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    • 1. 发明授权
    • Amorphous precipitated siliceous pigments and methods for their
production
    • 无定形沉淀硅质颜料及其制备方法
    • US4144321A
    • 1979-03-13
    • US653720
    • 1976-01-30
    • Satish K. Wason
    • Satish K. Wason
    • A61K8/22A61K8/25A61Q11/00C09C1/30A61K7/16C08H17/04
    • C09C1/3045A61K8/25A61Q11/00A61K2800/262C01P2002/02C01P2004/50C01P2006/10C01P2006/11C01P2006/12C01P2006/19C01P2006/60C01P2006/80C01P2006/82C01P2006/90
    • A new method for producing precipitated silicas having a unique combination of physical and chemical properties is disclosed. The silicas are produced by acidulating a solution of an alkali metal silicate having a specific SiO.sub.2 /Na.sub.2 O mol ratio with an acid until precipitation just beings. At this point, the reaction mass is aged for a period of time and thereafter the acid addition is continued until the precipitated product is obtained. Products produced in accordance with the invention exhibit lower wet cake moisture and are characterized by their low structure, low oil absorption, high abrasiveness and high pack density, and as such are distinctly different from silicas used as reinforcing fillers in rubber. In a particularly advantageous embodiment, an adduct material, such as aluminum, is added to control the refractive index of the precipitated pigment. Products produced in this manner have particular utility for use as abrasion and gelling agents in clear toothpaste compositions.
    • 公开了一种具有物理和化学性质独特组合的沉淀二氧化硅的新方法。 二氧化硅通过酸化具有特定SiO 2 / Na 2 O摩尔比的碱金属硅酸盐与酸的溶液直到沉淀出来而制备。 此时,将反应物料老化一段时间,然后继续进行酸加成直至获得沉淀的产物。 根据本发明生产的产品显示较低的湿饼水分,其特征在于其低结构,低油吸收性,高磨损性和高包装密度,因此与用作橡胶中的增强填料的二氧化硅明显不同。 在特别有利的实施方案中,加入诸如铝的加合物材料以控制沉淀的颜料的折射率。 以这种方式生产的产品具有在清洁牙膏组合物中用作磨损和胶凝剂的特殊用途。
    • 9. 发明授权
    • Process for the hydrophobization of higher dispersed oxides
    • 高分散氧化物的疏水化方法
    • US3873337A
    • 1975-03-25
    • US38642973
    • 1973-08-07
    • DEGUSSA
    • LAUFER SIEGMARROY WALDEMAR
    • C01B13/14C01F7/02C09C1/30C09C3/00C09K3/18C08H17/04
    • C09C1/309C01B13/145C01P2004/84C09C3/006C09C3/043C09C3/12
    • Highly dispersed oxides of metals and/or silicon are hydrophobized by treatment with volatilizable organosilicon compounds in the gas phase. The oxide particles either come fresh from the production plant or are previously absolutely dried, and activated i.e., freed of physically and chemically bound water, in a fluidized bed with a dry inert gas stream at a temperature of 550* to 1000*C., preferably 600* to 950*C. under normal pressure in a few seconds to a few minutes, preferably in a time of 1 to 60 seconds. The oxide particles are reacted with a stoichiometrical mixture of at least one dialkyldichlorosilane and water in the ratio of 1:1 at a temperature of 350*C. to 650*C. in an atmosphere of CO2. There can also be used diaryldichlorosilanes.
    • 金属和/或硅的高度分散的氧化物通过在气相中用可挥发的有机硅化合物处理来疏水化。 氧化物颗粒从生产设备中新鲜出来,或者在550℃至1000℃的温度下,在干燥的惰性气流中在流化床中预先绝对干燥并活化,即,物理和化学结合的水, 优选600-950℃,常压下几秒至几分钟,优选在1至60秒的时间内。 氧化物颗粒在CO 2气氛中,在350℃至650℃的温度下,以1:1的比例与至少一种二烷基二氯硅烷和水的化学计量混合物反应。 也可以使用二芳基二氯硅烷。