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1. 发明授权

US10982033B2 Polymer production method and radical polymerization initiating group-containing compound 有权
公开(公告)号：US10982033B2
公开(公告)日：2021-04-20
申请号：US16066972
申请日：2017-02-22
申请人： DAINICHISEIKA COLOR & CHEMICALS MFG. CO., LTD.
发明人： Hiroyuki Shimanaka , Yoichi Tagi , Yoshikazu Murakami
IPC分类号： C08F293/00 , C08F220/14 , C08F8/14 , C08F265/06 , C08F8/18 , C08F4/08 , C08F2/06 , C08F2/38 , C08F220/18 , C08F257/02 , C08F263/04 , C08K3/16 , C08K5/101 , C08K5/20 , C08K5/3417 , C08L101/00
摘要： The present invention provides: a novel production technique that enables production of a polymer whose molecular weight and molecular weight distribution are controlled and production of a polymer having a complicated structure in a desirably controlled manner using commercially available materials without using a radical polymerization initiator or a special material for use in living radical polymerization and without the need for strict polymerization conditions; and a radical polymerization initiating group-containing compound for use in the technique. The present invention relates to: a method for producing a polymer, the method including a polymerization step of mixing and warming (1) a radically polymerizable monomer, (2) an organic compound wherein at least one group that functions as a group for initiating polymerization of the monomer and that has a structure represented by formula 1 or formula 2 (X in the formula represents Cl or Br) is introduced in a molecule of the organic compound, and (3) an iodine-containing compound, thereby initiating, from the group having the structure, radical polymerization accompanied by a termination reaction; and the organic compound of (2) for use in the method.

2. 发明授权

US10562989B2 Fluorine-containing boric acid PVB composite 有权
公开(公告)号：US10562989B2
公开(公告)日：2020-02-18
申请号：US15557349
申请日：2016-03-10
申请人： UNIMATEC CO., LTD. , HIROSAKI UNIVERSITY
发明人： Takeshi Fukushima , Katsuyuki Sato , Hideo Sawada
IPC分类号： C08F8/18
摘要： A fluorine-containing boric acid PVB composite comprising a condensate of a fluorine-containing alcohol, boric acid and polyvinyl butyral, wherein the fluorine-containing alcohol is represented by the general formula: Rf(A-OH)k wherein k is 1 or 2; when k is 1, Rf is a perfluoroalkyl group having 6 or less carbon atoms, a polyfluoroalkyl group in which some of the fluorine atom or atoms of the perfluoroalkyl group are replaced by hydrogen atom or atoms, a polyfluoroalkyl group containing a terminal perfluoroalkyl group having 6 or less carbon atoms and a perfluoroalkylene group having 6 or less carbon atoms, or a linear or branched, perfluoroalkyl group containing a terminal perfluoroalkyl group having 6 or less carbon atoms, a perfluoroalkylene group having 6 or less carbon atoms and ether bonds; when k is 2, Rf is a linear or branched, perfluoroalkylene group or polyfluoroalkylene group, containing a perfluoroalkylene group having 6 or less carbon atoms and ether bonds; and A is an alkylene group having 1 to 6 carbon atoms.

3. 发明授权

US09410006B2 Fluorine-containing highly branched polymer and resin composition containing the same 有权
标题翻译：含氟的高支化聚合物和含有它的树脂组合物
公开(公告)号：US09410006B2
公开(公告)日：2016-08-09
申请号：US13322722
申请日：2010-05-31
申请人： Masayuki Haraguchi , Motonobu Matsuyama , Masaaki Ozawa , Misao Miyamoto
发明人： Masayuki Haraguchi , Motonobu Matsuyama , Masaaki Ozawa , Misao Miyamoto
IPC分类号： B32B3/00 , C08F8/18 , C08F220/22 , C08F2/48 , C08F220/18 , C08L67/04 , C09D4/06 , C09D133/16 , C08F220/24 , C08L33/16 , C08F212/36 , C08F222/10
CPC分类号： C08J3/28 , C08F2/48 , C08F212/36 , C08F220/18 , C08F220/22 , C08F220/24 , C08F222/1006 , C08J2335/02 , C08J2433/16 , C08L33/12 , C08L33/16 , C08L35/02 , C08L67/04 , C09D4/06 , C09D133/16 , C09D135/02 , Y10T428/24802 , C08L2666/04 , C08F265/06 , C08F2220/325
摘要： It is an object to provide a compound that can provide a molded article and a coating film excellent not only in solubility in an organic solvent, but also in miscibility with/dispersibility in a matrix resin, causing no aggregation in a matrix resin, excellent in surface modification property, and having high transparency. A fluorine-containing highly branched polymer obtained by polymerizing a monomer A having two or more radical polymerizable double bonds in the molecule thereof with a monomer B having a fluoroalkyl group and at least one radical polymerizable double bond in the molecule thereof in the presence of a polymerization initiator C in a content of 5% by mol or more and 200% by mol or less, based on the total molar amount of the monomer A and the monomer B; and a resin composition comprising the polymer.
摘要翻译：本发明的目的是提供一种化合物，其可以提供不仅在有机溶剂中的溶解性，而且在基质树脂中的混溶性/分散性优异的模塑制品和涂膜，不会在基体树脂中发生聚集，优异的表面改性性，透明度高。一种含氟高支链聚合物，其通过在其分子中在其分子中聚合具有两个或更多个可自由基聚合的双键的单体A与其分子中具有氟烷基和至少一个自由基聚合双键的单体聚合引发剂C的含量相对于单体A和单体B的总摩尔量为5摩尔％以上且200摩尔％以下。和包含该聚合物的树脂组合物。

4. 发明授权

US09243084B2 Method for producing chlorinated hyperbranched polymer 有权
标题翻译：生产氯化超支化聚合物的方法
公开(公告)号：US09243084B2
公开(公告)日：2016-01-26
申请号：US14003911
申请日：2012-03-02
申请人： Hideo Nagashima , Keisuke Kojima , Akihiro Tanaka , Keisuke Odoi , Osamu Uesugi
发明人： Hideo Nagashima , Keisuke Kojima , Akihiro Tanaka , Keisuke Odoi , Osamu Uesugi
IPC分类号： C08F8/20 , C08F8/18
CPC分类号： C08F8/20 , C08F8/18 , C08G83/006
摘要： There is provided a novel production method of a chlorinated hyperbranched polymer that is optically stable and is capable of derivatizing the chlorinated hyperbranched polymer into various compounds. A production method of a chlorinated hyperbranched polymer for producing a chlorinated hyperbranched polymer of Formula (1): {where X is a chlorine atom; R1 is a hydrogen atom or a methyl group; and A1 is a phenylene-alkylene group, n is the number of repeating unit structures and is an integer of 2 to 100,000}, comprising the step of substituting a dithiocarbamate group of a hyperbranched polymer of Formula (3): (where R1, A1, and n are the same as defined in Formula (1); and each of R2 and R3 is a C1-5 alkyl group, a C1-5 hydroxyalkyl group, or a C7-12 arylalkyl group, or R2 and R3 optionally form a ring together with a nitrogen atom bonded to R2 and R3) with a chlorine atom using sulfuryl chloride.
摘要翻译：提供了一种光学稳定且能将氯化超支化聚合物衍生成各种化合物的氯化超支化聚合物的新型制备方法。用于制备式（1）的氯化超支化聚合物的氯化超支化聚合物的制备方法：其中X是氯原子; R1是氢原子或甲基; A1是亚苯基 - 亚烷基，n是重复单元结构的数量，为2〜100,000的整数}，包括用式（3）的超支化聚合物的二硫代氨基甲酸酯基取代的步骤：（其中R1，A1 和n与式（1）中所定义相同; R 2和R 3各自为C 1-5烷基，C 1-5羟基烷基或C 7-12芳烷基，或者R 2和R 3可任选地形成与使用磺酰氯的氯原子与R2和R3键合的氮原子一起环。

5. 发明授权

US08236900B2 Modified polyolefin resin and uses thereof 有权
标题翻译：改性聚烯烃树脂及其用途
公开(公告)号：US08236900B2
公开(公告)日：2012-08-07
申请号：US12375032
申请日：2007-07-18
申请人： Yasutaka Watanabe , Kenichi Fujino , Hidetoshi Yoshioka , Naoshi Nagai , Sadahiko Matsuura
发明人： Yasutaka Watanabe , Kenichi Fujino , Hidetoshi Yoshioka , Naoshi Nagai , Sadahiko Matsuura
IPC分类号： C08F8/18 , C08F8/46 , C08F8/02
CPC分类号： C08L23/0815 , C08F8/00 , C08F255/00 , C08F255/02 , C08F299/00 , C08L23/10 , C08L51/06 , C08L2205/02 , C08L2666/02 , C08L2666/04 , C09J151/06 , C09J155/005 , C08F10/00 , C08L2666/24 , C08L2666/06
摘要： It is an object of the present invention to provide a modified polyolefin resin adhesive agent which is excellent in adhesiveness to a nonpolar substrate, particularly a poorly adhesive polyolefin substrate to which no surface treatment has been given and to a polar substrate, develops the excellent adhesiveness by drying or thermal compression bonding at relatively low temperature, and exhibits a low tack. That is, the present invention provides the modified polyolefin resin obtained by modifying a polyolefin resin with (A) a polarity imparting agent which is at least one selected from chlorine, unsaturated carboxylic acid, derivatives and anhydrides of unsaturated carboxylic acid and radical polymerizable monomers; and (B) an ethylene-α-olefin copolymer having an unsaturated bond at one end, and use of said modified polyolefin resin as an aqueous resin composition or an organic solvent resin composition.
摘要翻译：本发明的目的是提供一种与非极性基材，特别是不进行表面处理的粘合性差的聚烯烃基材和极性基材粘合性优异的改性聚烯烃树脂粘合剂，具有优异的粘合性通过在相对低的温度下进行干燥或热压接，并且具有低的粘性。也就是说，本发明提供了通过（A）极性赋予剂（其为选自氯，不饱和羧酸，不饱和羧酸的衍生物和酸酐和自由基聚合性单体）中的至少一种来改性聚烯烃树脂而获得的改性聚烯烃树脂; 和（B）一端具有不饱和键的乙烯-α-烯烃共聚物，使用所述改性聚烯烃树脂作为水性树脂组合物或有机溶剂树脂组合物。

6. 发明授权

US08198379B2 Halobutyl elastomers 有权
标题翻译：卤丁基弹性体
公开(公告)号：US08198379B2
公开(公告)日：2012-06-12
申请号：US11989650
申请日：2006-08-02
申请人： John Scott Parent , Ralph Allen Whitney , Sergio A. Guillén-Castellanos , Rui Resendes
发明人： John Scott Parent , Ralph Allen Whitney , Sergio A. Guillén-Castellanos , Rui Resendes
IPC分类号： C08F8/18 , C08F36/08 , C08F36/06 , C08F8/34 , C07C253/00
CPC分类号： C08L23/283 , C08F8/00 , C08F8/30 , C08L23/22 , C08L2666/02 , C08F8/26 , C08F8/20 , C08F210/12
摘要： The present invention relates to the modification of butyl elastomers, particularly halobutyl elastomers, under solvent free conditions with a phase transfer catalyst in the presence of an alkyl metal salt of an oxygen or sulfur-based nucleophile.
摘要翻译：本发明涉及在无溶剂条件下使用相转移催化剂在氧或硫基亲核试剂的烷基金属盐存在下改性丁基弹性体，特别是卤代丁基弹性体。

7. 发明授权

US08143354B2 Process for preparing acid-terminated ATRP products 失效
标题翻译：制备酸封端的ATRP产品的方法
公开(公告)号：US08143354B2
公开(公告)日：2012-03-27
申请号：US12373892
申请日：2007-05-15
申请人： Sven Balk , Gerd Loehden , Christine Miess , Christine Troemer , Monika Maerz
发明人： Sven Balk , Gerd Loehden , Christine Miess , Christine Troemer , Monika Maerz
IPC分类号： C08F20/44 , C08F36/00 , C08F8/34 , C08F36/08 , C08F36/06 , C08F8/18
CPC分类号： C08F8/34 , C08F8/26 , C08F220/18
摘要： The present invention relates to the in situ acid end group functionalization of polymer chains which have been prepared by means of atom transfer radical polymerization, and to the simultaneous removal of transition metals from polymer solutions.
摘要翻译：本发明涉及通过原子转移自由基聚合制备的聚合物链的原位酸端基官能化，以及同时从聚合物溶液中除去过渡金属。

8. 发明申请

US20120029154A1 GRAFTING METHOD TO IMPROVE CHROMATOGRAPHY MEDIA PERFORMANCE 审中-公开
标题翻译：提高色谱介质性能的方法
公开(公告)号：US20120029154A1
公开(公告)日：2012-02-02
申请号：US13191376
申请日：2011-07-26
申请人： Martin J. Deetz , John J. Maikner
发明人： Martin J. Deetz , John J. Maikner
IPC分类号： C08F8/18
CPC分类号： B01J20/3278 , B01J20/264 , B01J20/286 , B01J39/26 , B01J41/20
摘要： The invention also relates to improvements in the method of grafting polymeric ligands onto substrates used in protein separations, resulting in substrates having improved protein binding capacity, improved purification process operating windows and resin selectivity, and relating to making and using the same.
摘要翻译：本发明还涉及将聚合物配体接枝到蛋白质分离中使用的底物上的方法的改进，导致具有改善的蛋白质结合能力的底物，改进的纯化方法操作窗口和树脂选择性，以及制备和使用它们。

9. 发明申请

US20110250164A1 Antimicrobial Copolymer for Coating Surfaces, Obtained by Derivatization of a Vinylamine-Vinylalcohol Copolymer 审中-公开
标题翻译：用于涂料表面的抗微生物共聚物通过乙烯胺 - 乙烯醇共聚物的衍生获得
公开(公告)号：US20110250164A1
公开(公告)日：2011-10-13
申请号：US13140884
申请日：2009-12-03
申请人： John J. Stofko, Jr.
发明人： John J. Stofko, Jr.
IPC分类号： A01N33/02 , C08F8/18 , C08L29/04 , A01P1/00
CPC分类号： A01N25/34 , C08F8/02 , C08F8/12 , C08K5/04 , C08K5/06 , C08K5/101 , C09D5/1637 , C09D129/04 , A01N33/04
摘要： A composition including the reaction product of at least a vinylamine-vinyl alcohol copolymer; an epoxyalkane; and a fluorocarbon that includes a reactive portion capable of reacting with the vinylamine-vinyl alcohol copolymer. Articles including coatings of such compositions, methods of preparing antimicrobial water-repellant surfaces and methods of preparing an antimicrobial water-repellant composition are also included.
摘要翻译：包含至少乙烯胺 - 乙烯醇共聚物的反应产物的组合物; 环氧烷烃以及包含能够与乙烯胺 - 乙烯醇共聚物反应的反应部分的碳氟化合物。包括这种组合物的涂层，制备抗菌防水表面的方法和制备抗微生物防水组合物的方法的制品也包括在内。

10. 发明授权

US07825195B2 Dendrimers of rubbery polymers 失效
标题翻译：橡胶聚合物的树枝状聚合物
公开(公告)号：US07825195B2
公开(公告)日：2010-11-02
申请号：US12611807
申请日：2009-11-03
申请人： Adel Farhan Halasa , Wen-Liang Hsu , Chad Aaron Jasiunas
发明人： Adel Farhan Halasa , Wen-Liang Hsu , Chad Aaron Jasiunas
IPC分类号： C08C19/25 , C08F8/18 , C08F36/04 , C08J3/24 , B60C1/00
CPC分类号： C08C19/44 , B60C1/0016 , C08G83/003 , C08L15/00 , C08L101/005 , Y10T152/10 , Y10T152/10495
摘要： This invention discloses a process for synthesizing a dendrimer of a rubbery polymer comprising: (a) reacting a lithium terminated rubbery polymer with a halogenated silicon containing compound to produce a polymer which is terminated with halogenated silicon moieties, wherein the halogenated silicon contain compound has at least four halogen atoms which are bonded directly to silicon atoms, wherein the ratio of the lithium terminated rubbery polymer to halogen atoms in the halogenated silicon containing compound is within the range of 2:n to (n-1):n, wherein n represents the number of halogen atoms that are bonded directly to silicon atoms in the halogenated silicon containing compound, wherein the halogenated silicon containing compound contains at least three halogen atoms which are bonded directly to a silicon atom; (b) reacting the polymer which is terminated with halogenated silicon moieties with a molar excess of a tertiary alcohol to produce a polymer which is terminated with hydroxy silyl moieties; and (c) allowing the polymer which is terminated with the hydroxy silyl moieties to couple under conditions sufficient to produce a dendrimer containing siloxane linkages. It has also be found that similar dendrimers having improved processability can be make utilizing halogenated tin containing compounds in stead of the halogenated silicon containing compound.
摘要翻译：本发明公开了一种用于合成橡胶状聚合物树枝状聚合物的方法，其包括：（a）使锂封端的橡胶状聚合物与含卤化硅的化合物反应以制备用卤化硅部分封端的聚合物，其中卤化硅含有化合物在至少四个与硅原子直接键合的卤素原子，其中锂封端的橡胶状聚合物与含卤化硅化合物中的卤素原子的比例在2：n至（n-1）：n的范围内，其中n表示与卤代硅化合物中的硅原子直接键合的卤素原子数，其中含卤化硅的化合物含有至少三个与硅原子直接键合的卤素原子; （b）将用卤代硅部分封端的聚合物与摩尔过量的叔醇反应，以产生用羟基甲硅烷基部分封端的聚合物; 和（c）使在羟基甲硅烷基部分封端的聚合物在足以产生含有硅氧烷键的树枝状聚合物的条件下偶联。还可以发现，具有改进加工性能的类似树枝状大分子可以利用含卤化锡的化合物代替含卤化硅的化合物。

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