化学官能度。特别地，亲水性表面是通过共聚到聚合物基质中的支化亲水共聚物的表面偏析产生的。支链分子结构的使用为亲水性物质与表面的分离提供了一种热力学机制，也是实现亲水部分高表面覆盖度的手段。支链亲水共聚物可以通过包括两种或更多种甲基丙烯酸酯或丙烯酸酯单体的无规共聚物来限定，其中至少一种具有短亲水侧链如聚乙二醇侧链。支链亲水共聚物与丙烯酸酯聚合物基质相容并且良好缠结。

5. 发明申请

WO2004063271A2 STRUCTURED BAROPLASTIC MATERIALS 审中-公开
标题翻译：结构化的塑性材料
公开(公告)号：WO2004063271A2
公开(公告)日：2004-07-29
申请号：PCT/US2004/000334
申请日：2004-01-07
申请人： MASSACHUSETTS INSTITUTE OF TECHNOLOGY , MAYES, Anne, M. , RYU, Sang, Woog , ACAR, Metin, H. , GONZALEZ, Juan, A.
发明人： MAYES, Anne, M. , RYU, Sang, Woog , ACAR, Metin, H. , GONZALEZ, Juan, A.
IPC分类号： C08L
CPC分类号： C08L51/003 , B29C43/006 , B29C47/0016 , B29C47/04 , B29K2105/162 , B82Y30/00 , C08F257/02 , C08F265/04 , C08F265/06 , C08F285/00 , C08F287/00 , C08F293/005 , C08J3/005 , C08J3/126 , C08J5/18 , C08L51/006 , C08L53/00 , Y10T428/2929 , C08L2666/02
摘要： The present invention provides a series of baroplastic materials, and systems and methods of making and using such baroplastic materials. In one aspect of the invention, polymeric particles are provided that can be used to produce baroplastic materials under certain pressures and/or below certain temperatures. In one set of embodiments, the polymeric particles include an inner "core" region and an outer "shell" region. In some cases, more than one "shell" region may be present. In another arrangement the particles can include materials, or domains, in nanoscale proximity with each other. Non-particulate materials can also be processed in accordance with the invention. In another aspect of the invention, the invention provides for polymeric particles that can be processed and/or recycled multiple times, without causing significant degradation or alteration in the physical and/or chemical properties of the polymer. In yet another aspect, the invention provides compositions able to form baroplastic materials upon the application of certain pressures, where the composition includes at least two chemically distinct materials in nanoscale proximity to each other. In still another aspect of the invention, a method of mixing two polymers upon the application of pressure is provided.
摘要翻译：本发明提供了一系列的压塑材料，以及制造和使用这种压塑材料的系统和方法。在本发明的一个方面中，提供了可在一定压力和/或低于特定温度下用于生产压塑材料的聚合物颗粒。在一组实施例中，聚合物颗粒包括内部“芯” 区域和外部“壳” 地区。在一些情况下，多于一个的“壳” 区域可能存在。在另一种布置中，颗粒可以包括彼此纳米级接近的材料或区域。根据本发明也可以处理非颗粒材料。在本发明的另一方面，本发明提供了可以多次加工和/或再循环的聚合物颗粒，而不引起聚合物的物理和/或化学性质的显着降解或改变。在又一个方面，本发明提供了能够在施加一定压力时形成压塑材料的组合物，其中所述组合物包含至少两种化学上不同的纳米级彼此接近的材料。在本发明的另一方面，提供了一种在施加压力时混合两种聚合物的方法。

6. 发明申请

WO2007120631A1 FOULING RESISTANT MEMBRANES FORMED WITH POLYACRYLONITRILE GRAFT COPOLYMERS 审中-公开
标题翻译：用聚丙烯酰胺共聚物形成的防粘膜
公开(公告)号：WO2007120631A1
公开(公告)日：2007-10-25
申请号：PCT/US2007/008797
申请日：2007-04-10
申请人： MASSACHUSETTS INSTITUTE OF TECHNOLOGY , MAYES, Anne, M. , ASATEKIN, Ayse
发明人： MAYES, Anne, M. , ASATEKIN, Ayse
IPC分类号： B01D71/42 , B01D71/82
CPC分类号： B01D65/08 , B01D61/145 , B01D61/147 , B01D67/0093 , B01D69/02 , B01D71/42 , B01D71/78 , B01D2321/16 , B01D2323/02 , B01D2323/38 , B01D2325/20 , B01D2325/36
摘要： The present application is generally directed towards polyacrylonitrile- (PAN-) based, amphophilic graft copolymers, for example, for the production of membranes for liquid filtration. In one aspect, the present invention provides systems and methods for preparing high flux, fouling resistant nanofiltration membranes whose pore size can be readily tuned. In some cases, microphase separation of a graft copolymer comprising a backbone comprising polyacrylonitrile (PAN) and hydrophilic side-chains is used. In some cases, nanochannels of tunable width are formed, which may give the membrane permselective properties and/or anti-fouling character. In some cases, a copoylmer may be used as an additive in the immersion precipitation casting of ultrafiltration or microfiltration membranes. In certain instances, the additive can segregate to the membrane exterior and/or pore surfaces, e.g., due to favorable interactions between the hydrophilic side chains and the surrounding environment, which may create a surface that resists fouling, e.g., by biological molecules.
摘要翻译：本申请一般针对基于聚丙烯腈（PAN-）的两亲接枝共聚物，例如用于生产用于液体过滤的膜。一方面，本发明提供了制备高通量，耐污垢的纳滤膜的系统和方法，其孔径可以容易地调节。在一些情况下，使用包含包含聚丙烯腈（PAN）和亲水侧链的骨架的接枝共聚物的微相分离。在某些情况下，可形成可调宽度的纳米通道，这可以提供膜选择性和/或抗结垢特性。在一些情况下，可以在超滤或微滤膜的浸渍沉淀浇铸中使用共酰基树脂作为添加剂。在某些情况下，例如由于亲水性侧链和周围环境之间的有利相互作用，添加剂可以分离到膜外部和/或孔表面，这可能产生例如通过生物分子阻止结垢的表面。

7. 发明申请

WO2004063271A3 STRUCTURED BAROPLASTIC MATERIALS 审中-公开
标题翻译：结构化的材料
公开(公告)号：WO2004063271A3
公开(公告)日：2004-09-30
申请号：PCT/US2004000334
申请日：2004-01-07
申请人： MASSACHUSETTS INST TECHNOLOGY , MAYES ANNE M , RYU SANG WOOG , ACAR METIN H , GONZALEZ JUAN A
发明人： MAYES ANNE M , RYU SANG WOOG , ACAR METIN H , GONZALEZ JUAN A
IPC分类号： C08F257/02 , C08F265/04 , C08F265/06 , C08F285/00 , C08F287/00 , C08F293/00 , C08L20060101 , C08L9/06 , C08L25/00 , C08L47/00 , C08L51/00 , C08L53/00
CPC分类号： C08L51/003 , B29C43/006 , B29C47/0016 , B29C47/04 , B29K2105/162 , B82Y30/00 , C08F257/02 , C08F265/04 , C08F265/06 , C08F285/00 , C08F287/00 , C08F293/005 , C08J3/005 , C08J3/126 , C08J5/18 , C08L51/006 , C08L53/00 , Y10T428/2929 , C08L2666/02
摘要： The present invention provides a series of baroplastic materials, and systems and methods of making and using such baroplastic materials. In one aspect of the invention, polymeric particles are provided that can be used to produce baroplastic materials under certain pressures and/or below certain temperatures. In one set of embodiments, the polymeric particles include an inner "core" region and an outer "shell" region. In some cases, more than one "shell" region may be present. In another arrangement the particles can include materials, or domains, in nanoscale proximity with each other. Non-particulate materials can also be processed in accordance with the invention. In another aspect of the invention, the invention provides for polymeric particles that can be processed and/or recycled multiple times, without causing significant degradation or alteration in the physical and/or chemical properties of the polymer. In yet another aspect, the invention provides compositions able to form baroplastic materials upon the application of certain pressures, where the composition includes at least two chemically distinct materials in nanoscale proximity to each other. In still another aspect of the invention, a method of mixing two polymers upon the application of pressure is provided.
摘要翻译：本发明提供了一系列的压延材料，以及制造和使用这种压延材料的系统和方法。在本发明的一个方面，提供聚合物颗粒，其可用于在某些压力和/或低于某些温度下制备压延材料。在一组实施方案中，聚合物颗粒包括内部“芯”区域和外部“壳”区域。在某些情况下，可能存在多于一个“壳”区域。在另一种布置中，颗粒可以包括纳米级彼此接近的材料或结构域。也可以根据本发明加工非颗粒材料。在本发明的另一方面，本发明提供可以多次加工和/或回收的聚合物颗粒，而不会导致聚合物的物理和/或化学性质的明显降解或改变。在另一方面，本发明提供了能够在施加某些压力时形成压延材料的组合物，其中所述组合物包含至少两种在纳米级彼此接近的化学上不同的材料。在本发明的另一方面，提供了在施加压力时混合两种聚合物的方法。

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