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1. 发明申请

WO1995000589A1 PROCESS FOR PREPARING CERAMIC-LIKE MATERIALS AND THE CERAMIC-LIKE MATERIALS 审中-公开
标题翻译：制备陶瓷材料和陶瓷材料的方法
公开(公告)号：WO1995000589A1
公开(公告)日：1995-01-05
申请号：PCT/PL1993000013
申请日：1993-08-12
申请人： CYRKIEWICZ, Marceli , HERLING, Erwin , KLESZCZEWSKI, Jacek
IPC分类号： C08L67/00
CPC分类号： C08L63/00 , C08L67/00 , C08L67/06 , C08L2666/18
摘要： This invention is concerned with a process for preparing ceramic-like materials suitable for a wide range of application, by binding an inorganic filler of a grain size of up to 20 mu m, used in the form of phosphogypsum or phosphogypsum and magnetite, or phosphogypsum and glass-forming oxides, with epoxy resin or a mixture of epoxy resin and polyester resin, the latter amounting to 80 % by volume, with the volume ratio of the resin component to the filler being 1:0.45-2. The resultant ceramic-like materials are water resistant and can be easily formed, also by casting, and additionally by mechanical working, if required. The ceramic-like materials containing magnetite show magnetic properties, while those containing glass-forming oxides are able to absorb an X-radiation of 45-55 keV and a hard radiation of 0.6-1.25 MeV. The addition of an expanding agent such as butyl isocyanate to the raw composition makes it possible to prepare an expanded material with completely closed pores. Due to very good adhesion of the ceramic-like to metal, glass, plastics, concrete it can be easily joined with these materials both during the polymerization process and after its termination, also by using a prepolymerized composition as a binder.
摘要翻译：本发明涉及通过将以磷石膏或磷石膏和磁铁矿或磷石膏形式使用的至多20μm的晶粒尺寸的无机填料结合在一起制备适用于广泛应用的陶瓷类材料的方法。和环氧树脂或环氧树脂和聚酯树脂的混合物的玻璃形成氧化物，后者为80体积％，树脂组分与填料的体积比为1:0.45-2。所得到的陶瓷状材料是防水的，并且可以通过铸造容易地形成，并且如果需要，另外通过机械加工。含有磁铁矿的陶瓷状材料显示磁性，而含有玻璃形成氧化物的陶瓷状材料能够吸收45-55keV的X射线和0.6-1.25MeV的硬辐射。向原料组合物中加入异氰酸丁酯等发泡剂可以制备具有完全闭孔的发泡材料。由于陶瓷类与金属，玻璃，塑料，混凝土的非常好的粘附性，在聚合过程中和其终止之后，也可以通过使用预聚合的组合物作为粘合剂，容易地与这些材料接合。

2. 发明申请

WO1995000583A1 PROCESS FOR PREPARING CERAMIC-LIKE MATERIALS AND THE CERAMIC-LIKE MATERIALS 审中-公开
标题翻译：制备陶瓷材料和陶瓷材料的方法
公开(公告)号：WO1995000583A1
公开(公告)日：1995-01-05
申请号：PCT/PL1993000012
申请日：1993-08-12
申请人： CYRKIEWICZ, Marceli , HERLING, Erwin , KLESZCZEWSKI, Jacek
IPC分类号： C08K03/00
CPC分类号： H01F1/113 , C04B18/0445 , C04B26/18 , C04B2111/00258 , C04B2111/00422 , C04B2111/00862 , C08K3/32 , Y02W30/91 , C04B14/308 , C04B24/00 , C04B14/22 , C04B38/02 , C08L67/06
摘要： This invention relates to a process for preparing ceramic-like materials with specific properties by binding an inorganic filler in the form of a dry composition with a grain size of up to 25 mu m, containing in the volume ratio 1:0.-1.52 a waste phosphogypsum and magnetite or glass-forming oxides, with an unsaturated polyester resin in an amount of 46-220 volume parts per 100 volume parts of the filler. The use of magnetite makes it possible to prepare materials with magnetic properties, while glass-forming oxides enable preparing materials effective to absorb an X-radiation of 45-55 keV and a hard radiation of 0.6-1.25 MeV. When an expanding agent is added to the raw composition according to this invention, an expanded material is obtained, having completely closed pores, particularly useful in the building industry. The resultant ceramic-like materials are characterized by good adhesion to metals, plastics, glass, wood, concrete and can be easily joined with them both at the stage of polymerization and after its termination by using a prepolymerized resin as a binder.
摘要翻译：本发明涉及一种制备具有特定性能的陶瓷状材料的方法，该方法是将粒径达25μm的干组合物形式的无机填料与体积比1：-0.1.52a 废磷石膏和磁铁矿或玻璃形成氧化物，其中不饱和聚酯树脂的量为46-220体积份/ 100体积份填料。使用磁铁矿使得可以制备具有磁性能的材料，而玻璃形成氧化物使得能够制备有效吸收45-55keV的X射线和0.6-1.25MeV的硬辐射的材料。当根据本发明的原料组合物中加入发泡剂时，获得具有完全闭孔的膨胀材料，在建筑工业中特别有用。所得到的陶瓷状材料的特征在于对金属，塑料，玻璃，木材，混凝土具有良好的粘合性，并且可以在聚合阶段和通过使用预聚合树脂作为粘合剂在其终止后容易地与它们连接。

3. 发明申请

WO1995028440A1 A PROCESS FOR THE MANUFACTURE OF POLYMERIC MATERIALS WITH A HIGH CHEMICAL AND MECHANICAL RESISTANCE AND POLYMERIC MATERIALS WITH A HIGH CHEMICAL AND MECHANICAL RESISTANCE 审中-公开
标题翻译：具有高化学和机械电阻的高分子材料和具有高化学和机械电阻的聚合材料的制备方法
公开(公告)号：WO1995028440A1
公开(公告)日：1995-10-26
申请号：PCT/PL1995000005
申请日：1995-03-15
申请人： CYRKIEWICZ, Marceli , HERLING, Erwin , KLESZCZEWSKI, Jacek , KLESZCZEWSKI, Jacek
IPC分类号： C08K03/32
CPC分类号： C08K3/32 , C08L67/06
摘要： The process for the manufacture of materials with a high chemical and mechanical resistance consists in that per each 100 parts by volume of vinylester resin treated with 0.85-1.47 parts by volume of an accelerant in the form of cobalt naphthenate, there are added at least in two batches 50-900 parts by volume of an inorganic filler constituting previously roasted at a temperature not lower than 470 K disintegrated to a particle size of at least 30 mu m phosphogypsum or a composition of phosphogypsum with glass-forming oxides or phosphogypsum with magnetite or phosphogypsum with microsphere, after which on continuous stirring there is added, if necessary, up to 60 parts by volume of styrene and/or up to 0.2 parts by volume of dimethylaniline, and then the whole is polymerized in the presence of known initiators such as organic peroxides. The materials with a high chemical and mechanical resistance constitute polymerized composition of synthetic resin and inorganic fillers, consisting of 7.5-88.1 % by weight of vinylester resin, styrene and/or a low-molecular-weight unsaturated polyester resin in a quantity up to 34.1 % by weight, and 14.3-86.6 % by weight of phosphogypsum or 0.4-46.6 % by weight of phosphogypsum and 6.4-44.8 % by weight of glass-forming oxides or 4.6-53.5 % by weight of microsphere or 5.5-42.1 % by weight of magnetite. The process for the manufacture of these materials makes it possible to utilize industrial wastes resulted from production of phosphoric acid, while the material itself in all its varieties is characterized by a very good resistance to aggresive media, also at elevated temperatures, and suitable for processing by mechanical methods as well as for combining with other materials by using to that end an incompletely polymerized composition of the material.
摘要翻译：用于制造具有高化学和机械阻力的材料的方法在于每100体积份用0.85-1.47体积份的环烷酸钴形式的促进剂处理的乙烯基酯树脂，至少加入两批50-900份体积的预先在不低于470K的温度下焙烧的无机填料分散至至少30μm磷石膏的粒径或具有玻璃形成氧化物或磷石膏的磷石膏组合物或磁铁矿，或磷石膏与微球，然后在连续搅拌下加入高达60体积份苯乙烯和/或最多0.2体积份二甲基苯胺，然后在已知的引发剂如有机过氧化物。具有高化学和机械阻力的材料构成合成树脂和无机填料的聚合组合物，由7.5-88.1重量％的乙烯基酯树脂，苯乙烯和/或低至34.1的量的低分子量不饱和聚酯树脂组成，磷石膏的重量百分比为14.3-86.6％，磷石膏为0.4-46.6重量％，玻璃形成氧化物为6.4-44.8重量％，微球为4.6-5.35重量％，重量为5.5-42.1重量％的磁铁矿。制造这些材料的过程使得可以利用由磷酸生产产生的工业废物，而其所有品种的材料本身的特征在于在高温下也具有非常好的抗侵蚀性介质，并且适用于加工通过机械方法以及通过使用该材料的不完全聚合的组合物与其它材料结合。

4. 发明申请

WO1999003795A1 METHOD AND APPARATUS FOR THE PROCESSING OF PHOSPHATE GYPSUM WASTE 审中-公开
标题翻译：磷酸盐废水处理方法与装置
公开(公告)号：WO1999003795A1
公开(公告)日：1999-01-28
申请号：PCT/GR1997000030
申请日：1997-07-15
申请人： KARAGEORGIS, Ioannis , KLESZCZEWSKI, Jacek , CYRKIEWICZ, Marceli
发明人： KARAGEORGIS, Ioannis
IPC分类号： C04B11/02
CPC分类号： C04B28/04 , C01F11/468 , C04B11/02 , C04B11/0285 , C04B11/30 , C04B26/02 , C04B2111/00732 , C04B2111/0075 , C04B2111/60 , C09K17/10 , F27B7/02 , F27B7/10 , F27B7/166 , Y02W30/91 , Y02W30/92 , C04B11/26 , C04B14/06 , C04B14/305 , C04B18/0445 , C04B18/08
摘要： The present invention relates to a method for the wasteless processing of great quantities of phosphate gypsum waste into a form suitable for use as additive in colours, enamels, synthetic resins, and as binding component for especially loose soils for road constructions. The method for processing of phosphate gypsum waste consists of three heating steps in the temperature range of 460-650 K during about 60 minutes until pH over 5,9 is obtained. The process is running in machinery which includes a horizontal rotating chamber (1), on the inside of which on the axis a fixed cylinder (2) is attached, wherethrough a heating factor is passing in opposite direction. The rotating chamber (1) consists of three processing zones (3), (4), (5). The first zone (3) has on the inner periphery loosely set chain units (7), the second zone (4) is equipped with a worm-wheel (8) firmly set on the fixed cylinder (2), and the third zone (5) has on the full length a free hanging chain unit (11) and at least two rows of flat wing units (12).
摘要翻译：本发明涉及一种将大量磷酸盐石膏废料无害化处理成适合用作颜料，搪瓷，合成树脂添加剂的形式的方法，以及用于道路施工的特别松散的土壤的结合组分。磷酸石膏废料的处理方法由温度范围为460-650K，约60分钟内的三个加热步骤组成，直到获得pH超过5,9。该过程在包括水平旋转室（1）的机械中运行，在其上的内侧上安装有固定气缸（2），通过加热因子通过相反方向。旋转室（1）由三个处理区（3），（4），（5）组成。第一区域（3）在内周上松动地设置链条单元（7），第二区域（4）配备有牢固地设置在固定筒体（2）上的蜗轮（8）和第三区域 5）全长具有自由悬挂链单元（11）和至少两排平翼单元（12）。

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