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1. 发明授权

US10052807B2 Fiber manufacturing method, non-woven fabric manufacturing method, and fiber manufacturing equipment 有权
公开(公告)号：US10052807B2
公开(公告)日：2018-08-21
申请号：US15231094
申请日：2016-08-08
申请人： FUJIFILM Corporation
发明人： Yukihiro Katai , Shigehisa Sugiyama , Seiji Kasahara , Yasuhisa Shimoda , Masahiro Esaki
IPC分类号： D01D5/06 , D01D5/11 , D01F2/28 , D01F13/02 , D04H1/4258 , D04H1/72 , D04H1/736 , D21H13/02 , B29C47/00 , B29B11/04 , B29K1/00 , B29L7/00
CPC分类号： B29C48/08 , B29B11/04 , B29C48/05 , B29K2001/12 , B29L2007/008 , D01D5/06 , D01F2/28 , D01F13/02 , D04H1/4258 , D04H1/72 , D04H1/736 , D21H13/02 , Y02P70/627
摘要： A fiber manufacturing method includes the following steps of: dissolving a polymer in a solvent to obtain a polymer solution; spraying the polymer solution into a liquid heated to a boiling point of the solvent or higher, and evaporating the solvent to precipitate a fibrous polymer in a sealed precipitation tank, the liquid being immiscible with the polymer and the solvent; conveying the precipitated fibrous polymer in a liquid from the precipitation tank; water-rinsing the fibrous polymer conveyed in the liquid in the conveying step in a sealed water-rinsing tank; conveying the water-rinsed fibrous polymer in a liquid from the water-rinsing tank; and cooling and condensing solvent gas that is generated in the spraying step and the water-rinsing step.

2. 发明授权

US09670596B2 Production method for purified polysaccharide fibers, purified polysaccharide fibers, fiber-rubber complex, and tire 有权
公开(公告)号：US09670596B2
公开(公告)日：2017-06-06
申请号：US14402154
申请日：2013-05-21
申请人： BRIDGESTONE CORPORATION
发明人： Mitsuharu Koide , Kenichi Sugimoto
IPC分类号： D01F2/02 , D01F9/00 , C08L1/02 , C08L21/00 , D02G3/48 , D01F2/00 , B60C9/00 , D01D5/06 , D01F13/02 , B60C1/00
CPC分类号： D01F2/02 , B60C1/0041 , B60C9/0042 , B60C2001/0066 , B60C2001/0083 , C08L1/02 , C08L21/00 , C08L2205/16 , D01D5/06 , D01F2/00 , D01F9/00 , D01F13/02 , D02G3/48 , D10B2201/00 , Y02P70/627
摘要： The present invention provides a production method for purified polysaccharide fibers in which carbon disulfide emission is suppressed while efficiently producing purified polysaccharide fibers having excellent strength, purified polysaccharide fibers produced by using the production method, a fiber-rubber complex using the purified polysaccharide fibers, and a tire having excellent tire characteristics using the fiber-rubber complex. The production method for purified polysaccharide fibers of the present invention is a production method for purified polysaccharide fibers of wet-spinning or dry-wet-spinning polysaccharide by bringing a polysaccharide solution obtained by dissolving a polysaccharide raw material in a liquid including an ionic liquid into contact with a solidification liquid including an ionic liquid, in which a concentration of the ionic liquid in the solidification liquid is 0.4% by weight to 50% by weight and the anionic moieties of the ionic liquid in the polysaccharide solution and the ionic liquid in the solidification liquid have one or more types selected from the group consisting of a phosphinate ion, a phosphate ion, and a phosphonate ion.

3. 发明申请

US20160168772A1 Spunbond method for producing non-woven fabric of natural cellulose with flame-retarding feature 有权
标题翻译：用于生产具有阻燃特性的天然纤维素无纺织物的纺粘方法
公开(公告)号：US20160168772A1
公开(公告)日：2016-06-16
申请号：US14663762
申请日：2015-03-20
申请人： Acelon Chemicals and Fiber Corporation
发明人： Wen-Tung CHOU , Ming-Yi LAI , Kun-Shan HUANG
IPC分类号： D04H1/498 , D04H1/70 , D01D1/02 , D04H1/46 , D01D5/14 , D01D10/06
CPC分类号： D04H3/013 , D01D5/0985 , D01F2/00 , D01F13/02 , D04H3/105 , D04H3/11 , D06M13/292 , D06M2101/06 , D06M2200/30 , Y02P70/627
摘要： A spunbond method for producing non-woven fabric of natural cellulose with flame-retarding feature comprises following steps. Blend pulp and solvent of N-methylmorpholine N-oxide (NMMO) to form slurry. Evaporate water content from slurry by a Thin Film Evaporator to form dope. Extrude the dope off spin nozzles to form filament strand via spunbond method. Coagulating regenerate, water rinse, hydro-entangled needle-punch and dry the filament strand to form normal natural cellulose nonwoven, which is soaking rolled by flame retardant of N-hydroxymethyl-3-(dimethoxy-phosphate acyl) propyl amide, then orderly bake, alkaline clean, water rinse, dry and wind-up to convert it into modified natural cellulose nonwoven fabrics of long-acting flame retarding feature in coil manner. Because of cross-linking reaction between foregoing flame retardant and natural cellulose nonwoven, the flame-retarding capability thereof meet requirements of testing standards in American ASTM D6413-1999 and ASTM D2863-1995. Moreover, the wastes thereof meet environmental protection requirements.
摘要翻译：用于生产具有阻燃特性的天然纤维素无纺织物的纺粘方法包括以下步骤。混合纸浆和N-甲基吗啉N-氧化物（NMMO）的溶剂形成浆料。通过薄膜蒸发器从浆液中蒸发水分，形成涂料。通过旋转喷嘴将纺丝液挤出，通过纺粘法形成丝束。凝结再生，水冲洗，水缠结针刺，并干燥长丝线以形成通过N-羟甲基-3-（二甲氧基 - 磷酸酯酰基）丙基酰胺的阻燃剂浸泡的普通天然纤维素非织造布，然后有序烘烤，碱性清洁，水冲洗，干燥和卷绕，将其转化为线圈式长效阻燃特性的改性天然纤维素无纺布。由于前述阻燃剂与天然纤维素非织造布之间的交联反应，其阻燃性能符合美国ASTM D6413-1999和ASTM D2863-1995中测试标准的要求。此外，其废物符合环保要求。

4. 发明授权

US08932471B2 Method of recovering and concentrating an aqueous N-methylmorpholine-N-oxide (NMMO) solution 有权
标题翻译：回收和浓缩N-甲基吗啉-N-氧化物（NMMO）水溶液的方法
公开(公告)号：US08932471B2
公开(公告)日：2015-01-13
申请号：US13228946
申请日：2011-09-09
申请人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang , Hsiao-Chi Tsai , Chih-Chung Kuo
发明人： Wen-Tung Chou , Ming-Yi Lai , Kun-Shan Huang , Hsiao-Chi Tsai , Chih-Chung Kuo
IPC分类号： B01D17/00 , B01D1/26 , D01F13/02
CPC分类号： B01D1/26 , D01F13/02 , Y02P70/627
摘要： This disclosure relates to a method of recovering and concentrating an aqueous N-methylmorpholine-N-oxide (NMMO) solution.
摘要翻译：本公开涉及一种回收和浓缩N-甲基吗啉-N-氧化物（NMMO）水溶液的方法。

5. 发明授权

US06416725B1 Removal of contaminants from gas streams in rayon production 失效
标题翻译：在人造丝生产中清除气流中的污染物
公开(公告)号：US06416725B1
公开(公告)日：2002-07-09
申请号：US09424118
申请日：2000-02-22
申请人： Edward F. Spink , Christopher R. Mueller
发明人： Edward F. Spink , Christopher R. Mueller
IPC分类号： B01D5348
CPC分类号： B01D53/52 , B01D53/48 , C01B17/22 , C01B32/72 , D01F13/02 , Y02P70/627
摘要： Sulfurous gas streams comprising hydrogen sulfide and carbon disulfide, such as produced as a by-product of the rayon-forming process, are processed to recover the components in a useable form. The gas stream first is contacted with an aqueous sodium hydroxide to dissolve out hydrogen sulfide and some of the carbon disulfide. The dissolved carbon disulfide is driven off from the solution and condensed as a liquid concentrate. Carbon disulfide remaining the gas stream is recovered, such as by condensation. The aqueous sodium sulfide solution which remains from removal of carbon disulfide is concentrated and the pH is adjusted, as necessary, to a value at which the sodium sulfide is predominantly in the form of sodium bisulfide. The concentrated sodium bisulfide solution is capable of reuse in the rayon-forming process along with the liquid concentrate of carbon disulfide.
摘要翻译：处理包含硫化氢和二硫化碳的亚硫酸气流，例如作为人造丝形成工艺的副产物而生产的，以可回收的形式回收组分。首先将气流与氢氧化钠水溶液接触以溶解硫化氢和一些二硫化碳。溶解的二硫化碳从溶液中排出并作为液体浓缩物浓缩。残留气流的二硫化碳例如通过冷凝回收。将从二硫化碳中除去的硫酸钠水溶液浓缩，根据需要将pH调节至硫化钠主要为二硫化
钠形式的值。浓缩的二硫化钠溶液能够与人造丝形成过程一起再次与二硫化碳的液体浓缩物一起使用。

6. 发明授权

US5904818A Process for the regeneration of an aqueous process liquid of the amine-oxide process 失效
标题翻译：用于再生氧化胺工艺的含水工艺液体的方法
公开(公告)号：US5904818A
公开(公告)日：1999-05-18
申请号：US843851
申请日：1997-04-17
申请人： Wolfram Kalt , Dieter Eichinger , Bruno Mangeng , Heinrich Firgo
发明人： Wolfram Kalt , Dieter Eichinger , Bruno Mangeng , Heinrich Firgo
IPC分类号： C07D295/24 , C07D295/28 , C08B1/00 , D01F2/00 , D01F13/02 , C07D3/00 , C07D265/30
CPC分类号： C07D295/24 , C07D295/28 , C08B1/003 , D01F13/02 , D01F2/00 , Y02P70/627
摘要： The invention is concerned with a process for the production of a solution of N-methylmorpholine-N-oxide in water, characterized by the following steps:(a) providing an aqueous solution containing N-methylmorpholine and morpholine and exhibiting a pH value of from 6.0 to 9.0, thereafter(b) treating said aqueous solution with a peroxidic oxidant to oxidize N-methylmorpholine to N-methylmorpholine-N-oxide.
摘要翻译：本发明涉及一种制备N-甲基吗啉-N-氧化物在水中的溶液的方法，其特征在于以下步骤：（a）提供含有N-甲基吗啉和吗啉的水溶液，其pH值为 6.0〜9.0，此后（b）用过氧化物氧化剂处理所述水溶液以将N-甲基吗啉氧化成N-甲基吗啉-N-氧化物。

7. 发明授权

US5441689A Process of making regenerated cellulose articles 失效
标题翻译：制备再生纤维素制品的方法
公开(公告)号：US5441689A
公开(公告)日：1995-08-15
申请号：US240696
申请日：1994-05-09
申请人： Peter R. Laity
发明人： Peter R. Laity
IPC分类号： D01F2/02 , B01J41/04 , B01J49/00 , D01F2/00 , D01F13/02 , B01D15/04
CPC分类号： D01F13/02 , B01J41/043 , B01J49/0013 , D01F2/00 , Y02P70/627
摘要： Aqueous solutions of an amine N-oxide such as N-methyl morpholine N-oxide used in the manufacture of regenerated cellulose can be purified by passage through a strongly basic anion-exchange resin. The resin is regenerated by treatment with (1) an aqueous solution of a strong inorganic acid such as hydrochloric or sulphuric acid and (2) an aqueous solution of sodium hydroxide.
摘要翻译： PCT No.PCT / GB92 / 02233 Sec。 371日期1994年5月9日 102（e）日期1994年5月9日PCT提交1992年12月1日PCT公布。公开号WO93 / 11287 日期：1993年6月10日。用于制造再生纤维素的胺N-氧化物如N-甲基吗啉N-氧化物的水溶液可以通过强碱性阴离子交换树脂进行纯化。通过用（1）强无机酸的水溶液（如盐酸或硫酸）和（2）氢氧化钠水溶液处理来再生树脂。

8. 发明授权

US5118423A Method of removing water from a dilute solution of N-methylmorpholine-N-oxide, N-methylmorpholine, or morpholine 失效
标题翻译：从N-甲基吗啉-N-氧化物，N-甲基吗啉或吗啉的稀释溶液中除去水的方法
公开(公告)号：US5118423A
公开(公告)日：1992-06-02
申请号：US675565
申请日：1991-03-27
申请人： Stephan Astegger , Dieter Eichinger , Heinrich Firgo , Karin Weinzierl , Bernd Wolschner , Stefan Zikeli
发明人： Stephan Astegger , Dieter Eichinger , Heinrich Firgo , Karin Weinzierl , Bernd Wolschner , Stefan Zikeli
IPC分类号： B01D61/02 , C02F1/44 , C07D295/00 , C07D295/02 , C07D295/023 , C07D295/22 , C07D295/24 , D01F13/02
CPC分类号： C07D295/023 , B01D61/025 , C02F1/441 , D01F13/02 , Y02P70/627
摘要： For the removal of water from dilute aqueous solution of NMMO, N-methylmorpholine or morpholine or mixtures thereof, the solution is subjected to reverse osmosis at a pressure in excess of the osmotic pressure and probably around 40 bar and a temperature of 25.degree. C. to 75.degree. C. to form a retentate containing the amines and a permeate which is practically free from the amines. The permeate can be used as process water while the retentate can be worked up to NMMO for reuse in the cellulose solubilization process.
摘要翻译：为了从NMMO，N-甲基吗啉或吗啉或其混合物的稀水溶液中除去水，溶液在超过渗透压的压力下可能约为40巴，温度为25℃进行反渗透。至75℃以形成含有胺的渗余物和实际上不含胺的渗透物。渗透物可以用作工艺水，同时可以将渗余物加工至NMMO以在纤维素增溶过程中重新使用。

9. 发明授权

US3397960A Conversion of trithiane into carbon disulfide 失效
标题翻译：三噻烷转化成二硫化碳
公开(公告)号：US3397960A
公开(公告)日：1968-08-20
申请号：US59926466
申请日：1966-12-05
申请人： GLANZSTOFF AG
发明人： HANS-DIETER RUPP , ERHARD SIGGEL , GERHARD MEYER , HELMUT MAGERLEIN
IPC分类号： C01B31/26 , D01F13/02
CPC分类号： D01F13/02 , C01B32/70 , Y02P70/627

10. 发明授权

US3278657A Oil recovery in wet-spinning process 失效
标题翻译：湿法纺丝过程中的油回收
公开(公告)号：US3278657A
公开(公告)日：1966-10-11
申请号：US21865762
申请日：1962-08-22
申请人： CELANESE CORP
发明人： CLEMENTS JAMES S , LAUGHLIN KENNETH C
IPC分类号： D01F2/28
CPC分类号： C10G31/00 , D01F13/02 , Y02P70/627

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