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1. 发明授权

US06652829B2 Continuous calcination of mixed metal oxides 有权
公开(公告)号：US06652829B2
公开(公告)日：2003-11-25
申请号：US09928972
申请日：2001-08-13
申请人： Raymond E. Barnes , Richard A. Pipoly , Ivan H. Joyce , Javier Garcia Sainz
发明人： Raymond E. Barnes , Richard A. Pipoly , Ivan H. Joyce , Javier Garcia Sainz
IPC分类号： C01B1314
CPC分类号： F27B7/42 , C01B13/14 , C01G1/02 , C01G25/02 , C01G37/006 , C01P2006/60
摘要： A method for continuously calcinating product to form mixed metal oxide powders comprising providing a continuously operated indirectly heated rotary furnace having a heating cavity, introducing raw feedstock including product to be calcined into the heating cavity of the furnace while the heating cavity is maintained at temperature, and maintaining a controlled atmosphere in the heating cavity during the heating of the feedstock, and discharging and recovering the mixed metal oxide powders.

2. 发明授权

US06616744B1 Method of forming inorganic pigments 失效
标题翻译：无机颜料的形成方法
公开(公告)号：US06616744B1
公开(公告)日：2003-09-09
申请号：US10124740
申请日：2002-04-17
申请人： Javier Garcia Sainz , Rosario Blanch Castello , Rafael Mena Pla , Juan Carlos Gallart
发明人： Javier Garcia Sainz , Rosario Blanch Castello , Rafael Mena Pla , Juan Carlos Gallart
IPC分类号： C09C162
CPC分类号： C09C1/0009 , C01P2004/61 , C09C1/62
摘要： The present invention provides a method of forming inorganic pigments using one or more metal alloys. Metal alloys used in the method of the invention are preferably milled to a mean particle size of less than about 10 microns, may be mixed with other metal oxides, and calcined in the presence of oxygen in a rotary kiln. Inorganic pigments formed in accordance with the method of the invention can be used in a wide variety of applications, including the coloration of glass matrixes, ceramic bodies, polymers, and paints.
摘要翻译：本发明提供使用一种或多种金属合金形成无机颜料的方法。在本发明方法中使用的金属合金优选被研磨成小于约10微米的平均粒度，可与其它金属氧化物混合，并在氧气存在下在回转窑中煅烧。根据本发明方法形成的无机颜料可用于各种应用，包括玻璃基体，陶瓷体，聚合物和涂料的着色。

3. 发明授权

US06402823B1 Individual inks and an ink set for use in the color ink jet printing of glazed ceramic tiles and surfaces 有权
标题翻译：单独的油墨和用于彩色喷墨印刷釉面瓷砖和表面的油墨组
公开(公告)号：US06402823B1
公开(公告)日：2002-06-11
申请号：US09479350
申请日：2000-01-07
申请人： Javier Garcia Sainz , Carlos Benet Garcia , Jose Luis Fenollosa Romero , Antonio Manuel Querol Villalba , Patricia C. Secrest
发明人： Javier Garcia Sainz , Carlos Benet Garcia , Jose Luis Fenollosa Romero , Antonio Manuel Querol Villalba , Patricia C. Secrest
IPC分类号： C09D1100
CPC分类号： C09D11/40 , C04B41/009 , C04B41/52 , C04B41/89 , C04B2111/82 , C04B41/4578 , C04B41/5022 , C04B41/5041 , C04B41/4535 , C04B41/4554 , C04B41/4558 , C04B41/4572 , C04B2103/0013 , C04B2103/0014 , C04B41/522 , C04B2103/0022 , C04B2103/0018 , C04B2103/0019 , C04B2103/0021 , C04B2103/0015 , C04B2103/0017 , C04B33/00
摘要： Individual inks and an ink set for use in generating intermediate colors via the combination of separate inks applied by an ink jet printer to the glazed surface of an article, such as glazed ceramic architectural tile for example, that is to be heated to a temperature of greater than 300° C. The ink set according to the present invention includes at least three separate inks that upon heating decompose to form colored oxides or colored combinations with the materials of the glazed surface upon which they are applied. A first ink of the ink set includes a soluble cobalt complex for use in forming a cyan color. A second ink of the ink set includes a soluble gold complex for use in forming a magenta color. And, a third ink of the ink set includes a soluble transition metal complex for use in forming a yellow color. The third ink preferably includes a soluble praseodymium complex. Alternatively, the third ink includes a blend of soluble chromium and antimony complexes and/or soluble nickel and antimony complexes. The ink set also preferably includes a fourth ink including a soluble ruthenium complex for use in forming a black color. The inks preferably contain no suspended solids and are preferably water immiscible. The invention also provides a method of decorating a glazed article using the inks of the ink set, and an article having a decoration applied to at least one glazed surface thereof.
摘要翻译：单独的油墨和用于通过由喷墨打印机施加的单独油墨的组合产生中间颜色的油墨组件，例如被加热到制品的玻璃釉面，例如釉面陶瓷建筑砖，大于300℃。根据本发明的油墨组包括至少三种分开的油墨，其在加热时分解形成着色氧化物或着色组合与施加它们的玻璃表面的材料。墨水组的第一墨水包括用于形成青色的可溶性钴络合物。墨水组的第二墨水包括用于形成洋红色的可溶性金络合物。并且，墨水组的第三墨水包括用于形成黄色的可溶性过渡金属络合物。第三油墨优选包含可溶性镨络合物。或者，第三油墨包括可溶性铬和锑络合物和/或可溶性镍和锑络合物的共混物。油墨组还优选包括第四种油墨，其包括用于形成黑色的可溶性钌络合物。油墨优选不含悬浮固体，优选为水不混溶。本发明还提供了一种使用油墨组的油墨装饰釉面制品的方法，以及具有应用于其至少一个釉面的装饰物品。

4. 发明授权

US06565922B2 Method of decorating a ceramic substrate 失效
标题翻译：装饰陶瓷基板的方法
公开(公告)号：US06565922B2
公开(公告)日：2003-05-20
申请号：US10246291
申请日：2002-09-18
申请人： Carlos Benet Garcia , Javier Garcia Sainz , Juan Carlos Gallart
发明人： Carlos Benet Garcia , Javier Garcia Sainz , Juan Carlos Gallart
IPC分类号： B05D506
CPC分类号： C09D11/037
摘要： The present invention provides a method of decorating a ceramic substrate. The method according to the invention includes applying a slurry that includes solid particles of at least one color-contributing metal salt dispersed in a saturated solution of at least one color-contributing metal salt having a viscosity of from about 10 to about 20,000 centipoise to a ceramic substrate, applying a solvent to the ceramic substrate in amount sufficient to at least partially dissolve the solid particles, and firing the ceramic substrate. Preferably, the solid particles in the slurry have a diameter of less than about 40 microns. The present invention also provides a porcelain tile decorated in with the method.
摘要翻译：本发明提供一种装饰陶瓷基板的方法。根据本发明的方法包括将包含分散在至少一种粘度为约10至约20,000厘泊的至少一种着色金属盐的饱和溶液中的至少一种着色贡献金属盐的固体颗粒施加到陶瓷基板，以足以至少部分地溶解固体颗粒的量向陶瓷基板施加溶剂，以及烧制陶瓷基板。优选地，浆料中的固体颗粒具有小于约40微米的直径。本发明还提供了一种用该方法装饰的瓷砖。

5. 发明授权

US06464765B1 Saturated soluble salt slurries for coloring ceramics 失效
标题翻译：用于着色陶瓷的饱和可溶性盐浆
公开(公告)号：US06464765B1
公开(公告)日：2002-10-15
申请号：US09676252
申请日：2000-09-29
申请人： Carlos Benet Garcia , Javier Garcia Sainz
发明人： Carlos Benet Garcia , Javier Garcia Sainz
IPC分类号： C09D1100
CPC分类号： C09D11/037
摘要： The present invention provides a slurry for use in decorating a ceramic substrate. The slurry according to the invention includes solid particles of at least one color-contributing metal salt dispersed in a saturated solution of at least one color-contributing metal salt, and has a viscosity of from about 10 to about 20,000 centipoise. Preferably, the solid particles have a diameter of less than about 40 microns. The present invention also provides a method of decorating a surface of a ceramic substrate. The method according to the invention includes applying a slurry that includes solid particles of at least one color-contributing metal salt dispersed in a saturated solution of at least one color-contributing metal salt having a viscosity of from about 10 to about 20,000 centipoise to a ceramic substrate, applying a solvent to the ceramic substrate in amount sufficient to at least partially dissolve the solid particles, and firing the ceramic substrate.
摘要翻译：本发明提供一种用于装饰陶瓷基板的浆料。根据本发明的浆料包括分散在至少一种着色金属盐的饱和溶液中的至少一种着色贡献金属盐的固体颗粒，并且具有约10至约20,000厘泊的粘度。优选地，固体颗粒具有小于约40微米的直径。本发明还提供一种装饰陶瓷基板的表面的方法。根据本发明的方法包括将包含分散在至少一种粘度为约10至约20,000厘泊的至少一种着色金属盐的饱和溶液中的至少一种着色贡献金属盐的固体颗粒施加到陶瓷基板，以足以至少部分地溶解固体颗粒的量向陶瓷基板施加溶剂，以及烧制陶瓷基板。

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