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1. 发明申请

WO2006093728A2 PROCESS IMPROVEMENT USING SOLUBILITY CHARACTERISTICS 审中-公开
标题翻译：使用溶解度特性进行工艺改进
公开(公告)号：WO2006093728A2
公开(公告)日：2006-09-08
申请号：PCT/US2006/006135
申请日：2006-02-21
申请人： MALLINCKRODT INC. , GENTILCORE, Michael, J. , PERIASAMY, Muthunadar, P.
发明人： GENTILCORE, Michael, J. , PERIASAMY, Muthunadar, P.
IPC分类号： C07C201/12 , C07C205/57 , C07B41/12
CPC分类号： C07C201/12 , C07C205/57
摘要： The present invention is directed to a process of maximizing the solubility of a nonelectrolyte solute in a solvent by operating within an optimal temperature range at conditions wherein the nonelectrolyte solute is not a pure liquid. In particular, the process of the present invention is directed to conversion of a carboxylic acid compound to an ester under conditions wherein the solubility of the ester in an alcoholic solvent approaches ideal solubility behavior.
摘要翻译：本发明涉及通过在非电解质溶质不是纯液体的条件下在最佳温度范围内操作来使非电解质溶质在溶剂中的溶解度最大化的方法。特别地，本发明的方法涉及在酯在醇溶剂中的溶解度接近理想溶解度行为的条件下将羧酸化合物转化为酯。

2. 发明申请

WO2004002926A3 PURIFICATION OF N,N-DIMETHYLACETAMIDE 审中-公开
公开(公告)号：WO2004002926A3
公开(公告)日：2004-01-08
申请号：PCT/US2003/019405
申请日：2003-06-18
申请人： MALLINCKRODT INC. , GENTILCORE, Michael, J.
发明人： GENTILCORE, Michael, J.
IPC分类号： B01D3/14
摘要： A method to purify N,N-dimethylacetamide (DMAc) from an aqueous solution containing acetic acid as a contaminant. Two fractional distillation columns (10, 20) are arranged in series. The first column (10) has a condenser (11) overhead and a reboiler (13) at the bottom. The second column (20) also has a condenser (21) overhead and a reboiler (23) at the bottom. The solution containing the contaminant is provided to the first column (10) with a temperature profile to result in acetic acid partitioning into the overhead water. The material remaining in the bottom portion of the first column is recycled to the first column and also provided in a second column (20), whereby DMAc free of acetic acid contamination is recovered, and remaining DMAc and acetic acid are returned to the first column for further separation.

3. 发明申请

WO2009029464A1 REMOVAL OF SILICA FROM WATER SOLUBLE COMPOUNDS BY NANOFILTRATION AND REVERSE PHASE CHROMATOGRAPHY 审中-公开
标题翻译：通过硝化和反相色谱从水溶性化合物中除去二氧化硅
公开(公告)号：WO2009029464A1
公开(公告)日：2009-03-05
申请号：PCT/US2008/073796
申请日：2008-08-21
申请人： MALLINCKRODT INC. , BAILEY, Allan, R. , WHITE, David, H. , KASPAR, Derick, L. , VANDAS, Robert, E. , GENTILCORE, Michael, J. , NGUYEN, Hung, V. , FUKUNAGA, Anna, K.
发明人： BAILEY, Allan, R. , WHITE, David, H. , KASPAR, Derick, L. , VANDAS, Robert, E. , GENTILCORE, Michael, J. , NGUYEN, Hung, V. , FUKUNAGA, Anna, K.
IPC分类号： B01D61/02 , A61K49/04 , B01D15/32
CPC分类号： B01D61/027 , A61K49/0433 , A61K49/103 , A61K49/106 , B01D15/325 , B01D2315/16
摘要： A process for separating soluble silica species such as monomeric silicic acid (or monosilicic acid) and low molecular weight soluble polymeric silica from impure water soluble compounds by membrane nanofiltration is provided. A process for separating soluble silica species and colloidal silica from impure water soluble compounds by reverse phase liquid chromatography is also provided.
摘要翻译：提供了通过膜纳滤法从不纯的水溶性化合物中分离可溶性二氧化硅物质例如单体硅酸（或单硅酸）和低分子量可溶性聚合二氧化硅的方法。还提供了通过反相液相色谱从可溶性水溶性化合物中分离可溶性二氧化硅物质和胶体二氧化硅的方法。

4. 发明申请

WO2006093728A3 PROCESS IMPROVEMENT USING SOLUBILITY CHARACTERISTICS 审中-公开
标题翻译：使用可溶性特征的工艺改进
公开(公告)号：WO2006093728A3
公开(公告)日：2006-11-16
申请号：PCT/US2006006135
申请日：2006-02-21
申请人： MALLINCKRODT INC , GENTILCORE MICHAEL J , PERIASAMY MUTHUNADAR P
发明人： GENTILCORE MICHAEL J , PERIASAMY MUTHUNADAR P
IPC分类号： C07C201/12 , C07B41/12 , C07C205/57
CPC分类号： C07C201/12 , C07C205/57
摘要： The present invention is directed to a process of maximizing the solubility of a nonelectrolyte solute in a solvent by operating within an optimal temperature range at conditions wherein the nonelectrolyte solute is not a pure liquid. In particular, the process of the present invention is directed to conversion of a carboxylic acid compound to an ester under conditions wherein the solubility of the ester in an alcoholic solvent approaches ideal solubility behavior.
摘要翻译：本发明涉及通过在非电解质溶质不是纯液体的条件下在最佳温度范围内操作使非电解质溶质在溶剂中的溶解度最大化的方法。特别地，本发明的方法涉及在酯在醇类溶剂中的溶解度达到理想溶解行为的条件下将羧酸化合物转化为酯。

5. 发明申请

WO2004002926A2 PURIFICATION OF N,N-DIMETHYLACETAMIDE 审中-公开
标题翻译： N，N-二甲基乙酰胺的纯化
公开(公告)号：WO2004002926A2
公开(公告)日：2004-01-08
申请号：PCT/US0319405
申请日：2003-06-18
申请人： MALLINCKRODT INC , GENTILCORE MICHAEL J
发明人： GENTILCORE MICHAEL J
IPC分类号： B01D3/14 , B01D3/42 , C07C231/24 , C07C233/05 , C07C
CPC分类号： C07C231/24 , B01D3/146 , Y10S203/09 , C07C233/05
摘要： A method to purify N,N-dimethylacetamide (DMAc) from an aqueous solution containing acetic acid as a contaminant. Two fractional distillation columns are arranged in a series. The solution containing the contaminant is provided to the first column with a temperature profile to result in acetic acid partitioning into the overhead water. The material remaining in the bottom portion of the first column is recycled to the first column and also provided into a second column, whereby DMAc free of acetic acid contamination is recovered, and remaining DMAc and acetic acid are returned to the first column for further separation. The method uses standard fractional distillation procedures and equipment, thus eliminating the need for more complex extractions and/or chromatographic separations.
摘要翻译：从含有乙酸作为污染物的水溶液中净化N，N-二甲基乙酰胺（DMAc）的方法。两个分馏塔排列成一系列。将含有污染物的溶液以温度分布提供给第一塔，导致乙酸分配到塔顶水中。残留在第一塔底部的材料被再循环到第一塔并且还提供到第二塔中，由此回收不含乙酸污染的DMAc，并且将剩余的DMAc和乙酸返回到第一塔进行进一步分离。该方法使用标准的分馏程序和设备，因此不需要更复杂的萃取和/或色谱分离。

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