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    • 1. 发明授权
    • Preparation of translucent strontium barium niobate ceramics using reaction sintering
    • 使用反应烧结制备半透明锶钡铌酸钡陶瓷
    • US06403053B1
    • 2002-06-11
    • US09183901
    • 1998-10-30
    • Tsang-Tse FangWen-Jiung Lee
    • Tsang-Tse FangWen-Jiung Lee
    • C01B1314
    • C04B35/495
    • In this patent, reaction sintering was used to prepare translucent strontium barium niobate ceramics (SrxBa1-xNb2O6, x=0.2-0.7). High purity powders of strontium carbonate (SrCO3) and barium carbonate (BaCO3) were mixed with niobium oxide (Nb2O5), respectively, at the same mole using ball milling. The mixed powders were dried and ground by a mortar. Thereafter, they were calcined at 800-1050° C. for 1-4 h in air to form strontium niobate (SrNb2O6) and Barium niobate (BaNb2O6), respectively. Precursor powders of strontium niobate (SrNb2O6) and barium niobate (BaNb2O6) were mixed in appropriate ratios and pressed. Compacts were reaction-sintered in a temperature range of 1300 to 1320° C. in O2 and then heat-treated in a temperature range of 1260 to 1275° C. in O2. We also propose the related basic principles and microstructures.
    • 在该专利中,使用反应烧结制备半透明铌酸钡铌酸钡陶瓷(SrxBa1-xNb2O6,x = 0.2-0.7)。 将锶碳酸锶(SrCO 3)和碳酸钡(BaCO 3)的高纯度粉末分别用铌氧化物(Nb 2 O 5)与球磨相同的摩尔混合。 将混合的粉末干燥并用研钵研磨。 然后,将它们在空气中在800-1050℃下煅烧1-4小时,分别形成铌酸锶(SrNb 2 O 6)和铌酸钡(BaNb 2 O 6)。 将铌酸锶(SrNb2O6)和铌酸钡(BaNb2O6)的前体粉末以适当的比例混合并压制。 压块在氧气中在1300至1320℃的温度范围内进行反应烧结,然后在O2中在1260至1275℃的温度范围内进行热处理。 我们还提出了相关的基本原理和微观结构。
    • 4. 发明授权
    • Process for the extraction and regeneration of acids from spent acids
    • 从废酸中萃取和再生酸的方法
    • US06214310B1
    • 2001-04-10
    • US09129212
    • 1998-08-05
    • Albert Lebl
    • Albert Lebl
    • C01B1314
    • C23G1/36B01J8/003B01J8/087B01J8/10C01B7/035C01B13/18C01B13/34Y10S423/01Y10S423/02
    • Process and apparatus for regenerating spent acid liquor includes a primary roasting furnace for evaporating a substantial portion of the liquid from the spent acid to produce acid vapors and partially roasted metal salts. The partially roasted metal salts are transferred to a secondary roasting chamber where the acids adhering to the surface of the metal salts is vaporized and the metal salts are oxidized. The acid vapors from the primary roasting furnace are then transferred to an absorption column to regenerate the acid. The primary roasting furnace is operated at a different temperature from the secondary roasting chamber and has different retention times for the metal salts. The secondary roasting chamber includes a raking device to mix and convey the metal salts during the secondary roasting step to produce a uniformly roasted metal oxide.
    • 用于再生废酸液的方法和设备包括用于从废酸蒸发大部分液体以产生酸蒸气和部分焙烧的金属盐的初级焙烧炉。 将部分焙烧的金属盐转移到二次焙烧室中,其中附着在金属盐表面的酸被蒸发并且金属盐被氧化。 然后将来自初级焙烧炉的酸蒸汽转移到吸收塔中以再生酸。 初级焙烧炉在与二次焙烧室不同的温度下运行,并且对于金属盐具有不同的保留时间。 二次焙烧室包括在二次焙烧步骤期间混合和输送金属盐的耙装置以产生均匀焙烧的金属氧化物。