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1. 发明申请

WO2011137878A2 NANOTUBES BASED ON TITANIUM DIOXIDE WITH A HIGH ASPECT RATIO AND A METHOD OF THEIR PREPARATION 审中-公开
标题翻译：基于二氧化钛的高分子量纳米粒子及其制备方法
公开(公告)号：WO2011137878A2
公开(公告)日：2011-11-10
申请号：PCT/CZ2011/000045
申请日：2011-05-02
申请人： INSTITUTE OF MACROMOLECULAR CHEMISTRY AS CR, V. V. I. , SLOUF, Miroslav , KRALOVA, Daniela , KRULIS, Zdenek
发明人： SLOUF, Miroslav , KRALOVA, Daniela , KRULIS, Zdenek
CPC分类号： C01G23/047 , B82Y30/00 , C01P2002/72 , C01P2004/03 , C01P2004/04 , C01P2004/133 , C01P2004/54 , C01P2004/61 , C01P2004/64
摘要： Nanotubes based on titanium dioxide with a high aspect ratio (>50) and a new type of crystal structure characterized by three main maxima of electron diffraction pattern at the values of diffraction vector q = 1.75 Å -1 , 2.05 Å -1 and 3.35 Å -1 and two other broad peaks at q = 4.20 Å -1 and 5.25 Å -1 (diffraction vector q is defined by the equation q = 4π-sin(θ)/λ, where θ is the diffraction angle and λ is the wavelength of accelerated electrons).
摘要翻译：具有高纵横比（> 50）的二氧化钛和新型晶体结构的纳米管，其特征在于在衍射矢量q = 1.75Å-1，2.05Å-1和3.35Å的电子衍射图的三个主要最大值 -1和在q = 4.20埃-1和5.25埃-1处的另外两个宽峰（衍射矢量q由等式q = 4p-sin（λ）/λ定义，其中λ是衍射角，λ是波长的加速电子）。

2. 发明申请

WO2011035743A1 RAW MATERIAL FOR POLYURETHANE PRODUCTION AND PROCESS FOR ITS PREPARING FROM WASTE POLYURETHANE 审中-公开
标题翻译：用于聚氨酯生产的原料及其从废弃聚氨酯制备的方法
公开(公告)号：WO2011035743A1
公开(公告)日：2011-03-31
申请号：PCT/CZ2010/000101
申请日：2010-09-20
申请人： INSTITUTE OF MACROMOLECULAR CHEMISTRY AS CR, v.v.i. , VLCEK, Tomas , BENES, Hynek , KRULIS, Zdenek
发明人： VLCEK, Tomas , BENES, Hynek , KRULIS, Zdenek
IPC分类号： C08G18/83 , C08J11/00 , C08J11/04 , C08J11/10 , C08J11/18 , C08J11/24
CPC分类号： C08G18/83 , C08G18/831 , C08J11/24 , C08J2375/04 , Y02P20/582 , Y02W30/706
摘要： Raw material for polyurethane production and a process for its preparing from waste polyurethane Recycling of polyurethanes using bioreagents with functional hydroxy groups, when liquid products are obtained, which have a markedly lower hydroxyl number. This makes it possible to utilize them as a raw material for production of expanded and compact polyurethanes. By an appropriate choice of the bioreagent, the resulting functionality of the product, its hydroxyl number and reactivity depending on the content of primary and secondary alcoholic hydroxy groups and amino groups and thus to obtain a raw material for production of polyurethanes with optimum parameters according to the required applications.
摘要翻译：用于聚氨酯生产的原料及其由废弃聚氨酯制备的方法当获得具有明显较低羟值的液体产物时，使用具有官能羟基的生物反应器回收聚氨酯。这使得可以将其用作生产膨胀和紧凑型聚氨酯的原料。通过适当选择生物试剂，产生的产物官能度，其羟值和反应性取决于伯和仲醇羟基和氨基的含量，从而得到具有最佳参数的聚氨酯的生产原料，根据所需的应用程序。

3. 发明申请

WO2011137878A3 NANOTUBES BASED ON TITANIUM DIOXIDE WITH A HIGH ASPECT RATIO AND A METHOD OF THEIR PREPARATION 审中-公开
标题翻译：基于二氧化钛的高分子量纳米粒子及其制备方法
公开(公告)号：WO2011137878A3
公开(公告)日：2012-01-12
申请号：PCT/CZ2011000045
申请日：2011-05-02
申请人： INST OF MACROMOLECULAR CHEMISTRY AS CR V V I , SLOUF MIROSLAV , KRALOVA DANIELA , KRULIS ZDENEK
发明人： SLOUF MIROSLAV , KRALOVA DANIELA , KRULIS ZDENEK
IPC分类号： C01G23/047
CPC分类号： C01G23/047 , B82Y30/00 , C01P2002/72 , C01P2004/03 , C01P2004/04 , C01P2004/133 , C01P2004/54 , C01P2004/61 , C01P2004/64
摘要： Nanotubes based on titanium dioxide with a high aspect ratio (>50) and a new type of crystal structure characterized by three main maxima of electron diffraction pattern at the values of diffraction vector q = 1.75 Å-1, 2.05 Å-1 and 3.35 Å-1 and two other broad peaks at q = 4.20 Å-1 and 5.25 Å-1 (diffraction vector q is defined by the equation q = 4p-sin(?)/?, where ? is the diffraction angle and ? is the wavelength of accelerated electrons).
摘要翻译：具有高纵横比（> 50）的二氧化钛和新型晶体结构的纳米管，其特征在于在衍射矢量q = 1.75Å-1，2.05Å-1和3.35Å的电子衍射图的三个主要最大值 -1和在q = 4.20埃-1和5.25埃-1处的另外两个宽峰（衍射矢量q由等式q = 4p-sin（λ）/λ定义，其中λ是衍射角，λ是波长的加速电子）。

4. 发明申请

WO2009024102A4 METHOD OF RECYCLING WASTE POLYURETHANE FOAMS 审中-公开
公开(公告)号：WO2009024102A4
公开(公告)日：2009-02-26
申请号：PCT/CZ2008/000095
申请日：2008-08-20
申请人： INSTITUTE OF MACROMOLECULAR CHEMISTRY AS CR, V.V.I. , INSTITUTE OF CHEMICAL PROCESS FUNDAMENTALS AS CR, V.V.I. , KRULIS, Zdenek , HORAK, Zdenek , BENES, Hynek , HAJEK, Milan
发明人： KRULIS, Zdenek , HORAK, Zdenek , BENES, Hynek , HAJEK, Milan
IPC分类号： C08J11/24
摘要： The invention concerns the method of recycling waste polyurethane foams to a polyol mixture characterized in that the waste polyurethane is decomposed by the reaction with a low- molecular-weight polyhydric alcohol selected from the group consisting of ethylene glycol, propylene glycol, butanediol, pentanediol, hexanediol, 2-methylpropane-l,3-diol, diethylene glycol, dipropylene glycol, triethylene glycol, tripropylene glycol, trimethylolpropane (2,2- bis(hydroxymethyl)propan-l-ol), glycerol or their mixtures under the condition that the waste polyurethane and polyhydric alcohol are used in the weight ratio at least 3:1 and at most 1:3 and the reaction mixture is subjected to the action of electromagnetic radiation of a frequency ranging from 1 MHz to 10 GHz at the temperature from 50 °C - 300 °C.

5. 发明申请

WO2007087760A1 THERMOPLASTIC POLYMER COMPOSITION FOR SKELETAL REPLACEMENTS AND METHOD OF ITS PRODUCTION 审中-公开
标题翻译：用于骨骼替代的热塑性聚合物组合物及其生产方法
公开(公告)号：WO2007087760A1
公开(公告)日：2007-08-09
申请号：PCT/CZ2007/000007
申请日：2007-01-31
申请人： USTAV MAKROMOLEKULARNI CHEMIE AKADEMIE VED CESKE REPUBLIKY , KRULIS Zdenek , STARY Zdenek , HORAK, Zdenek , PETRTYL Miroslav
发明人： KRULIS Zdenek , STARY Zdenek , HORAK, Zdenek , PETRTYL Miroslav
IPC分类号： C08L13/02 , A61F2/28
CPC分类号： C08L23/06 , A61F2/28 , A61F2/30756 , A61F2002/30065 , A61F2210/0071 , C08L23/02 , C08L23/0815 , C08L23/0823 , C08L2666/06
摘要： The invention concerns thermoplastic polymer compositions for skeletal replacements and methods of their production. The composition according to the invention consists of 12 - 91 wt.% of a polyolefm with the glass transition temperature higher than 320 K, which is an ethene - bicyclo[2.2.1]hept-2-ene copolymer with molar concentration of the latter at least 25 % and 75 % at most, of 2 - 72 wt. % of a polyolefm with the glass transition temperature lower than 250 K, which is (i) ethene homopolymer of density at least 0.92 g.cm -3 and 0.97 g.cm -3 at most or (ii) copolymer of ethene with an α-olefin selected from a group consisting of propene, but-1-ene, hex-1-ene, oct-1-ene and dec-1-ene, with density at least 0.85 g.cm -3 and 0.96 g.cm -3 at most or a mixture of ethene homopolymer (i) and ethene - α-olefin copolymer (ii) in any ratio, and of 5-50 wt.% of carbon fibres with the carbon content at least 94 wt.%, density at least 1.80 g.cm -3 and 1.92 g.cm -3 at most and a fibre diameter of at least 4 µm and 9 µm at most. The described composition is prepared by mixing in the melt a polyolefm with the glass transition temperature higher than 320 K and a polyolefm with the glass transition temperature lower than 250 K at a melt temperature of the stirred mixture of at least 430 K. The formed thermoplastic polymer composition is irradiated with γ-rays or accelerated electrons at a dose of at least 20 kGy and 250 IcGy at most, to advantage in inert atmosphere, whereupon the irradiated material is mixed in the melt with carbon fibres at a temperature of at least 430 K. The material can be stabilized against oxidative degradation by admixture of at least 0.1 wt.% of α-tocopherol.
摘要翻译：本发明涉及骨架替代物的热塑性聚合物组合物及其生产方法。根据本发明的组合物由12.91重量％的玻璃化转变温度高于320K的聚烯烃组成，其为摩尔浓度为后者的乙烯 - 双环[2.2.1]庚-2-烯共聚物至多25％和75％，最多为2-72wt。玻璃化转变温度低于250K的聚烯烃的％，其是（i）密度至少为0.92g·cm -3和0.97g·cm -3的乙烯均聚物，或（ii）乙烯与选自丙烯，丁-1-烯，己-1-烯，辛-1-烯和癸-1-烯的α-烯烃的共聚物，密度至少0.85克/厘米3以上和0.96克/厘米3以上的乙烯均聚物（i）和乙烯-α-烯烃共聚物（ii）的混合物，以及5-50重量％的碳纤维的碳含量至少为94重量％，密度至少为1.80克/厘米3至1.92克/厘米3， -3至多，纤维直径至多为4μm，最大为9μm。所述的组合物通过在熔体中混合玻璃化转变温度高于320K的聚烯烃和在至少430K的搅拌混合物的熔融温度下玻璃化转变温度低于250K的聚烯烃来制备。所形成的热塑性塑料聚合物组合物以至少20kGy和250Icyy的剂量至少用α射线或加速电子照射，在惰性气氛中有利，随后将辐射材料与碳纤维在至少430℃的温度下混合该材料可以通过至少0.1重量％的α-生育酚的混合来稳定，防止氧化降解。

6. 发明申请

WO2004039875A1 METHOD OF RECYCLING OF COMMINGLED PLASTICS WASTE TO TOUGH THERMOPLASTIC MATERIALS 审中-公开
标题翻译：回收塑料废弃物对粗糙热塑性材料的回收方法
公开(公告)号：WO2004039875A1
公开(公告)日：2004-05-13
申请号：PCT/CZ2003/000059
申请日：2003-10-27
申请人： ÚSTAV MAKROMOLEKULÁRNÍ CHEMIE AKADEMIE VED CESKÉ REPUBLIKY , KRULIS, Zdenek , MICHÁLKOVÁ, Danuse , FORTELNY, Ivan , HORÁK, Zdenek
发明人： KRULIS, Zdenek , MICHÁLKOVÁ, Danuse , FORTELNY, Ivan , HORÁK, Zdenek
IPC分类号： C08J11/06
CPC分类号： C08J11/06 , C08J2323/02 , C08K5/17 , C08L23/02 , C08L23/16 , C08L53/02 , C08L2207/20 , Y02W30/701 , Y10T428/28 , Y10T428/31855 , C08L2666/06 , C08L2666/24
摘要： The application concerns the method of recycling commingled plastics waste containing min. 30 wt. % of polyolefins to a tough thermoplastic material. The method is based on the compatibilization of the polymer components of commingled plastics waste with an admixture of 2 - 15 wt. % of an ethylene - propylene copolymer or a styrene - butadiene block copolymer or a combination of an ethylene - propylene copolymer and a styrene - butadiene copolymer in any weight ratio, together with 0.1 - 2.5 wt. % of a secondary aromatic amine and by subsequent blend processing in the melt.
摘要翻译：该应用涉及回收混合塑料废物的方法，包括最小。 30重量％％的聚烯烃与韧性热塑性材料。该方法基于混合塑料废料的聚合物组分与2-15重量％的混合物的相容性。％的乙烯 - 丙烯共聚物或苯乙烯 - 丁二烯嵌段共聚物或任何重量比的乙烯 - 丙烯共聚物和苯乙烯 - 丁二烯共聚物的组合，以及0.1-2.5wt。％的仲芳族胺和通过在熔体中的随后的共混加工。

7. 发明申请

WO2009024102A3 METHOD OF RECYCLING WASTE POLYURETHANE FOAMS 审中-公开
公开(公告)号：WO2009024102A3
公开(公告)日：2009-02-26
申请号：PCT/CZ2008/000095
申请日：2008-08-20
申请人： INSTITUTE OF MACROMOLECULAR CHEMISTRY AS CR, V.V.I. , INSTITUTE OF CHEMICAL PROCESS FUNDAMENTALS AS CR, V.V.I. , KRULIS, Zdenek , HORAK, Zdenek , BENES, Hynek , HAJEK, Milan
发明人： KRULIS, Zdenek , HORAK, Zdenek , BENES, Hynek , HAJEK, Milan
IPC分类号： C08J11/24
摘要： The invention concerns the method of recycling waste polyurethane foams to a polyol mixture characterized in that the waste polyurethane is decomposed by the reaction with a low- molecular-weight polyhydric alcohol selected from the group consisting of ethylene glycol, propylene glycol, butanediol, pentanediol, hexanediol, 2-methylpropane-l,3-diol, diethylene glycol, dipropylene glycol, triethylene glycol, tripropylene glycol, trimethylolpropane (2,2- bis(hydroxymethyl)propan-l-ol), glycerol or their mixtures under the condition that the waste polyurethane and polyhydric alcohol are used in the weight ratio at least 3:1 and at most 1:3 and the reaction mixture is subjected to the action of electromagnetic radiation of a frequency ranging from 1 MHz to 10 GHz at the temperature from 50 °C - 300 °C.

8. 发明申请

WO2009024102A2 METHOD OF RECYCLING WASTE POLYURETHANE FOAMS 审中-公开
标题翻译：回收废聚氨酯泡沫的方法
公开(公告)号：WO2009024102A2
公开(公告)日：2009-02-26
申请号：PCT/CZ2008/000095
申请日：2008-08-20
申请人： INSTITUTE OF MACROMOLECULAR CHEMISTRY AS CR, V.V.I. , INSTITUTE OF CHEMICAL PROCESS FUNDAMENTALS AS CR, V.V.I. , KRULIS, Zdenek , HORAK, Zdenek , BENES, Hynek , HAJEK, Milan
发明人： KRULIS, Zdenek , HORAK, Zdenek , BENES, Hynek , HAJEK, Milan
IPC分类号： C08J11/24
CPC分类号： C08J11/24 , C08G18/831 , C08J2375/04 , Y02W30/706
摘要： The invention concerns the method of recycling waste polyurethane foams to a polyol mixture characterized in that the waste polyurethane is decomposed by the reaction with a low- molecular-weight polyhydric alcohol selected from the group consisting of ethylene glycol, propylene glycol, butanediol, pentanediol, hexanediol, 2-methylpropane-l,3-diol, diethylene glycol, dipropylene glycol, triethylene glycol, tripropylene glycol, trimethylolpropane (2,2- bis(hydroxymethyl)propan-l-ol), glycerol or their mixtures under the condition that the waste polyurethane and polyhydric alcohol are used in the weight ratio at least 3:1 and at most 1:3 and the reaction mixture is subjected to the action of electromagnetic radiation of a frequency ranging from 1 MHz to 10 GHz at the temperature from 50 °C - 300 °C.
摘要翻译：本发明涉及将废聚氨酯泡沫再循环到多元醇混合物中的方法，其特征在于废聚氨酯通过与选自乙二醇，丙二醇，丁二醇，戊二醇，戊二醇，己二醇，己二醇，2-甲基丙烷-1,3-二醇，二甘醇，二丙二醇，三甘醇，三丙二醇，三羟甲基丙烷（2,2-双（羟甲基）丙-1-醇），甘油或它们的混合物废聚氨酯和多元醇以重量比至少3:1且至多1:3使用，并且反应混合物在50℃的温度下经受频率范围为1MHz至10GHz的电磁辐射的作用 C - 300°C。

9. 发明申请

WO2007068216A1 METHOD OF MODIFICATION OF ULTRAHIGH-MOLECULAR-WEIGHT POLYETHYLENE FOR MANUFACTURE OF JOINT REPLACEMENTS WITH INCREASED LIFETIME 审中-公开
标题翻译：超分子量重聚乙烯改性联合替代物增加生命周期的方法
公开(公告)号：WO2007068216A1
公开(公告)日：2007-06-21
申请号：PCT/CZ2006/000089
申请日：2006-12-13
申请人： USTAV MAKROMOLEKULARNI CHEMIE AKADEMIE VEDCESKE REPUBLIKY , HORAK, Zdenek , SLOUF, Miroslav , KRULIS, Zdenek , FENCL, Jaroslav
发明人： HORAK, Zdenek , SLOUF, Miroslav , KRULIS, Zdenek , FENCL, Jaroslav
IPC分类号： A61F2/30 , A61L27/16 , C08J3/24 , C08J3/28
CPC分类号： A61L27/16 , C08J3/28 , C08J7/123 , C08J2323/06 , C08L23/06 , C08L2312/06
摘要： The solution concerns the method of modification of ultrahigh-molecular-weight polyethylene increasing the lifetime of joint replacements characterized in that the polymer is irradiated in inert atmosphere with γ-rays at dose rates 0.25 kGy/h - 10 kGy/h for 4-220 h or with accelerated electrons at dose rates at least 1200 kGy/h - 12000 kGy/h for at least 12 s and 10 min at the maximum, the total irradiation dose ranging from 40 IcGy to maximum 200 kGy and the thus irradiated ultrahigh-molecular-weight polyethylene is subsequently heated at 90- 200 0C for 5 min - 10 h in inert atmosphere and then continually cooled at a maximum rate of 20 °C/min.
摘要翻译：该解决方案涉及改性超高分子量聚乙烯的方法，增加了联合置换的使用寿命，其特征在于聚合物在惰性气氛中用γ射线以0.25kGy / h-10kGy / h的剂量辐射4-220 h或加速电子，剂量率至少为1200 kGy / h - 12000 kGy / h，最大为12 s和10 min，总照射剂量范围为40 IcGy至最大200 kGy，并由此照射超高分子量随后在惰性气氛中在90-200℃加热5分钟-10小时，然后以20℃/ min的最大速率连续冷却。

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