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1. 发明申请

WO03000652A8 PROCESS FOR PREPARATION OF CYCLOHEXANOL DERIVATIVES 审中-公开
标题翻译：环己烷衍生物的制备方法
公开(公告)号：WO03000652A8
公开(公告)日：2004-05-21
申请号：PCT/US0219753
申请日：2002-06-21
申请人： WYETH CORP , KIM KEUN-SIK , KIM KWANG-IL , LEE SUNG-WOO , PARK JIN-SOO , CHAI KI-BYUNG
发明人： KIM KEUN-SIK , KIM KWANG-IL , LEE SUNG-WOO , PARK JIN-SOO , CHAI KI-BYUNG
IPC分类号： C07C261/00 , C07B61/00 , C07C253/30 , C07C255/37
CPC分类号： C07C253/30 , C07C2601/14 , C07C255/37
摘要： A process for the preparation of cyclohexanol derivatives of formula (I) by reacting a compound of formula (II) with a compound of formula (III) in the presence of a base catalyst of formula (IV) or (V). In the above formula, R1-R9, A, B, X and p have tghe meanings given in the specification.
摘要翻译：在式（Ⅳ）或（Ⅴ）的碱催化剂存在下，使式（Ⅳ）化合物与式（Ⅳ）化合物反应制备式（Ⅰ）的环己醇衍生物的方法。在上式中，R1-R9，A，B，X和p具有本说明书中给出的含义。

2. 发明申请

WO2013015654A3 METHOD FOR PREPARING AMINO-TRIAZOLINONE 审中-公开
标题翻译：制备氨基三唑啉酮的方法
公开(公告)号：WO2013015654A3
公开(公告)日：2013-06-13
申请号：PCT/KR2012006031
申请日：2012-07-27
申请人： KS LAB CO LTD , KIM KEUN SIK , CHOI YEON TAK
发明人： KIM KEUN SIK , CHOI YEON TAK
IPC分类号： C07D249/14 , A01N43/653 , C07D249/12
CPC分类号： C07D249/12
摘要： The present invention relates to a method for preparing an amino-triazolinone which can be used as a raw material for amicarbazone and has chemical formula (I). The method for preparing the amino-triazolinone comprises the steps of: reacting an acyl hydrazide of chemical formula (II) with a carbamating agent of chemical formula (III) or (IV) so as to obtain a hydrazine carboxylic acid of chemical formula (V); and reacting the thus-obtained hydrazine carboxylic acid of chemical formula (V) with a hydrazine hydrate under the presence of a base catalyst. According to the present invention, the amino-triazolinone may be stably prepared without using safety equipment or safety facilities for a possible leakage of phosgene, which has been used as a conventional reactant. Thus, manufacturing costs for amicarbazone, which is used as an herbicide for farm products such as sugar cane, corn, or the like, can be reduced so as to achieve improved price competitiveness, and further to achieve improved cost competitiveness compared to other herbicides.
摘要翻译：本发明涉及一种制备氨基三唑啉酮的方法，该氨基三唑啉酮可以用作氨基脲的原料并且具有化学式（I）。制备氨基三唑啉酮的方法包括以下步骤：使化学式（II）的酰基肼与化学式（III）或（IV）的氨基甲酸化剂反应，以获得化学式（V）的肼羧酸）; 并在碱催化剂存在下将由此获得的化学式（V）的肼羧酸与肼水合物反应。根据本发明，可以稳定地制备氨基三唑啉酮而不使用已经用作常规反应物的可能泄漏光气的安全设备或安全设施。因此，可以减少用作甘蔗，玉米等农产品除草剂的氨力农碱的制造成本，从而实现提高的价格竞争力，并且与其他除草剂相比，成本竞争力进一步提高。

3. 发明申请

WO2004080934A2 PROCESS FOR PREPARATION OF PHENETHYLAMINE DERIVATIVES 审中-公开
标题翻译：制备苯乙烯衍生物的方法
公开(公告)号：WO2004080934A2
公开(公告)日：2004-09-23
申请号：PCT/US2004/007861
申请日：2004-03-09
申请人： WYETH , KIM, Keun-Sik , KIM, Kwang-il , CHAI, Ki-Byung
发明人： KIM, Keun-Sik , KIM, Kwang-il , CHAI, Ki-Byung
IPC分类号： C07C
CPC分类号： C07C213/02 , C07C2601/14 , C07C215/42 , C07C217/74
摘要： A process for the preparation of a compound of formula (I), wherein R 1 , and R 2 are ortho or para substituents, independently selected from the group consisting of hydrogen, hydroxyl, C 1 -C 6 alkyl, C 1 -C 6 alkoxy, C 7 -C 9 aralkoxy, C 2 -C 7 alkanoyloxy, C 1 -C 6 alkylmercapto, halo and trifluoromethyl; R 3 is hydrogen or C 1 -C 6 alkyl; R 4 is hydrogen, C 1 -C 6 alkyl, formyl or C 2 -C 7 alkanoyl; n is one of the integers 0, 1, 2, 3 or 4; and the dotted line represents optional olefinic unsaturation; comprising hydrogenating a compound of formula (III), in the presence of a nickel or cobalt catalyst at a temperature of about 5°C to 25°C.
摘要翻译：一种制备式（I）化合物的方法，其中R 1和R 2是独立地选自氢，羟基，C 1 -C 6烷基，C 1 -C 6烷氧基，C 7 -C 9芳烷氧基的邻位或对位取代基，C 2 -C 7烷酰氧基，C 1 -C 6烷基巯基，卤素和三氟甲基; R3是氢或C1-C6烷基; R4是氢，C1-C6烷基，甲酰基或C2-C7烷酰基; n是整数0,1,2,3或4之一; 并且虚线表示任选的烯属不饱和键; 包括在约5℃至25℃的温度下，在镍或钴催化剂的存在下氢化式（III）的化合物。

4. 发明申请

WO2004080934A3 PROCESS FOR PREPARATION OF PHENETHYLAMINE DERIVATIVES 审中-公开
标题翻译：制备苯乙胺衍生物的方法
公开(公告)号：WO2004080934A3
公开(公告)日：2004-10-28
申请号：PCT/US2004007861
申请日：2004-03-09
申请人： WYETH CORP , KIM KEUN-SIK , KIM KWANG-IL , CHAI KI-BYUNG
发明人： KIM KEUN-SIK , KIM KWANG-IL , CHAI KI-BYUNG
IPC分类号： C07C213/02 , C07C215/42 , C07C217/74 , C07C217/14
CPC分类号： C07C213/02 , C07C2601/14 , C07C215/42 , C07C217/74
摘要： A process for the preparation of a compound of formula (I), wherein R1, and R2 are ortho or para substituents, independently selected from the group consisting of hydrogen, hydroxyl, C1-C6 alkyl, C1-C6 alkoxy, C7-C9 aralkoxy, C2-C7 alkanoyloxy, C1-C6 alkylmercapto, halo and trifluoromethyl; R3 is hydrogen or C1-C6 alkyl; R4 is hydrogen, C1-C6 alkyl, formyl or C2-C7 alkanoyl; n is one of the integers 0, 1, 2, 3 or 4; and the dotted line represents optional olefinic unsaturation; comprising hydrogenating a compound of formula (III), in the presence of a nickel or cobalt catalyst at a temperature of about 5°C to 25°C.
摘要翻译：制备式（I）化合物的方法，其中R 1和R 2是邻位或对位取代基，独立地选自氢，羟基，C 1 -C 6烷基，C 1 -C 6烷氧基，C 7 -C 9芳烷氧基，C 2 -C 7烷酰氧基，C 1 -C 6烷基巯基，卤素和三氟甲基; R3是氢或C1-C6烷基; R4是氢，C1-C6烷基，甲酰基或C2-C7链烷酰基; n是整数0,1,2,3或4中的一个; 虚线代表任选的烯属不饱和度; 包括在镍或钴催化剂存在下在约5℃至25℃的温度下氢化式（III）的化合物。

5. 发明申请

WO2003000652A1 PROCESS FOR PREPARATION OF CYCLOHEXANOL DERIVATIVES 审中-公开
标题翻译：环己烷衍生物的制备方法
公开(公告)号：WO2003000652A1
公开(公告)日：2003-01-03
申请号：PCT/US2002/019753
申请日：2002-06-21
申请人： WYETH A Corporation of the State of Delaware, USA , KIM, Keun-Sik , KIM, Kwang-il , LEE, Sung-Woo , PARK, Jin-Soo , CHAI, Ki-Byung
发明人： KIM, Keun-Sik , KIM, Kwang-il , LEE, Sung-Woo , PARK, Jin-Soo , CHAI, Ki-Byung
IPC分类号： C07C253/30
CPC分类号： C07C253/30 , C07C2601/14 , C07C255/37
摘要： A process for the preparation of cyclohexanol derivatives of formula (I) by reacting a compound of formula (II) with a compound of formula (III) in the presence of a base catalyst of formula (IV) or (V). In the above formula, R 1 -R 9 , A, B, X and p have tghe meanings given in the specification.
摘要翻译：在式（Ⅳ）或（Ⅴ）的碱催化剂存在下，使式（Ⅳ）化合物与式（Ⅳ）化合物反应制备式（Ⅰ）的环己醇衍生物的方法。在上式中，R1-R9，A，B，X和p具有本说明书中给出的含义。

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