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    • 2. 发明授权
    • Process for the obtention of fructose and fructose-rich syrups from
xerophyte plants
    • 从干旱植物中获取果糖和果糖丰富的糖浆的方法
    • US4138272A
    • 1979-02-06
    • US851657
    • 1977-11-15
    • Enrique Zepeda-Castillo, deceasedby Isaura N. Vda. de Zepeda, executrix
    • Enrique Zepeda-Castillo, deceasedby Isaura N. Vda. de Zepeda, executrix
    • C13B5/00C13C1/00C13D3/02C13K11/00
    • C13B5/00
    • A process for the obtention of fructose and fructose-rich syrups from xerophyte plants, particularly of the genus Amarillidaceae, such as Agave, comprises separately collecting the plant material consisting of the leaf portions and the core portions of the plant; admixing and washing with water said plant materials; chopping the washed plant material to form small pieces and recovering the juices released by the chopping operation; subjecting the chopped material to an extraction process with an aqueous liquor expressing the residual solid plant material to expel the enriched extractant therefrom; admixing the plant juice and extractant to obtain a mixed juice, settling and clarifying said mixed juice; acidulating the liquid phase of the process at a preselected moment in the sequence, such that the settled and clarified juice will be brought to a pH of from about 3 to about 4; allowing said acidulated liquid phase to stand for a period of time of from about 2 to 3 hours at a temperature of from about 85.degree. C. to the boiling point; neutralizing the acidulated juice, clarifying the filtered and neutralized juice, heating the clarified and filtered juice, concentrating the heated juice by evaporation; pasteurizing the concentrated juice whereby to obtain a fructose-rich syrup; and crystallizing said fructose-rich syrup to recover crystallized fructose therefrom.
    • 从干旱植物,特别是阿马里亚科,例如龙舌兰植物获得果糖和果糖丰富的糖浆的方法包括分别收集由植物叶片部分和核心部分组成的植物材料; 用水混合洗涤说植物材料; 切碎洗涤后的植物材料,形成小块,回收剁碎操作释放的果汁; 用表面残留的固体植物材料的含水液体对切碎的材料进行萃取处理,以从其中排出富集的萃取剂; 混合植物汁和提取剂以获得混合果汁,沉淀和澄清所述混合汁; 在序列中的预选时刻酸化过程的液相,使得沉降和澄清的果汁的pH值达到约3至约4; 使所述酸化液相在约85℃至沸点的温度下静置约2至3小时; 中和酸化果汁,澄清过滤和中和的汁液,加热澄清和过滤的果汁,通过蒸发浓缩加热的果汁; 将浓缩的汁进行巴氏杀菌,从而得到富含果糖的糖浆; 并结晶所述富含果糖的糖浆以从其中回收结晶的果糖。
    • 3. 发明授权
    • Process for decolorization of solutions
    • 溶液脱色方法
    • US5932016A
    • 1999-08-03
    • US836581
    • 1997-07-17
    • Hannu A. PaananenTong Wen
    • Hannu A. PaananenTong Wen
    • C13B20/00C13D3/02B01D21/01
    • C13B20/005
    • The invention relates to a process for decolorization of solutions of sugars, sugar alcohols and betaine. In accordance with the process, a polyaluminium chloride is added to a solution of sugar, sugar alcohol or betaine having a dry substance content of 10 to 70% by weight and a temperature of 60 to 105.degree. C. in a suitable amount so as to obtain a mixture having a pH of 5.5 to 9.5, thereby precipitating the coloured substances, and the formed precipitate is separated from the solution. The invention also relates to the use of a polyaluminium chloride for decolorization of solutions of sugars, sugar alcohols and betaine.
    • PCT No.PCT / FI95 / 00629 Sec。 371日期1997年7月17日 102(e)日期1997年7月17日PCT 1994年11月14日PCT PCT。 WO96 / 15274 PCT出版物 日期1996年5月23日本发明涉及糖,糖醇和甜菜碱溶液的脱色方法。 根据该方法,将聚氯化铝加入到干物质含量为10至70重量%且温度为60至105℃的糖,糖醇或甜菜碱溶液中,其温度为适宜的量,以便 得到pH5.5〜9.5的混合物,使有色物质沉淀,将形成的沉淀物与溶液分离。 本发明还涉及聚氯化铝用于糖,糖醇和甜菜碱的溶液的脱色的用途。
    • 4. 发明授权
    • Process for the purification of sugar syrups
    • 糖浆的净化方法
    • US4478645A
    • 1984-10-23
    • US470118
    • 1983-04-21
    • Geir V. Gudnason
    • Geir V. Gudnason
    • C13B20/00C13B20/02C13B20/12C13D3/00C13D3/02
    • C13B20/02C13B20/005C13B20/123
    • A process for removing color, turbidity, flavor, and odor from impure, high Brix, sugar syrup involves entrapping the sugar impurities in an insoluble, primary calcium phosphate or aluminum hydroxide floc at about neutral pH, dividing the sugar syrup into a small portion and a large portion, aerating the small portion of the syrup at a specific Brix, recombining the small portion and the large portion, adding a polyelectrolyte to convert the primary floc into a secondary floc to which the air bubbles easily adhere and to cause flotation of said secondary floc, thus forming a scum mat at the top of the vessel. The purified sugar syrup is then filtered with or without activated carbon and small amounts of a filter aid to produce a sugar syrup with substantially reduced color, turbidity, flavor, and odor. The sugar in the scum is recovered by mixing it with water and allowing a second flotation to take place without any further aeration or chemicals addition.
    • 一种从不纯的白利糖度糖浆中除去颜色,浊度,风味和气味的方法包括将糖杂质包裹在约中性pH下的不溶性原始磷酸钙或氢氧化铝絮状物中,将糖浆分成小部分, 大部分,以特定的白利糖度使小部分糖浆充气,使小部分和大部分重新组合,加入聚电解质将初级絮凝物转化成二次絮凝物,气泡容易粘附到第二絮凝物,并引起所述 次级絮凝物,从而在容器的顶部形成浮渣垫。 然后将纯化的糖浆用或不用活性炭和少量助滤剂过滤以产生具有显着降低的颜色,浊度,风味和气味的糖浆。 通过将其与水混合并回收浮渣中的糖,并允许进行第二次浮选而不进行任何进一步的曝气或化学品添加。
    • 5. 发明授权
    • Clarification and treatment of sugar juice
    • 澄清和处理糖汁
    • US3994743A
    • 1976-11-30
    • US417269
    • 1973-11-19
    • Lewis A. Paley
    • Lewis A. Paley
    • C13B20/02C13B20/12C13D1/00C13D3/02C13D3/12C13D3/16
    • C13B20/123C13B20/02
    • Method and apparatus for treating fresh, unheated sugar cane juice which involves adding a sufficient amount of an aqueous alkaline slurry containing powdered active carbon to the juice to raise the pH of the juice to 6.8-8.5. The resulting mud is separated and a water white juice is obtained. The water white juice is concentrated to form a direct white sugar and an edible molasses having a natural maple flavor and odor. The juice may be subjected to a preliminary cyclone separation and the sugar cane from which the juice is obtained may be subjected to a steam-cleaning operation to remove cane wax and dirt.
    • 用于处理新鲜未加热的甘蔗汁的方法和装置,其包括向汁液中加入足量的含有粉末状活性炭的碱性水性浆料,以将果汁的pH提高至6.8-8.5。 分离得到的泥浆,得到水白汁。 水白汁浓缩形成直接白糖和具有天然枫叶风味和气味的可食用糖蜜。 可以对果汁进行初步旋风分离,并且可以从其获得果汁的甘蔗进行蒸汽清洁操作以除去拐杖蜡和污垢。
    • 6. 发明授权
    • Process and apparatus for treatment of cane sugar juice
    • 甘蔗糖汁处理工艺及设备
    • US3963513A
    • 1976-06-15
    • US516341
    • 1974-10-21
    • John A. Casey
    • John A. Casey
    • C13B20/02C13D3/02B01F5/00
    • C13B20/02Y10S159/13
    • Method and apparatus for controlled growth of precipitates in systems requiring separation of undesirable contaminants from a solution prior to treatment with a coagulant aid. Cane sugar juice, as exemplary, is introduced at an elevated temperature into an apparatus having means for maintaining a mildly reduced pressure. The apparatus has a conical funnel with a downwardly extending tubular outlet. Means are provided for incrementally and continuously introducing a chemical treating agent into the juice, as it flows down the funnel toward the outlet. Juice discharge means allows for control of the retention time in the tower. The method of treating cane sugar juice is as follows. Cane sugar juice, preferably partially limed, is introduced into the top of the funnel at an elevated temperature and allowed to flow by gravity flow through the funnel, while additional milk of lime is incrementally and continuously introduced into the cane sugar. The cane sugar juice flows downwardly through an outlet and then upwardly to allow for controlled formation of insoluble precipitate particles.
    • 在用凝结剂助剂处理之前,需要在不需要的污染物与溶液分离的系统中控制沉淀物生长的方法和装置。 蔗糖作为示例,在升高的温度下被引入到具有维持轻微降低压力的装置的装置中。 该装置具有锥形漏斗和向下延伸的管状出口。 提供了用于逐渐地和连续地将化学处理剂引入果汁中的装置,因为它向漏斗向着出口流下。 果汁排放装置允许控制塔中的保留时间。 甘蔗糖汁的处理方法如下。 将蔗糖优选地部分地加入到漏斗的顶部并在高温下通过重力流动通过漏斗流动,而另外的石灰奶被递增并连续地引入蔗糖中。 甘蔗糖汁向下流过出口,然后向上流动以允许控制形成不溶性沉淀颗粒。
    • 7. 发明授权
    • Process for making L-sugars and D-fructose
    • 制备L-糖和D-果糖的方法
    • US4421568A
    • 1983-12-20
    • US296403
    • 1981-08-26
    • Derk T. A. Huibers
    • Derk T. A. Huibers
    • C07H3/02C12P19/02C13K11/00C13D3/02C13K13/00
    • C07H3/02C12P19/02C13K11/00Y10S435/823
    • A method for producing L-sugars including L-idose and L-gulose as well as D-fructose from D-glucose. The method comprises epimerizing D-glucose to a mixture of D-glucose and D-mannose, hydrogenating the mixture in a fixed catalyst bed to provide D-sorbitol and D-mannitol, separating the D-mannitol by fractional crystallization, oxydizing separately the D-sorbitol and D-mannitol to provide L-sorbose and D-fructose, respectively; and racemizing the L-sorbose in a weak alkaline solution to provide a mixture of L-sorbose, L-idose and L-gulose, and precipitating the remaining L-sorbose with a dilute lime solution. The unconverted L-sorbose is recovered and recycled.
    • 一种D-葡萄糖的L-果糖和D-果糖的L-糖的生产方法。 该方法包括将D-葡萄糖对D-葡萄糖和D-甘露糖的混合物进行差向异构化,在固定的催化剂床中氢化混合物,得到D-山梨糖醇和D-甘露糖醇,通过分级结晶分离D-甘露糖醇,分别进行氧化 - 山梨糖醇和D-果糖分别提供L-山梨糖和D-果糖; 并将L-山梨糖在弱碱性溶液中外消旋化以提供L-山梨糖,L-阿糖和L-古洛糖的混合物,并用稀的石灰溶液沉淀剩余的L-山梨糖。 未转化的L-山梨糖被回收和再循环。