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11. 发明申请

WO2012166836A2 METHOD FOR CAPTURING AND RECYCLING IRON CATALYST USED IN THE PRODUCTION OF HALOALKANE COMPOUNDS 审中-公开
标题翻译：用于生产氢化铝化合物的铁电催化剂的回收和回收方法
公开(公告)号：WO2012166836A2
公开(公告)日：2012-12-06
申请号：PCT/US2012040070
申请日：2012-05-31
申请人： HONEYWELL INT INC , CLOSE JOSHUA , WANG HAIYOU , TUNG HSUEH SUNG , COTTRELL STEPHEN A
发明人： CLOSE JOSHUA , WANG HAIYOU , TUNG HSUEH SUNG , COTTRELL STEPHEN A
IPC分类号： B01J23/745 , B01J19/08 , B01J19/20 , C07C21/06
CPC分类号： B01J8/10 , B01J8/005 , B01J8/0075 , B01J23/745 , B03C1/0335 , B03C5/00 , C07C17/275 , C07C17/278 , Y02P20/584 , C07C19/01
摘要： Disclosed is a method for capturing and recycling iron catalyst used in the production of haloalkane compounds and more particularly, to an improved process for the manufacture of the compound 1,1,1,3,3-pentachloropropane (HCC-240fa), in which an electromagnetic separation unit (EMSU) is used to facilitate the reaction. When energized, the EMSU functions to remove the iron particles from the reactor effluent; when de-energized, the iron particles captured by the EMSU can be flushed back into the reactor for re-use in the continued production of HCC-240fa. The present invention is also useful in the manufacturing processes for other haloalkane compounds such as HCC-250 and HCC-360.
摘要翻译：公开了一种用于捕获和再循环用于制备卤代烷烃化合物的铁催化剂的方法，更具体地说，涉及制备化合物1,1,1,3,3-五氯丙烷（HCC-240fa）的改进方法，其中使用电磁分离单元（EMSU）来促进反应。当通电时，EMSU用于从反应器流出物中除去铁颗粒; 当断电时，由EMSU捕获的铁颗粒可以冲洗回反应器，以便在继续生产HCC-240fa时重新使用。本发明也可用于其它卤代烷烃化合物如HCC-250和HCC-360的制备方法。

12. 发明申请

WO2011056441A3 INTEGRATED PROCESS FOR FLUORO-OLEFIN PRODUCTION 审中-公开
标题翻译：氟 - 烯烃生产的集成工艺
公开(公告)号：WO2011056441A3
公开(公告)日：2011-09-15
申请号：PCT/US2010053486
申请日：2010-10-21
申请人： HONEYWELL INT INC , KOPKALLI HALUK , CHIU YUON , COTTRELL STEPHEN A , TUNG HSUEH SUNG , ULRICH KEVIN D
发明人： KOPKALLI HALUK , CHIU YUON , COTTRELL STEPHEN A , TUNG HSUEH SUNG , ULRICH KEVIN D
IPC分类号： C07C17/20 , C07C17/25 , C07C21/18 , C09K5/02
CPC分类号： C07C21/18 , C01B7/0718 , C01B7/0737 , C01B7/195 , C07C17/087 , C07C17/10 , C07C17/206 , C07C17/25 , Y02P20/125 , C07C19/10
摘要： Disclosed is a process for the manufacture of HFO-1234yf from TCP in three integrated steps that include hydrofluorination of TCP (tetrachloropropene) to HCFC-1233xf in the vapor phase followed by hydrofluorination of HCFC-1233xf to HCFC-244bb in the liquid phase which is then followed by dehydrochlorination in liquid or vapor phase to produce HFO-1234yf. The vapor phase hydrofluorination is carried out at a higher pressure than the liquid phase hydrofluorination, thereby eliminating the need for compression and/or intermediate recovery. Also, any HCl generated from this reaction is fed to the liquid phase hydrofluorination section to promote agitation and mixing. This results in a more economical process from an initial capital and operating cost versus conducting the 3-steps sequentially.
摘要翻译：公开了一种由TCP以三个整合步骤制造HFO-1234yf的方法，其包括在气相中将TCP（四氯丙烯）氢氟化为HCFC-1233xf，接着在液相中将HCFC-1233xf氢氟化为HCFC-244bb 然后在液相或汽相中进行脱氯化氢反应，生成HFO-1234yf。气相氢氟化在比液相氢氟化更高的压力下进行，由此消除了压缩和/或中间回收的需要。而且，由该反应产生的任何HCl被供给到液相氢氟化部分以促进搅拌和混合。这从最初的资本和运营成本中获得了更经济的过程，而不是依次进行3个步骤。

13. 发明申请

WO2011025674A4 HYDROGENATION PROCESS FOR FLUOROCARBONS 审中-公开
标题翻译：氟化氢加氢过程
公开(公告)号：WO2011025674A4
公开(公告)日：2011-05-12
申请号：PCT/US2010045416
申请日：2010-08-13
申请人： HONEYWELL INT INC , KOPKALLI HALUK , CHIU YUON , RODRIGUES ORLANDO GEORGE , CERRI GUS , TUNG HSUEH SUNG , COTTRELL STEPHEN A
发明人： KOPKALLI HALUK , CHIU YUON , RODRIGUES ORLANDO GEORGE , CERRI GUS , TUNG HSUEH SUNG , COTTRELL STEPHEN A
IPC分类号： B01J8/06 , C07C17/354 , C07C19/08
CPC分类号： B01J8/067 , B01J2208/00849 , B01J2208/00884 , C07C17/354 , C07C19/08
摘要： Disclosed is a process and apparatus for the catalytic hydrogenation of fluoroolefins to fluorocarbons where the reaction is carried out in a multi-tube shell and tube reactor. Reactions involving hydrogenation of fluoro-olefins are typically exothermic. In commercial processes where a fluoro-olefin C(n)H(2n-x)F(x) to C(n)H(2n-x+2)F(x) is hydrogenated (e.g. hexafluoropropylene to 236ea, 1225ye to 245eb, and the like), inadequate management or control of heat removal may induce excess hydrogenation, decomposition and hot spots resulting in reduced yields and potential safety issues. In the hydrogenation of fluoro-olefins, it is therefore necessary to control the reaction temperature as precisely as practical to overcome challenges associated with heat management and safety.
摘要翻译：公开了将氟烯烃催化氢化成碳氟化合物的方法和装置，其中反应在多管壳管式反应器中进行。涉及氟代烯烃氢化的反应通常是放热的。在氟化烯烃C（n）H（2n-x）F（x）至C（n）H（2n-x + 2）F（x）被氢化（例如六氟丙烯至236ea，1225ye至245eb），等等），不充分的除热控制或控制可能引起过度的氢化，分解和热点，导致产量降低和潜在的安全问题。在氟代烯烃的氢化中，因此需要精确地控制反应温度以克服与热管理和安全相关的挑战。

14. 发明申请

WO2004106271A2 METHOD OF MAKING HYDROFLUOROCARBONS 审中-公开
标题翻译：制备氢氟碳化合物的方法
公开(公告)号：WO2004106271A2
公开(公告)日：2004-12-09
申请号：PCT/US2004016231
申请日：2004-05-21
申请人： HONEYWELL INT INC , TUNG HSUEH SUNG , COTTRELL STEPHEN A , MARKS CHAD L
发明人： TUNG HSUEH SUNG , COTTRELL STEPHEN A , MARKS CHAD L
IPC分类号： C07C17/20 , C07C17/21 , C07C17/00
CPC分类号： C07C17/21 , C07C17/206 , C07C19/08
摘要： A manufacturing process for making hydrofluorocarbons (HFCs), by reacting a hydrochlorocarbon and HF in a liquid phase catalytic reactor using a large mole ratio of HF to hydrochlorocarbon to minimize formation of high boiling byproducts and improve HF consumption and hydrofluorocarbon yields.
摘要翻译：通过使用大量摩尔比的HF与氢氯化碳在液相催化反应器中使氢氟烃和HF反应制备氢氟烃（HFCs）的制造方法，以最小化高沸点副产物的形成并提高HF消耗量和氢氟碳化合物产率。

15. 发明申请

WO2012166754A2 METHOD FOR AVOIDING THE GENERATION OF BY-PRODUCTS DURING THE PRODUCTION OF HALOALKANE COMPOUNDS 审中-公开
标题翻译：避免生成HALOALKANE化合物时副产物生成的方法
公开(公告)号：WO2012166754A2
公开(公告)日：2012-12-06
申请号：PCT/US2012039914
申请日：2012-05-30
申请人： HONEYWELL INT INC , CLOSE JOSHUA , WANG HAIYOU , TUNG HSUEH SUNG
发明人： CLOSE JOSHUA , WANG HAIYOU , TUNG HSUEH SUNG
IPC分类号： C07C17/275 , B01J23/745 , C07C19/01
CPC分类号： C07C17/278 , B01J23/745 , B01J35/023 , C07C17/275 , C07C19/01
摘要： Disclosed is a process for the manufacture of haloalkane compounds, and more particularly, to an improved process for the manufacture of the compound 1,1,1,3,3-pentachloropropane (HCC-240fa), which mitigates the formation of by-products. The present invention is also useful in the manufacture of other haloalkane compounds such as HCC-250 and HCC-360. One embodiment of the process comprises a method and system for avoiding the formation of polyvinyl chloride during the production of HCC-240fa from CCl4, in which vinyl chloride (VCM) is fed into a reactor as a vapor instead of as a liquid, using a diffusing device to further increase the contact surface between VCM vapor and CCl4.
摘要翻译：公开了一种制备卤代烷烃化合物的方法，更具体地说，涉及制备化合物1,1,1,3,3-五氯丙烷（HCC-240fa）的改进方法，其减少了副产物的形成。本发明也可用于制备其它卤代烷烃化合物如HCC-250和HCC-360。该方法的一个实施方案包括在CCl 4生产HCC-240fa期间避免形成聚氯乙烯的方法和系统，其中将氯乙烯（VCM）作为蒸气而不是作为液体加入到反应器中，使用扩散装置进一步增加VCM蒸气与CCl4之间的接触面。

16. 发明申请

WO2011119370A3 METHOD FOR MAKING HEXAFLUORO-2-BUTENE 审中-公开
标题翻译：制备六氟-2-丁烯的方法
公开(公告)号：WO2011119370A3
公开(公告)日：2011-12-22
申请号：PCT/US2011028476
申请日：2011-03-15
申请人： HONEYWELL INT INC , TUNG HSUEH SUNG , WANG HAIYOU
发明人： TUNG HSUEH SUNG , WANG HAIYOU
IPC分类号： C07C17/20 , B01J23/26 , B01J27/10 , C07C17/23 , C07C21/18
CPC分类号： C07C21/18 , C07B2200/09 , C07C17/206 , C07C17/25 , C07C17/278 , C07C17/358 , C07C19/10
摘要： Hexafluoro-2-butene (HFO-1336) is a low global warming potential blowing agent, refrigerant and solvent. This invention provides a method for making the compound, including the cis-isomer, from the readily available raw materials, carbon tetrachloride and 3,3,3-trifluoropropene. The trans-isomer formed in the process can be isomerized into cis-isomer by the use of an isomerization catalyst.
摘要翻译：六氟-2-丁烯（HFO-1336）是一种低全球升温潜能值的发泡剂，制冷剂和溶剂。本发明提供了由容易获得的原料，四氯化碳和3,3,3-三氟丙烯制备包括顺式异构体的化合物的方法。在该方法中形成的反式异构体可以通过使用异构化催化剂异构化为顺式异构体。

17. 发明申请

WO2011119388A3 PROCESS FOR THE MANUFACTURE OF HEXAFLUORO-2-BUTENE 审中-公开
标题翻译：十六烷基二丁二烯的制备方法
公开(公告)号：WO2011119388A3
公开(公告)日：2011-12-15
申请号：PCT/US2011028608
申请日：2011-03-16
申请人： HONEYWELL INT INC , TUNG HSUEH SUNG , WANG HAIYOU
发明人： TUNG HSUEH SUNG , WANG HAIYOU
IPC分类号： C07C17/20 , B01J23/26 , B01J27/10 , C07C17/23 , C07C21/18
CPC分类号： C07C21/18 , C07B2200/09 , C07C17/206 , C07C17/25 , C07C17/275 , C07C17/278 , C07C17/358 , C07C19/10 , C07C21/04 , C07C19/01
摘要： Hexafluoro-2-butene (HFO-1336) is a low global warming potential blowing agent, refrigerant and solvent. This invention provides methods for making the compound, including the cis-isomer, from the readily available raw materials, carbon tetrachloride and ethylene. The trans-isomer formed in the process can be isomerized into cis-isomer by the use of an isomerization catalyst.
摘要翻译：六氟-2-丁烯（HFO-1336）是全球变暖潜能低的发泡剂，制冷剂和溶剂。本发明提供从容易获得的原料四氯化碳和乙烯制备包括顺式异构体的化合物的方法。该方法中形成的反式异构体可以通过使用异构化催化剂异构化成顺式异构体。

18. 发明申请

WO2011017138A3 HYDROGENATION CATALYST 审中-公开
标题翻译：加氢催化剂
公开(公告)号：WO2011017138A3
公开(公告)日：2011-06-23
申请号：PCT/US2010043460
申请日：2010-07-28
申请人： HONEYWELL INT INC , WANG HAIYOU , TUNG HSUEH SUNG , MERKEL DANIEL C
发明人： WANG HAIYOU , TUNG HSUEH SUNG , MERKEL DANIEL C
IPC分类号： B01J23/38 , B01J23/70 , B01J37/02 , C07C17/25 , C07C19/08
CPC分类号： B01J32/00 , B01J21/04 , B01J23/36 , B01J23/40 , B01J23/44 , B01J23/48 , B01J23/70 , B01J35/1014 , B01J37/18 , C07C17/354 , C07C19/08
摘要： An alpha-alumina support for a hydrogenation catalyst useful in hydrogenating fluoroolefins is provided.
摘要翻译：提供了用于加氢氟代烯烃的氢化催化剂的α-氧化铝载体。

19. 发明申请

WO2009064939A3 MANUFACTURE OF 1,1,1,2,3,3-HEXAFLUOROPROPANE AND 1,1,1,2-TETRAFLUOROPROPANE VIA CATALYTIC HYDROGENATION 审中-公开
标题翻译： 1,1,1,2,3,3-十六烷基和1,1,1,2-四氢呋喃的制备通过催化氢化
公开(公告)号：WO2009064939A3
公开(公告)日：2009-08-13
申请号：PCT/US2008083479
申请日：2008-11-14
申请人： HONEYWELL INT INC , YANG SHUWU , TUNG HSUEH SUNG
发明人： YANG SHUWU , TUNG HSUEH SUNG
IPC分类号： C07C17/38 , B01J23/72 , B01J23/745 , B01J23/75 , B01J23/755 , C07C19/08
CPC分类号： C07C17/354 , B01J21/18 , B01J23/26 , B01J23/40 , B01J23/42 , B01J23/48 , B01J23/70 , B01J23/72 , B01J23/75 , B01J23/755 , C07C19/08
摘要： A process for producing hydrofluorocarbon compounds represented by the following formula: CF3CHFCHm+1Fn wherein m is 0, 1, or 2; n is 0, 1, or 2; and m + n = 2. The process has the step of contacting, i.e., reacting, hydrogen with a precursor compound represented by the following formula: CF3CF=CHmFn wherein m is 0, 1, or 2; n is 0, 1, or 2; and m + n = 2. The contact is carried out in the presence of a solid catalyst and in the presence or absence of an inert gas. The catalyst is selected from the group consisting of: Fe, Co, Ni, Cu, Cr, Ru, Rh, Ag, Re, Os, Ir, Pt, Au, Sn, and any combinations thereof. For the hydrogenation of 1234yf to 254eb, Pd can also be used as catalyst in addition to the other above-referenced metals. These metals are preferably supported on a carrier such as activated carbon.
摘要翻译：由下式表示的氢氟烃化合物的制造方法：CF 3 CHFCH m + 1 F n其中m为0,1或2; n为0,1或2; 并且m + n = 2。该方法具有使氢与由下式表示的前体化合物接触，即使其反应的步骤：CF 3 CF = CH m F n，其中m为0,1或2; n为0,1或2; 并且m + n = 2。该接触在固体催化剂存在下和在惰性气体存在或不存在下进行。催化剂选自：Fe，Co，Ni，Cu，Cr，Ru，Rh，Ag，Re，Os，Ir，Pt，Au，Sn及其任何组合。对于1234yf至254eb的氢化，除了其它上述金属之外，Pd也可用作催化剂。这些金属优选负载在载体如活性炭上。

20. 发明申请

WO2007058836A8 1,1,1,3,3,3-HEXAFLUOROPROPANE PURIFICATION WITH PHOTOCHLORINATION EQUIPMENT 审中-公开
标题翻译： 1,1,1,3,3,3-HEXAFLORORROPANE用光电设备进行纯化
公开(公告)号：WO2007058836A8
公开(公告)日：2008-08-14
申请号：PCT/US2006043417
申请日：2006-11-08
申请人： HONEYWELL INT INC , CHIU YUON , MERKEL DAVID , TUNG HSUEH SUNG
发明人： CHIU YUON , MERKEL DAVID , TUNG HSUEH SUNG
IPC分类号： C07C17/395 , C07C19/08
CPC分类号： C07C17/38 , C07C17/395 , C07C19/08
摘要： A continuous, vapor phase method for purifying a crude mixture of 1,1,1,3,3,3-hexafluoropropane and one or more unsaturated fluorocarbon compounds, the process comprising: a) providing a photochlorinator vessel comprising : 1) a UV lamp unit comprising a UV lamp located in a transparent inner well, the transparent inner well being located within a transparent outer well, the outer well being provided with material for cooling walls of the inner and outer wells; the inner well and the outer well defining separate chambers isolated from each other; and 2) a reaction vessel into which the UV lamp unit has been inserted; b) introducing into the reaction vessel a gaseous mixture of Cb and a distillation inseparable mixture of 1,1,1,3,3,3-hexafluoropropane and one or more unsaturated fluorocarbon compdunds; c) reacting, in the gaseous state and in the presence of UV light from the photochlorinator, the mixture with CI 2 with the distillation inseparable mixture of 1,1,1,3,3,3-hexafluoropropane and one or more unsaturated compounds to saturate unsaturated fluorocarbons into a reacted mixture, and d) separating a purified 1, 1,1, 3,3, 3-hexafluoroporpane product containing less than 1000 ppm, most preferably less than 100 ppm unsaturated fluorocarbons.
摘要翻译：一种用于纯化1,1,1,3,3,3-六氟丙烷和一种或多种不饱和碳氟化合物的粗混合物的连续气相法，该方法包括：a）提供光氯化器容器，其包括：1）UV灯该单元包括位于透明内部井中的UV灯，所述透明内部井位于透明外部井内，所述外部井具有用于冷却所述内部和外部井的壁的材料; 所述内部井和所述外部井定义分离的彼此隔离的室; 和2）UV灯单元插入其中的反应容器; b）向反应容器中引入Cb的气态混合物和1,1,1,3,3,3-六氟丙烷与一种或多种不饱和氟碳化合物的蒸馏不可分离的混合物; c）以气态和在来自光氯提取器的紫外光的存在下，与CI 2的混合物与1,1,1,3,3,3-六氟丙烷的蒸馏不可分离的混合物反应和一种或多种使不饱和碳氟化合物饱和至反应混合物中的不饱和化合物，和d）分离含有小于1000ppm，最优选小于100ppm的不饱和碳氟化合物的纯化1,1,1,3,3,3-六氟丙烷产物。

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