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1. 发明授权

US08636890B2 Method for refurbishing PtAl coating to turbine hardware removed from service 有权
标题翻译：将PtAl涂层翻新到从服务中除去的涡轮机硬件的方法
公开(公告)号：US08636890B2
公开(公告)日：2014-01-28
申请号：US13242548
申请日：2011-09-23
申请人： Nicholas Shawn Woodard , Michael H. Rucker , John Louis Cupito , Richard R. Worthing, Jr. , Albert King
发明人： Nicholas Shawn Woodard , Michael H. Rucker , John Louis Cupito , Richard R. Worthing, Jr. , Albert King
IPC分类号： C25D17/00 , C25D5/02 , C25D5/34 , C25D7/00 , B23P6/00 , C25D17/12 , F01D5/00 , C23C10/02 , C23C10/58 , C25D3/50 , F01D5/28
CPC分类号： B23P6/002 , C23C10/02 , C23C10/58 , C25D3/50 , C25D5/02 , C25D5/50 , C25D7/008 , C25D17/00 , C25D17/007 , C25D17/008 , C25D17/06 , C25D17/10 , C25D17/12 , F01D5/005 , F01D5/288
摘要： A method of repairing damaged airfoils. The method comprises the steps of stripping thermal barrier coatings from the airfoil. After the coatings are removed, cracks are removed from the airfoil. Cracks that appear in the bond coat area over the airfoil fillet portion are removed by locally grit blasting the fillet portion of the airfoil. This operation also results in locally removing the bond coating from the fillet portion. Cracks and other damage sustained by the airfoil tip are removed and replaced by welding superalloy material. The airfoil then may be cleaned by thermal etching. The airfoil is then placed in a plating tool permitting preferential plating of airfoil areas from which plating has been removed. After plating, the airfoil is then heat treated to diffuse the platinum coating with the superalloy substrate materials. The diffusion heat treated airfoil is aluminided by any aluminiding process, forming a PtAl coating.
摘要翻译：修复受损翼型的方法。该方法包括从翼型件剥离热障涂层的步骤。在去除涂层之后，从翼型上除去裂纹。出现在机翼片部分上的粘合涂层区域中的裂纹通过局部喷砂来喷射翼型件的圆角部分而被去除。该操作也导致从圆角部分局部去除粘结涂层。由翼面尖端保持的裂纹和其他损伤被去除并由焊接超合金材料代替。然后可以通过热蚀刻来清洁翼型件。然后将翼型件放置在电镀工具中，允许优先电镀已经从其中去除电镀的翼型区域。电镀后，然后对该翼型进行热处理，以使铂镀层与超合金基板材料扩散。通过任何铝化处理使扩散热处理的翼型铝化，形成PtAl涂层。

2. 发明授权

US07138189B2 Heat-resistant Ti alloy material excellent in resistance to corrosion at high temperature and to oxidation 失效
标题翻译：耐高温钛合金材料耐高温腐蚀和氧化
公开(公告)号：US07138189B2
公开(公告)日：2006-11-21
申请号：US10509028
申请日：2003-03-25
申请人： Toshio Narita , Takumi Nishimoto
发明人： Toshio Narita , Takumi Nishimoto
IPC分类号： B32B15/00 , C22C14/00 , C23C10/38 , C23C10/58
CPC分类号： C23C28/021 , C22C14/00 , C23C10/16 , C23C10/56 , C23C28/028 , Y10T428/12458 , Y10T428/12743 , Y10T428/12806
摘要： Disclosed is a heat-resistant Ti alloy material excellent in high-temperature corrosion resistance and oxidation resistance, which comprises a base made of a heat-resistant Ti alloy and a surface layer formed on the surface of the base. The surface layer has a multilayer structure including an inner layer and an outer layer. The inner layer has three coexistent phases consisting of a β phase, a γ phase and a Laves phase in the phase diagram of a Ti—Al—Cr based alloy, and the outer layer is made of an Al—Ti—Cr based alloy having an Al concentration of 50 atomic % or more. The heat-resistant Ti alloy material is produced by subjecting a substrate made of a heat-resistant Ti alloy to a Cr diffusion treatment at a temperature within a β single-phase region in the phase diagram of a Ti—Al—Cr based alloy, precipitating a γ phase and a Laves phase from the β phase during a cooling process to form the inner layer with three coexistent phases consisting of the β, γ and Laves phases, and then subjecting the obtained product to an Al diffusion treatment to form the outer layer. The heat-resistant Ti alloy material can prevent the diffusion of Al from the outer layer to the base and the diffusion of elements of the base to the outer layer while forming a protective Al2O3 film in a self-repairing manner, to provide excellent high-temperature corrosion resistance and oxidation resistance to the heat-resistant Ti alloy base.
摘要翻译：本发明公开了一种耐高温耐氧化性优异的耐热性Ti合金材料，其特征在于，包括由耐热Ti合金构成的基体和形成在基材表面的表面层。表面层具有包括内层和外层的多层结构。内层在Ti-Al-Cr基合金的相图中具有由β相，γ相和Laves相组成的三个共存相，外层由Al-Ti-Cr基合金制成，其具有 50原子％以上的Al浓度。耐热性Ti合金材料通过在Ti-Al-Cr系合金的相图中，使耐热Ti合金的基板在β单相区域内的温度下进行Cr扩散处理而制造，在冷却过程中从β相沉淀出γ相和Laves相，以形成由β，γ和Laves相组成的三个共存相的内层，然后将所得产物进行Al扩散处理以形成外层层。耐热Ti合金材料可以防止Al从外层扩散到基底，并且可以在形成保护性Al 2 O 3的同时将基体的元素扩散到外层以自修复方式，以耐热Ti合金基材提供优异的耐高温耐腐蚀性和抗氧化性。

3. 发明申请

US20050287388A1 Metal based resistance heating element and method for preparation therefor 失效
标题翻译：金属基电阻加热元件及其制备方法
公开(公告)号：US20050287388A1
公开(公告)日：2005-12-29
申请号：US10519802
申请日：2003-06-30
申请人： Toshio Narita
发明人： Toshio Narita
IPC分类号： C22C21/00 , C22C27/00 , C23C10/02 , C23C10/28 , C23C10/52 , C23C10/58 , C23C26/00 , C23C28/00 , C23C28/02 , C23C30/00 , C25D5/10 , C25D5/50 , C25D7/06 , H05B3/12 , B32B15/01
CPC分类号： C23C28/021 , C23C10/02 , C23C10/52 , C23C10/58 , C23C26/00 , C23C28/028 , H05B3/12 , Y10T428/12458 , Y10T428/12736 , Y10T428/12771 , Y10T428/12875 , Y10T428/12944
摘要： Discloses is a metal-based resistance heat-generation element. The element comprises a core made of a platinum group metal or refractory metal, and a coating film formed on the core. The coating film has at least two layers including a core-side inner layer of a Re—Cr based σ (sigma) phase and a surface-side outermost layer of an aluminide or silicide. Alternatively, the element may comprise a core made of an alloy containing a platinum group metal or refractory metal and Re and Cr diffused therein, and a coating film formed on the core. The coating film has at least one layer including an aluminide or silicide layer.
摘要翻译：公开了一种金属基电阻发热元件。元件包括由铂族金属或难熔金属制成的芯和形成在芯上的涂膜。涂膜具有至少两层，包括Re-Cr系的σ（sigma）相的芯侧内层和铝化物或硅化物的表面侧最外层。或者，元件可以包括由包含铂族金属或难熔金属的合金制成的芯，并且在其中扩散的Re和Cr以及形成在芯上的涂膜。涂膜具有至少一层包括铝化物或硅化物层。

4. 发明授权

US6080246A Method of aluminising a superalloy 失效
标题翻译：高温合金的镀铝方法
公开(公告)号：US6080246A
公开(公告)日：2000-06-27
申请号：US892588
申请日：1997-07-14
申请人： Rodney G. Wing
发明人： Rodney G. Wing
IPC分类号： C23C10/02 , C22C19/05 , C23C10/06 , C23C10/28 , C23C10/48 , C23C10/58 , C23C12/00 , C23C14/14 , C23C16/06 , C23C28/02 , C23C10/16 , C23C10/50
CPC分类号： C23C28/021 , C23C10/58 , C23C28/023 , C23C28/028
摘要： A high rhenium containing single crystal superalloy (30) is chromized, or coated with cobalt, before the conventional aluminising process steps to modify the surface of the high rhenium containing single crystal superalloy to prevent the formation of topologically close packed phases at the interface between the aluminide coating (32) and the rhenium containing single crystal superalloy. The invention is particularly applicable to platinum aluminide coatings, platinum aluminide-silicide coatings and aluminide-silicide coatings.
摘要翻译：在常规的铝化工艺步骤之前，将高铼含有单晶超合金（30）镀铬或涂覆有钴，以改变含高铼单晶超耐热合金的表面，以防止在该界面上形成拓扑紧密堆积相铝化物涂层（32）和含铼单晶超合金。本发明特别适用于铂铝化物涂层，铂铝化硅 - 硅化物涂层和铝化硅 - 硅化物涂层。

5. 发明授权

US5989734A Aluminum product having metal diffusion layer, process for producing the same, and paste for metal diffusion treatment 失效
标题翻译：具有金属扩散层的铝制品，其制造方法和用于金属扩散处理的糊料
公开(公告)号：US5989734A
公开(公告)日：1999-11-23
申请号：US934754
申请日：1997-09-22
申请人： Hirohisa Miura , Nagayoshi Matsubara , Yasuhiro Yamada , Haruzo Katoh , Takashi Watsuji
发明人： Hirohisa Miura , Nagayoshi Matsubara , Yasuhiro Yamada , Haruzo Katoh , Takashi Watsuji
IPC分类号： C23C10/36 , C23C10/30 , C23C10/58 , C23C12/02 , B32B15/00
CPC分类号： C23C12/02 , C23C10/30 , Y10T428/12778
摘要： An aluminum product having the metal diffusion layer in the present invention has, on the surface thereof, a metal diffusion layer comprising aluminum and a diffusion metal which is diffused setting aluminum as a matrix and which includes at least one selected from the group consisting of Ni, Cr, Cu, Zn, Mg, Ti and Ag; wherein the diffusion layer is formed by diffusing inclinatorily not less than 1 .mu.m from the surface thereof; and the diffusion metal is not less than 1.0% by weight when the whole of the metal diffusion layer is set to be 100% by weight. Also, in a process for producing an aluminum product having a metal diffusion layer, the surface of the aluminum product is brought into contact with the processing agent including at least the diffusion metal powder; and in this state by conducting heat treatment in the atmosphere including nitrogen, the diffusion metal is diffused on the surface of the aluminum product and the metal diffusion layer is formed. Thus, the present invention supplies the aluminum product having the metal diffusion layer on the surface thereof and the process for producing the aluminum product having this kind of metal diffusion layer on the surface thereof.
摘要翻译：本发明的具有金属扩散层的铝制品在其表面上具有包含铝和扩散金属的金属扩散层，扩散金属以铝为基质扩散，并且包括选自Ni ，Cr，Cu，Zn，Mg，Ti和Ag; 其特征在于，所述扩散层通过从其表面不均匀地扩散至少1μm而形成。并且当全部金属扩散层设定为100重量％时，扩散金属不小于1.0重量％。此外，在具有金属扩散层的铝制品的制造方法中，使铝制品的表面与至少包含扩散金属粉末的处理剂接触，通过在包括氮的气氛中进行热处理，在该状态下，扩散金属扩散到铝制品的表面，形成金属扩散层。因此，本发明在其表面上提供具有金属扩散层的铝制品及其表面上具有这种金属扩散层的铝制品的制造方法。

6. 发明授权

US5958204A Enhancement of coating uniformity by alumina doping 失效
标题翻译：通过氧化铝掺杂增强涂层均匀性
公开(公告)号：US5958204A
公开(公告)日：1999-09-28
申请号：US938169
申请日：1997-09-26
申请人： George Edward Creech , Paul Stephen Korinko , Michael Joe Barber , Subhash K. Naik
发明人： George Edward Creech , Paul Stephen Korinko , Michael Joe Barber , Subhash K. Naik
IPC分类号： C23C10/58 , C25D13/02
CPC分类号： C25D13/02 , C23C10/58
摘要： A method of controlling the final coating thickness of a diffused aluminide coating on a metal substrate. The method includes: (a) depositing an alumina-doped platinum-silicon powder onto a metal substrate, (b) heating the coated substrate to diffuse the platinum-silicon powder into the substrate and removing the undiffused scale, (c) depositing an aluminum-bearing powder onto the platinum-silicon-enriched substrate, and (d) heating the coated substrate to diffuse the aluminum-bearing powder into the substrate and removing the undiffused scale. The depositions are preferably done electrophoretically, in which case the Pt--Si deposition bath is doped with alumina or some other inert particulate. Alternatively, slurry deposition may be used. The method may also be used to deposit Pd--Si coatings onto metal substrates.
摘要翻译：控制金属基底上扩散的铝化物涂层的最终涂层厚度的方法。该方法包括：（a）将氧化铝掺杂的铂硅粉末沉积到金属基底上，（b）加热涂覆的基底以将铂硅粉末扩散到基底中并去除未扩散的刻度，（c）沉积铝并且（d）加热涂覆的基材以将含铝粉末扩散到基材中并除去未扩散的氧化皮。沉积物优选地进行电泳，在这种情况下，Pt-Si沉积浴中掺杂有氧化铝或其它惰性颗粒。或者，可以使用浆料沉积。该方法也可用于将Pd-Si涂层沉积在金属基底上。

7. 发明授权

US5922409A Method for forming a coating substantially free of deleterious refractory elements on a nickel- and chromium-based superalloy 失效
$Method for forming a coating substantially free of deleterious refractory elements on a nickel- and chromium-based superalloy$
标题翻译：在镍基和铬基超级合金上形成基本上不含有害耐火材料的涂层的方法
公开(公告)号：US5922409A
公开(公告)日：1999-07-13
申请号：US802661
申请日：1997-02-19
申请人： Bruce G. McMordie , Thomas A. Kircher
发明人： Bruce G. McMordie , Thomas A. Kircher
IPC分类号： C23C10/20 , C23C10/18 , C23C10/28 , C23C10/44 , C23C10/48 , C23C10/58 , C23C30/00 , B05D3/02
CPC分类号： C23C10/26 , Y10T428/12458 , Y10T428/1275 , Y10T428/12944
摘要： The oxidation and corrosion resistance of a nickel-base alloy are enhanced by a process which includes first enriching the surface of an alloy substrate with platinum, as by electrolytic deposition, and then simultaneously diffusing aluminum and silicon from a molten state into the platinum-enriched substrate. The invention further provides coatings and coated substrates with enhanced oxidation and corrosion resistance.
摘要翻译：镍基合金的抗氧化和耐腐蚀性通过包括首先通过电解沉积使铂富集合金基底的表面，然后将铝和硅从熔融状态同时扩散到富铂的方法来增强基质。本发明还提供具有增强的抗氧化和耐腐蚀性的涂层和涂覆的基材。

8. 发明授权

US5409748A Heat radiating tube for annealing furnace, with ceramic coated on the inside thereof 失效
标题翻译：用于退火炉的散热管，其内部涂有陶瓷
公开(公告)号：US5409748A
公开(公告)日：1995-04-25
申请号：US815078
申请日：1991-12-27
申请人： Jin W. Song , Soon Y. Whang , Byong K. Sung
发明人： Jin W. Song , Soon Y. Whang , Byong K. Sung
IPC分类号： C21D1/34 , C21D9/00 , C23C4/02 , C23C4/04 , C23C10/58 , F23D14/12 , F27D99/00 , B32B15/04
CPC分类号： F27D99/0035 , C21D9/0006 , C23C4/02 , Y02T50/67 , Y10T428/12292 , Y10T428/131 , Y10T428/1317
摘要： A heat radiating tube for an annealing furnace is disclosed. An aluminide layer and an aluminum diffusion sublayer are formed by an aluminum diffusion coating method on one side or both sides of the tube portions which are subjected during use to high temperature oxidation corrosion. Subsequently, a coating of MCrAlY is applied on selected inside portions exposed to the combustion gas flame collision in order to reinforce the bonding strength of the protective coating. A layer of ceramic is then coated thereupon. Prior to applying the MCrAlY and ceramic coatings, the tube surface to be coated is ground to a depth equal to the coating thicknesses in order to make the heights of the coated layer and the surface of the remaining portions of the tube even each other.
摘要翻译：公开了一种用于退火炉的散热管。通过铝扩散涂覆法，在使用中经受高温氧化腐蚀的管部分的一侧或两侧上形成铝化物层和铝扩散子层。随后，在暴露于燃烧气体火焰碰撞的选定内部施加MCrAlY涂层，以增强保护涂层的粘接强度。然后在其上涂覆一层陶瓷。在施加MCrAlY和陶瓷涂层之前，待涂覆的管表面被研磨至等于涂层厚度的深度，以使涂层的高度和管的剩余部分的表面彼此均匀。

9. 发明授权

US4965095A Method for refurbishing used jet engine hot section airfoils 失效
标题翻译：二手喷气发动机热区翼型的翻新方法
公开(公告)号：US4965095A
公开(公告)日：1990-10-23
申请号：US289595
申请日：1988-12-22
申请人： Alfonso L. Baldi
发明人： Alfonso L. Baldi
IPC分类号： B22F7/00 , B65D43/02 , C06B21/00 , C06B45/00 , C06B45/14 , C06C15/00 , C08F283/01 , C09D5/04 , C23C10/02 , C23C10/04 , C23C10/06 , C23C10/30 , C23C10/34 , C23C10/42 , C23C10/56 , C23C10/58 , C23C10/60 , C23C12/02 , C23C22/74 , G01N15/00 , G01N21/35 , G01N21/47
CPC分类号： B22F7/002 , B65D43/022 , C06B21/0083 , C06B45/00 , C06B45/14 , C06C15/00 , C08F283/01 , C09D5/04 , C23C10/02 , C23C10/04 , C23C10/06 , C23C10/30 , C23C10/34 , C23C10/42 , C23C10/56 , C23C10/58 , C23C10/60 , C23C12/02 , C23C22/74 , B65D2543/00092 , B65D2543/0037 , B65D2543/00435 , B65D2543/00509 , B65D2543/00546 , F05B2250/62 , G01N2015/0046 , H05K2201/0209 , Y02T50/67
摘要： Workpieces are very rapidly diffusion coated by heating the packed workpiece at a rate that brings the workpiece to diffusion-coating temperature and then completing the diffusion coating, all in less than 50 minutes, then cooling. Workpiece can have top coating layer of aluminum flake covered by a layer of extremely fine alumina or silica in a magnesium chromate binder, to provide surface having roughness at least about 10 micro-inches smoother than before the top coating. Used aluminized jet engine hot section members can be reconditioned by a fluoridizing treatment that deoxidizes and also removes residual aluminizing, so that the members can then be repaired if necessary and re-aluminized.
摘要翻译：通过以使工件扩散涂覆温度然后在不到50分钟内完成扩散涂层然后冷却的速度加热填充的工件来快速地扩散工件。工件可以在铬酸铬粘合剂中具有由极细的氧化铝或二氧化硅层覆盖的铝薄片的顶部涂层，以提供比顶涂层之前更平滑的至少约10微英寸的表面。二氧化铝喷射发动机热段成员可以通过氟化处理进行再生处理，其脱氧并除去残余的镀铝，从而可以在必要时修复成员并再次镀铝。

10. 发明授权

US4528215A Diffusion aluminizing of cobalt-base superalloys 失效
标题翻译：钴基超级合金的扩散镀铝
公开(公告)号：US4528215A
公开(公告)日：1985-07-09
申请号：US548937
申请日：1983-11-07
申请人： Alfonso L. Baldi , Victor V. Damiano
发明人： Alfonso L. Baldi , Victor V. Damiano
IPC分类号： B01J35/04 , C23C10/02 , C23C10/40 , C23C10/48 , C23C10/56 , C23C10/58 , C23C10/60 , C23C11/00 , C23C13/00
CPC分类号： C23C10/40 , B01J35/04 , C23C10/02 , C23C10/48 , C23C10/56 , C23C10/58 , C23C10/60
摘要： In the pack diffusion coating of chromium into the surface of a superalloy, the formation of undesirable oxide inclusion is reduced when the diffusion coating pack contains at least about 3% Ni.sub.3 Al. Also the formation of alpha-chromium is reduced when the pack diffusion is carried out in a retort effectively not over five inches in height. On the other hand an alpha-chromium-rich layer at least 0.2 mil thick can be deliberately formed and the superalloy thus coated subjected to an aluminizing treatment to convert the alpha-chromium into islands that provide very high sulfidation resistance. Pack aluminizing in the presence of chromium makes a very effective aluminum- or chromium-containing top coating over platinum plated or platinum coated nickel-base superalloys. Depletion of diffusible material from workpieces heated in a powder-pack can also provide a surface on which aluminizing produces a highly impact-resistant coating.
摘要翻译：在将包含在超级合金表面中的铬扩散涂层中，当扩散涂层包含至少约3％Ni 3 Al时，形成不期望的氧化物夹杂物减少。当包装扩散在有效地不超过五英寸高的蒸馏器中进行时，还可以减少α-铬的形成。另一方面，可以有意地形成至少0.2密耳厚的富铬的层，并且如此涂覆的超级合金进行镀铝处理以将α-铬转化为提供非常高的耐硫化性的岛。在镀铬的情况下，镀铝处理使镀铂或镀铂镍基超级合金上的铝或铬的顶涂层非常有效。从粉末包装中加热的工件中消散可扩散材料还可以提供一种表面，在该表面上，铝化产生高度耐冲击的涂层。

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