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1. 发明申请

WO2015195149A1 INTEGRATED PROCESS FOR CO-PRODUCTION OF CARBOXYLIC ACIDS AND HALOGEN PRODUCTS FROM CARBON DIOXIDE 审中-公开
标题翻译：从二氧化碳共同生产羧酸和卤素产物的综合方法
公开(公告)号：WO2015195149A1
公开(公告)日：2015-12-23
申请号：PCT/US2014/046555
申请日：2014-07-14
申请人： LIQUID LIGHT, INC
发明人： KACZIR, Jerry, J. , LAKKARAJU, Prasad
IPC分类号： C07C51/02
CPC分类号： C25B3/04 , C25B1/10 , C25B1/24 , C25B1/34 , C25B1/46 , C25B9/18 , C25B15/08 , Y02P20/125
摘要： The present disclosure is a method and system for production of carboxylic based chemicals. A method for producing at oxalic acid may include receiving an anolyte feed at an anolyte region of an electrochemical cell including an anode and receiving a catholyte feed including cartoon dioxide and an alkali metal bicarbonate at a catholyte region of the electrochemical cell including a cathode.
摘要翻译：本公开是用于生产羧基化学品的方法和系统。用于草酸生产的方法可包括在包括阳极的电化学电池的阳极电解液区域接收阳极电解液进料，并在包括阴极的电化学电池的阴极电解液区域接收包含卡通二氧化物和碱金属碳酸氢盐的阴极电解质进料。

2. 发明申请

WO2014046795A3 ELECTROCHEMICAL CO-PRODUCTION OF CHEMICALS WITH SULFUR-BASED REACTANT FEEDS TO ANODE 审中-公开
标题翻译：化学反应生物化学与硫酸反应物进料到阳极
公开(公告)号：WO2014046795A3
公开(公告)日：2014-10-09
申请号：PCT/US2013053587
申请日：2013-08-05
申请人： LIQUID LIGHT INC
发明人： KACZUR JERRY J , TEAMEY KYLE
IPC分类号： C01B17/76 , C25B1/22 , C25B7/00
CPC分类号： C25B9/08 , C25B3/02 , C25B3/04 , C25B9/00 , C25B15/08 , Y02P20/132 , Y02P20/582 , Y02P30/42
摘要： A system and method produces a first product from a first region of an electrochemical cell having a cathode and a second product from a second region of the electrochemical cell having an anode. The method may include a step of contacting the first region with a catholyte comprising carbon dioxide. The method may include another step of contacting the second region with an anolyte comprising a sulfur-based reactant. Further, the method may include a step of applying an electrical potential between the anode and the cathode sufficient to produce a first product recoverable from the first region and a second product recoverable from the second region. An additional step of the method may include removing the second product and an unreacted sulfur-based reactant from the second region and recycling the unreacted sulfur-based reactant to the second region.
摘要翻译：系统和方法从具有阴极的电化学电池的第一区域产生第一产物，并且从具有阳极的电化学电池的第二区域产生第二产物。该方法可以包括使第一区域与包含二氧化碳的阴极电解液接触的步骤。该方法可以包括使第二区域与包含硫基反应物的阳极电解液接触的另一步骤。此外，该方法可以包括在阳极和阴极之间施加足以产生可从第一区域回收的第一产物和从第二区域可回收的第二产品的电势的步骤。该方法的另外的步骤可以包括从第二区域除去第二产物和未反应的硫基反应物并将未反应的基于硫的反应物再循环到第二区域。

3. 发明申请

WO2014100828A1 METHOD AND SYSTEM FOR PRODUCTION OF OXALIC ACID AND OXALIC ACID REDUCTION PRODUCTS 审中-公开
标题翻译：用于生产含氧酸和减少酸的产品的方法和系统
公开(公告)号：WO2014100828A1
公开(公告)日：2014-06-26
申请号：PCT/US2013/077610
申请日：2013-12-23
申请人： LIQUID LIGHT, INC.
发明人： TEAMEY, Kyle , KACZUR, Jerry J. , COLE, Emily Barton , SIVASANKAR, Narayanappa , MAJSZTRIK, Paul , LEONARD, George , PARAJULI, Rishi , KEETS, Kate A. , KRAMER, Theodore J. , FARRAUTO, Robert , AUGUSTINE, Robert , TANIELYAN, Setrak , KASIREDDY, Mohanreddy , ZHU, Yizu , TWARDOWSKI, Zbigniew , DHUN, Farah , BAUER, Alexander
IPC分类号： C25B3/00
CPC分类号： C25B9/18 , C25B1/24 , C25B3/04 , C25B15/08
摘要： The present disclosure is a method and system for production of oxalic acid and oxalic acid reduction products. The production of oxalic acid and oxalic acid reduction products may include the electrochemical conversion of CO 2 to oxalate and oxalic acid. The method and system for production of oxalic acid and oxalic acid reduction products may further include the acidification of oxalate to oxalic acid, the purification of oxalic acid and the hydrogenation of oxalic acid to produce oxalic acid reduction products.
摘要翻译：本公开是用于生产草酸和草酸还原产物的方法和系统。草酸和草酸还原产物的生产可能包括将CO 2电化学转化为草酸和草酸。用于生产草酸和草酸还原产物的方法和系统还可以包括草酸向草酸的酸化，草酸的纯化和草酸的氢化以产生草酸还原产物。

4. 发明申请

WO2014046798A2 ELECTROCHEMICAL REDUCTION OF CO2 WITH CO-OXIDATION OF AN ALCOHOL 审中-公开
标题翻译：用醇氧化的电化学还原CO2
公开(公告)号：WO2014046798A2
公开(公告)日：2014-03-27
申请号：PCT/US2013/053607
申请日：2013-08-05
申请人： LIQUID LIGHT, INC.
发明人： TEAMEY, Kyle , KACZUR, Jerry, J. , COLE, Emily, Barton , MAJSZTRIK, Paul , SIVASANKAR, Narayanappa , BOCARSLY, Andrew, B.
IPC分类号： C25B9/10 , C25B3/02 , C25B1/00
CPC分类号： C25B9/08 , C25B3/02 , C25B3/04 , C25B9/00 , C25B15/08 , Y02P20/132 , Y02P20/582 , Y02P30/42
摘要： The present disclosure is a system and method for producing a first product from a first region of an electrochemical cell having a cathode and a second product from a second region of the electrochemical cell having an anode. The method may include the step of contacting the first region of the electrochemical cell with a catholyte comprising an alcohol and carbon dioxide. Another step of the method may include contacting the second region of the electrochemical cell with an anolyte comprising the alcohol. Further, the method may include a step of applying an electrical potential between the anode and the cathode sufficient to produce a first product recoverable from the first region and a second product recoverable from the second region.
摘要翻译：本公开是用于从具有阴极的电化学电池的第一区域和来自具有阳极的电化学电池的第二区域的第二产物生产第一产物的系统和方法。该方法可以包括使电化学电池的第一区域与包含醇和二氧化碳的阴极电解液接触的步骤。该方法的另一个步骤可以包括使电化学电池的第二区域与包含醇的阳极电解液接触。此外，该方法可以包括在阳极和阴极之间施加足以产生可从第一区域回收的第一产品和可从第二区域回收的第二产品的电势的步骤。

5. 发明申请

WO2014032000A1 REDUCING CARBON DIOXIDE TO PRODUCTS WITH AN INDIUM OXIDE ELECTRODE 审中-公开
标题翻译：将二氧化碳还原成具有氧化铝氧化物电极的产品
公开(公告)号：WO2014032000A1
公开(公告)日：2014-02-27
申请号：PCT/US2013/056457
申请日：2013-08-23
申请人： LIQUID LIGHT, INC. , THE TRUSTEES OF PRINCETON UNIVERSITY
发明人： BOCARSLY, Andrew, B. , DETWEILER, Zachary, M.
IPC分类号： H01M4/02
CPC分类号： C25B3/04 , C25B9/08 , C25B11/04 , C25B11/0452 , C25D11/34
摘要： A method reducing carbon dioxide to one or more organic products may include steps (A) to (E). Step (A) may introduce an anolyte to a first compartment of an electrochemical cell. The first compartment may include an anode. Step (B) may introduce a catholyte and carbon dioxide to a second compartment of the electrochemical cell. Step (C) may oxidize an indium cathode to produce an oxidized indium cathode. Step (D) may introduce the oxidized indium cathode to the second compartment. Step (E) may apply an electrical potential between the anode and the oxidized indium cathode sufficient for the oxidized indium cathode to reduce the carbon dioxide to a reduced product.
摘要翻译：将二氧化碳还原成一种或多种有机产物的方法可包括步骤（A）至（E）。步骤（A）可将阳极电解液引入电化学电池的第一隔室。第一隔室可包括阳极。步骤（B）可以向电化学电池的第二隔室引入阴极电解质和二氧化碳。步骤（C）可以氧化铟阴极以产生氧化的铟阴极。步骤（D）可以将氧化的铟阴极引入第二隔室。步骤（E）可以在阳极和氧化的铟阴极之间施加足以使氧化的铟阴极将二氧化碳还原成还原产物的电位。

6. 发明申请

WO2012015909A2 HETEROCYCLE CATALYZED ELECTROCHEMICAL PROCESS 审中-公开
标题翻译：杂环催化电化学工艺
公开(公告)号：WO2012015909A2
公开(公告)日：2012-02-02
申请号：PCT/US2011/045521
申请日：2011-07-27
申请人： LIQUID LIGHT, INC. , PRINCETON UNIVERSITY , COLE, Emily, Barton , BOCARSLY, Andrew, B.
发明人： COLE, Emily, Barton , BOCARSLY, Andrew, B.
IPC分类号： C25B3/04
CPC分类号： C25B3/04 , C25B1/003 , C25B3/105
摘要： A method for heterocycle catalyzed electrochemical reduction of a carbonyl compound is disclosed. The method generally includes steps (A) to (C). Step (A) may introduce the carbonyl compound into a solution of an electrolyte and a heterocycle catalyst in a divided electrochemical cell. The divided electrochemical cell may include an anode in a first cell compartment and a cathode in a second cell compartment. The cathode generally reduces the carbonyl compound to at least one aldehyde compound. Step (B) may vary which of the aldehyde compounds is produced by adjusting one or more of (i) a cathode material, (ii) the electrolyte, (iii) the heterocycle catalyst, (iv) a pH level and (v) an electrical potential. Step (C) may separate the aldehyde compounds from the solution.
摘要翻译：公开了一种用于羰基化合物的杂环催化的电化学还原的方法。该方法通常包括步骤（A）至（C）。步骤（A）可以将羰基化合物引入电解质和杂环催化剂的溶液中。分隔的电化学电池可以包括第一电池室中的阳极和第二电池室中的阴极。阴极通常将羰基化合物还原成至少一种醛化合物。步骤（B）可以通过调节（i）阴极材料，（ii）电解质，（iii）杂环催化剂，（iv）pH水平和（v））中的一种或多种来改变哪种醛化合物的产生电位步骤（C）可以将醛化合物与溶液分离。

7. 发明申请

WO2014046796A3 A METHOD AND SYSTEM FOR THE ELECTROCHEMICAL CO-PRODUCTION OF HALOGEN AND CARBON MONOXIDE FOR CARBONYLATED PRODUCTS 审中-公开
标题翻译：用于羰基化产物的卤素和一氧化碳的电化学共生的方法和系统
公开(公告)号：WO2014046796A3
公开(公告)日：2014-11-06
申请号：PCT/US2013053592
申请日：2013-08-05
申请人： LIQUID LIGHT INC
发明人： TEAMEY KYLE , KACZUR JERRY J , SHIRTUM ROBERT PAGE
IPC分类号： C25B3/10
CPC分类号： C25B9/08 , C25B3/02 , C25B3/04 , C25B9/00 , C25B15/08 , Y02P20/132 , Y02P20/582 , Y02P30/42
摘要： The present disclosure is a system and method for producing a first product from a first region of an electrochemical cell having a cathode and a second product from a second region of the electrochemical cell having an anode. The method may include a step of contacting the first region with a catholyte including carbon dioxide and contacting the second region with an anolyte including a recycled reactant. The method may further include applying an electrical potential between the anode and the cathode sufficient to produce carbon monoxide recoverable from the first region and a halogen recoverable from the second region.
摘要翻译：本公开是用于从具有阴极的电化学电池的第一区域和来自具有阳极的电化学电池的第二区域的第二产物生产第一产物的系统和方法。该方法可包括使第一区域与包含二氧化碳的阴极电解液接触并使第二区域与包含再循环反应物的阳极电解液接触的步骤。该方法可进一步包括在阳极和阴极之间施加足以产生可从第一区域回收的一氧化碳和从第二区域回收的卤素的电势。

8. 发明申请

WO2014152883A1 METHOD FOR SYNTHESIS OF SUB 100-NM INDIUM NANOPARTICLES 审中-公开
标题翻译：用于合成100-NM纳米纳米粒子的方法
公开(公告)号：WO2014152883A1
公开(公告)日：2014-09-25
申请号：PCT/US2014/028105
申请日：2014-03-14
申请人： LIQUID LIGHT INC.
发明人： KRAMER, Theodore, J.
IPC分类号： B32B15/04
CPC分类号： B01J35/0013 , B01J23/08 , B01J35/0033 , B01J35/006 , B01J37/16 , B22F1/0018 , B22F9/24
摘要： The present disclosure generally relates to a method for the synthesis and production of indium nanoparticles. More particularly, disclosed is a method of making indium nanoparticles in a nonpolar solvent. The indium nanopatl icles are prepared by reducing an indium fatty acid carboxylate in the presence of a surfactant. Indium is a useful electrocatalyst and electrode material for performing certain electrochemical reactions. Because electrochemical reactions generally occur on the electrode surface, a high surface area of electrode material, or material coated on an electrode is desirable. One way to achieve high surface area is to use a coating of small particles such as nanoparticles.
摘要翻译：本发明一般涉及铟纳米粒子的合成和生产方法。更具体地，公开了在非极性溶剂中制造铟纳米颗粒的方法。通过在表面活性剂的存在下还原铟脂肪酸羧酸酯制备铟纳米颗粒。铟是用于进行某些电化学反应的有用的电催化剂和电极材料。因为电化学反应通常发生在电极表面上，所以电极材料的高表面积或涂在电极上的材料是理想的。实现高表面积的一种方法是使用小颗粒如纳米颗粒的涂层。

9. 发明申请

WO2014046797A3 ELECTROCHEMICAL CO-PRODUCTION OF CHEMICALS UTILIZING A HALIDE SALT 审中-公开
标题翻译：电化学生产利用卤化物盐的化学品
公开(公告)号：WO2014046797A3
公开(公告)日：2014-05-22
申请号：PCT/US2013053600
申请日：2013-08-05
申请人： LIQUID LIGHT INC
发明人： TEAMEY KYLE , KACZUR JERRY J
IPC分类号： C02F1/461 , C25B1/14 , C25B3/06 , H01M4/90
CPC分类号： C25B9/08 , C25B3/02 , C25B3/04 , C25B9/00 , C25B15/08 , Y02P20/132 , Y02P20/582 , Y02P30/42
摘要： A system and method for co-produces a first product and a second product. The system may include a first electrochemical cell, at least one second reactor, and an acidification chamber. The method and system for co-producing a first product and a second product may include co-producing a carboxylic acid and at least one of an alkene, alkyne, aldehyde, ketone, or an alcohol while employing a recycled halide salt.
摘要翻译：一种用于共同生产第一产品和第二产品的系统和方法。该系统可以包括第一电化学电池，至少一个第二反应器和酸化室。用于共同生产第一产物和第二产物的方法和系统可以包括在使用再循环卤化物盐的同时共同产生羧酸和烯烃，炔烃，醛，酮或醇中的至少一种。

10. 发明申请

WO2014046794A2 SYSTEM AND METHOD FOR OXIDIZING ORGANIC COMPOUNDS WHILE REDUCING CARBON DIOXIDE 审中-公开
标题翻译：在减少二氧化碳时氧化有机化合物的系统和方法
公开(公告)号：WO2014046794A2
公开(公告)日：2014-03-27
申请号：PCT/US2013/053583
申请日：2013-08-05
申请人： LIQUID LIGHT, INC.
发明人： TEAMEY, Kyle , KACZUR, Jerry, J. , SIVASANKAR, Narayanappa , MAJSZTRIK, Paul , COLE, Emily, Barton , BOCARSLY, Andrew, B.
IPC分类号： C25B3/02
CPC分类号： C25B3/04 , C25B1/00 , C25B15/08
摘要： Methods and systems for electrochemically generating an oxidation product and a reduction product may include one or more operations including, but not limited to: receiving a feed of at least one organic compound into an anolyte region of an electrochemical cell including an anode; at least partially oxidizing the at least one organic compound at the anode to generate at least carbon dioxide; receiving a feed including carbon dioxide into a catholyte region of the electrochemical cell including a cathode; and at least partially reducing carbon dioxide to generate a reduction product at the cathode.
摘要翻译：用于电化学生成氧化产物和还原产物的方法和系统可以包括一种或多种操作，包括但不限于：将至少一种有机化合物的进料接收到包括阳极的电化学电池的阳极电解液区域中; 至少部分地氧化阳极上的至少一种有机化合物以产生至少二氧化碳; 将包含二氧化碳的进料接收到包括阴极的电化学电池的阴极电解液区域中; 并且至少部分还原二氧化碳以在阴极产生还原产物。

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