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1. 发明授权

US06773554B1 Hazardous waste disposal 失效
标题翻译：危险废物处理
公开(公告)号：US06773554B1
公开(公告)日：2004-08-10
申请号：US09566469
申请日：2000-05-08
申请人： John W. Moore, Jr.
发明人： John W. Moore, Jr.
IPC分类号： B01D314
CPC分类号： B01D5/006
摘要： Contaminated glycol is refined by vacuum distillation. Specifically the evaporator is heated to a temperature below the degradation temperature of the glycol. The vacuum is used to bring the flashpoint down sufficiently so that glycol evaporates or flashes at that temperature. The glycol is condensed and filtered through activated granular carbon. The principal use of refining the glycol is to refine the triethylene glycol used in natural gas dehydration plants. For such purposes the equipment is mounted upon a trailer to be taken to the plant for cleaning glycol. In such instance, in addition to refining the glycol, a cleaning agent (which contains a degreaser) is added to the refined glycol. The glycol is refined while the natural gas dehydration plant is in normal operation and therefore it is not necessary to stop the natural gas dehydration plant for refining the glycol used therein. In addition, by the addition of the cleaning agent, the dehydrating plant equipment may be cleansed of hazardous waste. The hazardous waste will be separated and concentrated in the distillation. Therefore, the transportation of the hazardous waste to a disposal location is simplified.
摘要翻译：污染的二醇通过真空蒸馏精制。具体地说，将蒸发器加热到低于二醇降解温度的温度。使用真空使闪点足够下降，使得二醇在该温度下蒸发或闪蒸。将二醇冷凝并通过活性颗粒碳过滤。精炼二醇的主要用途是精炼天然气脱水设备中使用的三甘醇。为了这样的目的，将设备安装在拖车上以被带到工厂以清洁二醇。在这种情况下，除了精制二醇之外，将还原剂（其含有脱脂剂）加入到精制二醇中。在天然气脱水装置正常运行的同时，乙二醇精制，因此不需要停止天然气脱水装置来精制其中使用的二醇。此外，通过添加清洁剂，可以将脱水设备设备清洗成危险废物。危险废物将在蒸馏中分离和浓缩。因此，将危险废物运往处置场所简化。

2. 发明授权

US06569291B1 Liquid distributor for separation columns 失效
标题翻译：分离柱用液体分配器
公开(公告)号：US06569291B1
公开(公告)日：2003-05-27
申请号：US09287680
申请日：1999-04-06
申请人： Martin Knoche
发明人： Martin Knoche
IPC分类号： B01D314
CPC分类号： B01D3/008
摘要： The liquid distributor (2) for columns (1) comprises at least one tub shaped or tubular part (3) of a rigid material. Outflow elements (4) of yielding, in particular elastomeric material are tightly inserted into apertures (30) of the tub shaped or tubular part. A liquid (6) to be distributed can flow off in each case through at least one opening (40) in the outflow element. This opening has a precisely predeterminable geometry.
摘要翻译：用于塔（1）的液体分配器（2）包括至少一个刚性材料的桶状或管状部分（3）。屈服的流出元件（4）特别是弹性体材料被紧密地插入到桶状或管状部分的孔（30）中。待分配的液体（6）可以在每种情况下通过流出元件中的至少一个开口（40）流出。该开口具有精确可预先确定的几何形状。

3. 发明授权

US06692616B2 Method for purifying trimethylolpropane, which is produced by hydrogenation, by means of continuous distillation 失效
标题翻译：通过连续蒸馏通过氢化制备三羟甲基丙烷的方法
公开(公告)号：US06692616B2
公开(公告)日：2004-02-17
申请号：US10168980
申请日：2002-06-26
申请人： Matthias Dernbach , Detlef Kratz , Achim Stammer , Harald Rust , Gerhard Schulz
发明人： Matthias Dernbach , Detlef Kratz , Achim Stammer , Harald Rust , Gerhard Schulz
IPC分类号： B01D314
CPC分类号： C07C29/80 , C07C31/225 , C07C31/12 , C07C31/245 , C07C31/04
摘要： A process is disclosed for the purification, by distillation, of trimethylolpropane originating from the hydrogenation of 2,2-dimethylolbutanal, said process including the following steps: (a) reaction of n-butyraldehyde with formaldehyde in the presence of catalytic amounts of a tertiary amine, and hydrogenation of the resulting mixture to give a mixture containing trimethylolpropane; (b) separation of water, methanol, trialkylamine and/or trialkylammonium formate by distillation; (c) heating of the residue obtained in (b) under reduced pressure to a temperature at which TMP is volatile and compounds boiling above TMP are cleaved, in order to separate off, by distillation, TMP and compounds more volatile than TMP; (d) distillation of the distillate obtained in (c) in order to separate off the more volatile compounds and recover pure TMP; and (e) optional distillation of the TMP obtained in (d) in order to recover TMP with a low APHA color index. A process is also disclosed in which trialkylammonium formate is distilled under mild conditions from crude mixtures of polyhydric alcohols, predominantly trimethylolpropane.
摘要翻译：公开了一种通过蒸馏纯化来自2,2-二羟甲基丁烷的氢化的三羟甲基丙烷的方法，所述方法包括以下步骤：（a）在催化量的叔碳酸存在下，正丁醛与甲醛的反应胺，并氢化得到的混合物，得到含有三羟甲基丙烷的混合物;（b）通过蒸馏分离水，甲醇，三烷基胺和/或三烷基铵甲酸盐;（c）将（b）中得到的残余物在减压下加热至 TMP挥发的温度和TMP沸点高的化合物被切割，以便通过蒸馏分离TMP和比TMP更易挥发的化合物;（d）蒸馏（c）中获得的馏出物，以分离出更多的挥发性化合物，回收纯TMP; 为了回收具有低APHA颜色指数的TMP，还可以任选地蒸馏（d）中获得的TMP。还公开了一种方法，其中在温和条件下从多元醇，主要是三羟甲基丙烷的粗混合物中蒸馏出三烷基铵甲酸盐。

4. 发明授权

US06485613B1 Batch-continuous countercurrent mass transfer process 失效
标题翻译：批量连续逆流传质过程
公开(公告)号：US06485613B1
公开(公告)日：2002-11-26
申请号：US09530692
申请日：2000-05-04
申请人： Josephus Johannes Petrus Maria Goorden
发明人： Josephus Johannes Petrus Maria Goorden
IPC分类号： B01D314
CPC分类号： B01D53/18 , B01D3/02 , B01D3/14 , B01D3/146 , B01D11/0219 , B01D11/0284 , B01D11/043 , B01D11/0457 , B01D11/0488 , B01D47/12 , Y10S203/11 , Y10S203/13 , Y10S203/17
摘要： Mass transfer process, in which, in at least two contact stages, and at least two liquid or gaseous phases are brought into contact with one another, at least one component being transferred between the phases and the phases moving countercurrently. The flow through at least one of the contact stages is batchwise for one phase and continuous for another phase. The phases flow through contact stages which are formed by trays in a column, which trays are opened periodically so that the phase which flows through the column in a batchwise manner flows to the next tray.
摘要翻译：在至少两个接触阶段和至少两个液相或气相彼此接触的质量传递过程中，在相和相之间转移的至少一个组分逆流运动。通过至少一个接触级的流是间歇式的，用于一相，另一相连续流。这些相通过由塔中的塔板形成的接触阶段，其中塔板周期性地打开，使得以间歇方式流过塔的相流动流到下一个塔盘。

5. 发明授权

US06419796B1 Solvent distillation apparatus 失效
标题翻译：溶剂蒸馏装置
公开(公告)号：US06419796B1
公开(公告)日：2002-07-16
申请号：US09805037
申请日：2001-03-14
申请人： Masato Kitamura , Ryoji Noyori , Toshiaki Noda
发明人： Masato Kitamura , Ryoji Noyori , Toshiaki Noda
IPC分类号： B01D314
CPC分类号： B01D3/14 , B01D3/42 , B01D3/4205 , B01D5/0063 , Y10S203/02
摘要： The object of the invention is to provide a solvent distillation apparatus capable of preparing a highly pure anoxic, dehydrated solvent. A distilling flask is connected to a vacuum double-barrel fractionating column by a glass flange. The upper end of the fractionating column is connected to a middle portion of a reflux condenser. The upper end of the reflux condenser is provided with an outlet for a purge gas, and the lower end thereof is connected to a condensate reservoir. The base of the condensate reservoir is connected to the fractionating column near a lower end thereof via a Young cock, and also connected to a collecting flask via a Young cock and a glass flange. An immersion tube is used to blow an inactive gas into a base portion of the condensate reservoir. The fractionating column, the reflux condenser and the condensate reservoir are integrated as one body.
摘要翻译：本发明的目的是提供能够制备高纯度的缺氧脱水溶剂的溶剂蒸馏装置。蒸馏瓶通过玻璃法兰连接到真空双筒分馏塔。分馏塔的上端与回流冷凝器的中间部分连接。回流冷凝器的上端设置有用于吹扫气体的出口，其下端连接到冷凝物储存器。冷凝水槽的底部经由Young旋塞连接到靠近其下端的分馏塔，并且还通过Young旋塞和玻璃凸缘连接到收集烧瓶。浸入管用于将惰性气体吹入冷凝物储存器的基底部分。分馏塔，回流冷凝器和冷凝水储存器整合为一体。

6. 发明授权

US06821394B2 Process of extracting from haw-pit by dry distillation and its device 失效
标题翻译：通过干馏从鹰嘴提取的方法及其装置
公开(公告)号：US06821394B2
公开(公告)日：2004-11-23
申请号：US10311461
申请日：2003-04-21
申请人： Yi Shi
发明人： Yi Shi
IPC分类号： B01D314
CPC分类号： B01D3/40 , A01N65/34 , A61K36/734 , Y02E50/14 , Y10S203/13 , Y10S203/16
摘要： The present invention relates to a process of extracting haw pits by dry distillation and the device used therein. The process includes the following steps: removing the impurities of haw pits and drying them; immersing haw pits in water and then dripping and charging the dried pit into the furnace for dry distillation; gradually raising the temperature and dry distilling the haw pits at two temperature ranges of 105-195° C. and 305-380° C. respectively and collecting the distillate; mixing together the distillate, allowing them to separate into layers by specific gravity difference and separating out the final brownish red transparent liquor by siphon. The method of the present invention can provide high yield of extraction and the present device is simple in structure. Further, the present invention is easy to be employed on the industrial scale.
摘要翻译：本发明涉及通过干馏提取洼坑的方法及其中使用的装置。该过程包括以下步骤：去除洼坑杂质并将其干燥; 将洼坑浸入水中，然后将干燥的坑浸入炉中进行干馏; 逐渐升高温度，并在105-195℃和305-380℃的两个温度范围内分别干燥窖穴并收集馏出物; 将馏出物混合在一起，使它们通过比重差异分离成层，并通过虹吸分离出最终的棕红色透明液体。本发明的方法可以提供高产率的提取，本装置的结构简单。此外，本发明容易在工业规模上应用。

7. 发明授权

US06780289B2 Process for the purification and recovery of acetonitrile 有权
标题翻译：纯化和回收乙腈的方法
公开(公告)号：US06780289B2
公开(公告)日：2004-08-24
申请号：US09906299
申请日：2001-07-16
申请人： Sanjay P. Godbole
发明人： Sanjay P. Godbole
IPC分类号： B01D314
CPC分类号： C07C253/26 , C07C253/24 , C07C253/34 , Y10S203/20 , C07C255/03
摘要： A method for the purification of crude acetonitrile comprising distilling the crude acetonitrile in a first fractional distillation column at below atmospheric pressure, withdrawing a first side draw fraction comprising acetonitrile, distilling the first side draw fraction in a second fractional distillation column at super atmospheric pressure, and withdrawing from the second distillation a second side draw fraction comprising purified acetonitrile.
摘要翻译：一种用于纯化粗乙腈的方法，包括在低于大气压的第一分馏塔中蒸馏粗乙腈，取出包含乙腈的第一侧馏分，在第二分馏塔中在超大气压下蒸馏第一侧馏分，并从第二次蒸馏中取出包含纯化乙腈的第二侧馏分。

8. 发明授权

US06770173B1 Column partition 有权
标题翻译：列分区
公开(公告)号：US06770173B1
公开(公告)日：2004-08-03
申请号：US09672252
申请日：2000-09-28
申请人： Helmut Jansen , Jochen Leben , Thomas Rietfort , Egon Zich
发明人： Helmut Jansen , Jochen Leben , Thomas Rietfort , Egon Zich
IPC分类号： B01D314
CPC分类号： B01D3/141 , B01D3/32
摘要： Partitions for columns for the separation of components or chemical reactions are assembled from plates or wall elements provided with plug and clamp connectors along respective edges and formed by strips so that the partitions can be easily and safely assembled and disassembled.
摘要翻译：用于分离组分或化学反应的柱的分隔体由沿着相应边缘提供有插塞和夹持连接器的板或壁元件组装，并由条形成，使得隔板可以容易且安全地组装和拆卸。

9. 发明授权

US06551465B1 Dividing wall column control system 有权
标题翻译：分隔墙柱控制系统
公开(公告)号：US06551465B1
公开(公告)日：2003-04-22
申请号：US09840224
申请日：2001-04-23
申请人： Charles P. Van Zile , James W. Harris
发明人： Charles P. Van Zile , James W. Harris
IPC分类号： B01D314
CPC分类号： B01D3/141 , B01D3/14 , B01D3/4238 , Y10S203/09 , Y10S203/19 , Y10S203/20
摘要： The operation of the dividing wall section of a dividing wall column is controlled by a control apparatus comprising a ratio controller which divides the liquid flowing into the dividing wall section. The rate of return of overhead liquid to the column is set by monitoring the temperature in the top of the product dividing wall section and the sidecut product draw rate is set by monitoring a temperature in the bottom of the product dividing wall section.
摘要翻译：分隔壁柱的分隔壁部分的操作由包括比例控制器的控制装置控制，该比率控制器将流入分隔壁部分的液体分开。通过监测产品分隔壁部分的顶部的温度来设定塔顶液体向塔的返回率，通过监视产品分隔壁部分的底部的温度来设定副产品的拉伸速度。

10. 发明授权

US06500310B1 Process for the treatment of waste water 失效
标题翻译：废水处理流程
公开(公告)号：US06500310B1
公开(公告)日：2002-12-31
申请号：US09719624
申请日：2000-12-14
申请人： Robert Frank Dee , Marinus Van Zwienen
发明人： Robert Frank Dee , Marinus Van Zwienen
IPC分类号： B01D314
CPC分类号： C02F1/048 , B01D3/146
摘要： A process for treating waste water streams containing at least hydrocarbons and salts to yield a clean water product, a concentrated brine product and a hydrocarbon-rich product, which process includes the steps of: (a) feeding the waste water feed into a first distillation column at a stage in the range of from 0.05 to 0.15 from the top, wherein n represents the total number of theoretical stages of the first distillation column and has a value in the range of from 20 to 40; (b) drawing off a vapor stream at a stage in the range of from 0.55 to 0.75 from the top and feeding this vapor stream into the bottom of a second distillation column having m theoretical stages, with m having a value in the range of from 3 to 10; (c) drawing off the clean water product as the top fraction from the second distillation column and drawing off a bottom stream from the second distillation column, which is fed back into the first distillation column below the draw off of the vapor stream in step (b) at a stage in the range of from 0.60 to 0.85 from the top; (d) drawing off the concentrated brine product as the bottom fraction of the first distillation column; and (e) drawing off the hydrocarbon stream as the top fraction of the first distillation column.
摘要翻译：一种用于处理含有至少烃和盐的废水流以产生清洁水产品，浓缩的盐水产物和富含烃的产品的方法，该方法包括以下步骤：（a）将废水进料送入第一蒸馏塔的顶部从0.05至0.15的范围内，其中n表示第一蒸馏塔的理论级总数，其值在20至40的范围内; （b）从顶部抽出0.55至0.75范围内的蒸气流，并将该蒸汽流送入具有理论级的第二蒸馏塔的底部，其中m的值范围为 3至10; （c）从第二蒸馏塔抽出清洁水产品作为顶级馏分，并从第二蒸馏塔中抽出底部物流，该第二蒸馏塔在第一蒸馏塔中被反馈到低于蒸气流的蒸馏流的步骤 b）在从顶部的0.60至0.85范围内的阶段; （d）抽出浓缩的盐水产物作为第一蒸馏塔的塔底部分; 和（e）除去作为第一蒸馏塔顶馏分的烃流。

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