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1. 发明授权

US5904818A Process for the regeneration of an aqueous process liquid of the amine-oxide process 失效
标题翻译：用于再生氧化胺工艺的含水工艺液体的方法
公开(公告)号：US5904818A
公开(公告)日：1999-05-18
申请号：US843851
申请日：1997-04-17
申请人： Wolfram Kalt , Dieter Eichinger , Bruno Mangeng , Heinrich Firgo
发明人： Wolfram Kalt , Dieter Eichinger , Bruno Mangeng , Heinrich Firgo
IPC分类号： C07D295/24 , C07D295/28 , C08B1/00 , D01F2/00 , D01F13/02 , C07D3/00 , C07D265/30
CPC分类号： C07D295/24 , C07D295/28 , C08B1/003 , D01F13/02 , D01F2/00 , Y02P70/627
摘要： The invention is concerned with a process for the production of a solution of N-methylmorpholine-N-oxide in water, characterized by the following steps:(a) providing an aqueous solution containing N-methylmorpholine and morpholine and exhibiting a pH value of from 6.0 to 9.0, thereafter(b) treating said aqueous solution with a peroxidic oxidant to oxidize N-methylmorpholine to N-methylmorpholine-N-oxide.
摘要翻译：本发明涉及一种制备N-甲基吗啉-N-氧化物在水中的溶液的方法，其特征在于以下步骤：（a）提供含有N-甲基吗啉和吗啉的水溶液，其pH值为 6.0〜9.0，此后（b）用过氧化物氧化剂处理所述水溶液以将N-甲基吗啉氧化成N-甲基吗啉-N-氧化物。

2. 发明授权

US5858285A Process for the production of an aqueous solution of a tertiary amine-oxide 失效
标题翻译：制备叔胺氧化物水溶液的方法
公开(公告)号：US5858285A
公开(公告)日：1999-01-12
申请号：US843395
申请日：1997-04-15
申请人： Johann Manner , Heinrich Firgo , Bruno Mangeng , Eduard Mulleder , Wolfram Kalt
发明人： Johann Manner , Heinrich Firgo , Bruno Mangeng , Eduard Mulleder , Wolfram Kalt
IPC分类号： C07D295/28 , C08B1/00 , D01F2/00 , D01F13/02 , D01F2/02
CPC分类号： C07D295/28 , C08B1/003 , D01F13/02 , D01F2/00 , Y02P70/627
摘要： The invention is concerned with a process for the production of an aqueous amine-oxide solution used in the amine-oxide process for the production of a mouldable cellulose solution, wherein aqueous, amine-oxide containing solutions produced in said amine-oxide process particularly as precipitation baths are purified and concentrated, characterized in that a microbiocide agent is added to said aqueous, amine-oxide containing solutions before, during or after purification.
摘要翻译：本发明涉及生产用于制备可模塑纤维素溶液的氧化胺方法中的氧化胺水溶液的方法，其中在所述氧化胺方法中生产的含水氧化胺的溶液特别是纯化和浓缩沉淀浴，其特征在于，在纯化之前，期间或之后，向所述含水胺氧化物溶液中加入杀微生物剂。

3. 发明授权

US5628941A Process for the production of cellulose moulded bodies 失效
标题翻译：生产纤维素成型体的方法
公开(公告)号：US5628941A
公开(公告)日：1997-05-13
申请号：US454320
申请日：1995-06-05
申请人： Wolfram Kalt , Heinrich Firgo , Johann Manner , Eduard Mulleder , Bruno Mangeng , Arnold Nigsch , Franz Schwenninger , Christoph Schrempf
发明人： Wolfram Kalt , Heinrich Firgo , Johann Manner , Eduard Mulleder , Bruno Mangeng , Arnold Nigsch , Franz Schwenninger , Christoph Schrempf
IPC分类号： D01F2/02 , B01J39/22 , B01J41/16 , C07C291/04 , C08B1/00 , C08J3/09 , C08J5/00 , C08L1/02 , D01F2/00 , D01F13/02 , C07C291/00 , D01F2/24
CPC分类号： C07C291/04 , C08B1/003 , C08J3/096 , C08L1/02 , D01F2/00 , C08J2301/00
摘要： The invention is concerned with a process for the production of cellulose moulded bodies. In this process, cellulose is first dissolved in an aqueous solution of a tertiary amine-oxide, in particular N-methylmorpholine-N-oxide (NMMO), to produce a mouldable cellulose solution. Second, the cellulose solution is molded and conducted into an aqueous precipitation bath, wherein the cellulose is precipitated, which produces a moulded body and a spent precipitation bath. Next, the spent precipitation bath is regenerated. This regenerated aqueous amine-oxide solution is re-used to dissolve cellulose, thereby repeating the process. In the above process, the repeated aqueous amine-oxide solution has a pH within certain defined limits.
摘要翻译： PCT No.PCT / AT95 / 00021 Sec。 371日期：1995年6月5日 102（e）日期1995年6月5日PCT 1995年2月1日PCT PCT。第WO95 / 23827号公报日期1995年9月8日本发明涉及生产纤维素成型体的方法。在该方法中，首先将纤维素溶解在叔胺氧化物，特别是N-甲基吗啉-N-氧化物（NMMO）的水溶液中，以制备可塑的纤维素溶液。其次，将纤维素溶液模塑并导入含水沉淀浴中，其中纤维素被沉淀，产生成型体和废沉淀浴。接下来，废水沉淀浴再生。该再生的氧化胺水溶液再次用于溶解纤维素，从而重复该过程。在上述方法中，重复的氧化胺水溶液的pH值在一定的限定范围内。

4. 发明授权

US6113799A Process for selective separation of morpholine 失效
标题翻译：选择性分离吗啉的方法
公开(公告)号：US6113799A
公开(公告)日：2000-09-05
申请号：US843850
申请日：1997-04-17
申请人： Bruno Mangeng , Heinrich Firgo , Johann Manner
发明人： Bruno Mangeng , Heinrich Firgo , Johann Manner
IPC分类号： C07D295/023 , C07D295/28 , B01D15/04
CPC分类号： C07D295/023 , C07D295/28
摘要： The invention is concerned with a process for the selective separation of morpholine from an aqueous solution containing morpholine, N-methylmorpholine and N-methylmorpholine-N-oxide, characterized by the following steps:(A) passing said aqueous solution over a cation exchanger capable of adsorbing morpholine in such an amount until it cannot be charged substantially with morpholine any more and an eluate substantially free from morpholine but containing N-methyhnorpholine and N-methylmorpholine-N-oxide is obtained, and(B) regenerating the cation exchanger charged with morpholine and reusing it in step (A).
摘要翻译：本发明涉及从含有吗啉，N-甲基吗啉和N-甲基吗啉-N-氧化物的水溶液中选择性分离吗啉的方法，其特征在于以下步骤：（A）使所述水溶液通过具有阳离子交换能力吸附吗啉直到不能充分地加入吗啉，得到基本上不含吗啉但含有N-甲基吗啉-N-甲基吗啉-N-氧化物的洗脱液，（B）再生阳离子交换剂，吗啉并在步骤（A）中重复使用。

5. 发明授权

US5795488A Process for transporting a solution of cellulose in an aqueous tertiary amine-oxide 失效
标题翻译：在叔胺氧化物水溶液中输送纤维素溶液的方法
公开(公告)号：US5795488A
公开(公告)日：1998-08-18
申请号：US715763
申请日：1996-09-19
申请人： Wolfram Kalt , Johann Manner , Heinrich Firgo , Franz Schwenninger
发明人： Wolfram Kalt , Johann Manner , Heinrich Firgo , Franz Schwenninger
IPC分类号： C07D295/22 , B01D29/01 , B29C47/68 , D01D1/06 , D01F2/00 , F04C15/00 , F16K51/00 , B01D37/00
CPC分类号： D01D1/06 , B01D29/01
摘要： The invention is concerned with a process for transporting a solution of cellulose in an aqueous tertiary amine-oxide through a component wherein said cellulose solution has different flow rates in said component, characterized in that an outlet wherethrough part of said cellulose solution is discharged from said component is provided at a point within said component whereat said flow rate is relatively low. (FIG. 2)
摘要翻译：本发明涉及一种在叔胺氧化物水溶液中输送纤维素溶液的方法，其中所述纤维素溶液在所述组分中具有不同的流速，其特征在于，通过部分所述纤维素溶液从所述在所述组分内的点处提供组分，其中所述流速相对较低。（图2）

6. 发明授权

US5679146A Moulding materials and spinning materials containing cellulose 失效
标题翻译：含纤维素的成型材料和纺丝材料
公开(公告)号：US5679146A
公开(公告)日：1997-10-21
申请号：US644260
申请日：1996-05-10
申请人： Wolfram Kalt , Johann Manner , Heinrich Firgo
发明人： Wolfram Kalt , Johann Manner , Heinrich Firgo
IPC分类号： C08B1/00 , C08J5/18 , C08K5/17 , C08L1/00 , C08L1/02 , D01F2/00 , D01F2/02 , C09D101/02 , C09D101/24
CPC分类号： C08L1/02 , D01F2/00
摘要： Moulding material and spinning material respectively containing cellulose, an aqueous tertiary amine-oxide, a non-solvent and a stabiliser, characterised in that, one or more stabilisers are provided which altogether have a basic and antioxidant action with the proviso that the basic stabiliser is not phosphate. The moulding material and spinning material respectively according to the invention are thermally stabilised against a runaway of the decomposition reaction. The degradation of the cellulose and of the amine-oxide is also largely prevented.
摘要翻译：分别含有纤维素，叔胺氧化物，非溶剂和稳定剂的成型材料和纺丝材料，其特征在于，提供一种或多种稳定剂，其总共具有碱性和抗氧化作用，条件是碱性稳定剂是不是磷酸盐。分别根据本发明的成型材料和纺丝材料对于分解反应的失控而进行热稳定化。纤维素和氧化胺的降解也大大地被防止。

7. 发明授权

US5503749A Process for the purification of aqueous solutions of amine-oxides 失效
标题翻译：纯化氧化胺水溶液的方法
公开(公告)号：US5503749A
公开(公告)日：1996-04-02
申请号：US424266
申请日：1995-04-19
申请人： Johann Manner , Heinrich Firgo , Wolfram Kalt , Werner Richardt
发明人： Johann Manner , Heinrich Firgo , Wolfram Kalt , Werner Richardt
IPC分类号： B01D61/24 , D01F13/02 , B01D15/04
CPC分类号： B01D61/246 , D01F13/02 , Y02P70/627
摘要： A process for the purification of aqueous solutions of amine-oxides, characterized in that said solutions are contacted with an aqueous purification solution of an alkali hydroxide and/or ion pair reagent by means of an anion active membrane. By means of the process according to the invention, an efficient separation, particularly of anions of lower carboxylic acids and inorganic acids, can be achieved.
摘要翻译： PCT No.PCT / AT94 / 00105 Sec。 371日期1995年04月19日 102（e）1995年4月19日PCT PCT 1994年8月2日PCT公布。出版物WO95 / 05888 日本1993年3月2日。一种用于纯化氧化胺水溶液的方法，其特征在于所述溶液通过阴离子活性膜与碱金属氢氧化物和/或离子对试剂的水性纯化溶液接触。通过本发明的方法，可以实现有效的分离，特别是低级羧酸和无机酸的阴离子。

8. 发明授权

US5766530A Process for the production of cellulose moulded bodies 失效
标题翻译：生产纤维素成型体的方法
公开(公告)号：US5766530A
公开(公告)日：1998-06-16
申请号：US471842
申请日：1995-06-06
申请人： Wolfram Kalt , Johann Manner , Arnold Nigsch , Heinrich Firgo , Christian Hager , Wolfgang Helmut Schkorwaga
发明人： Wolfram Kalt , Johann Manner , Arnold Nigsch , Heinrich Firgo , Christian Hager , Wolfgang Helmut Schkorwaga
IPC分类号： D01D4/02 , D01F2/00 , B29C47/00
CPC分类号： D01F2/00
摘要： The invention is concerned with a process for the production of cellulose moulded bodies wherein a suspension of cellulose in an aqueous solution of a tertiary amine-oxide is transformed into a mouldable solution, said solution being extruded by means of a forming tool and conducted into a precipitation bath. The process is characterized in that at least part of the materials in devices and pipes for the transportation and processing of the solution, which material is in contact with the mouldable solution contains at a minimum of 90% up to a depth of at least 0,5 .mu.m, preferably more than 1 .mu.m, at least one element of the group consisting of titanium, zirconium, chromium and nickel in elementary form and/or in the form of compounds provided that the remaining of the material does not contain any of the elements of the group consisting of copper, molybdenum, tungsten or cobalt. By means of the use of certain elements and compounds according to the invention, it is possible to control the occurrence and the extent of exothermal degradation reactions in the cellulose solution.
摘要翻译：本发明涉及生产纤维素模塑体的方法，其中将纤维素在叔胺氧化物的水溶液中的悬浮液转化成可模制的溶液，所述溶液通过成形工具挤出并进入沉淀浴该方法的特征在于，用于运输和处理溶液的装置和管道中的至少一部分材料，该材料与可成型溶液接触，包含至少90％，至少为0的深度， 5微米，优选大于1微米，元素形式和/或化合物形式的钛，锆，铬和镍中的至少一种元素，条件是剩余的材料不含任何由铜，钼，钨或钴组成的组元素。通过使用根据本发明的某些元素和化合物，可以控制纤维素溶液中放热降解反应的发生和程度。

9. 发明授权

US5556452A Moulding materials and spinning materials containing cellulose 失效
标题翻译：含纤维素的成型材料和纺丝材料
公开(公告)号：US5556452A
公开(公告)日：1996-09-17
申请号：US293056
申请日：1994-08-19
申请人： Wolfram Kalt , Johann M anner , Heinrich Firgo
发明人： Wolfram Kalt , Johann M anner , Heinrich Firgo
IPC分类号： C08B1/00 , C08J5/18 , C08K5/17 , C08L1/00 , C08L1/02 , D01F2/00 , D01F2/02 , C08L1/24 , C09D101/02 , C09D101/24
CPC分类号： C08L1/02 , D01F2/00
摘要： Moulding material and spinning material respectively containing cellulose, an aqueous tertiary amine-oxide, a non-solvent and a stabiliser, characterised in that, one or more stabilisers are provided which altogether have a basic and antioxidant action with the proviso that the basic stabiliser is not phosphate. The moulding material and spinning material respectively according to the invention are thermally stabilised against a runaway of the decomposition reaction. The degradation of the cellulose and of the amine-oxide is also largely prevented.
摘要翻译：分别含有纤维素，叔胺氧化物，非溶剂和稳定剂的成型材料和纺丝材料，其特征在于提供一种或多种稳定剂，其总共具有碱性和抗氧化作用，条件是碱性稳定剂是不是磷酸盐。分别根据本发明的成型材料和纺丝材料对于分解反应的失控而进行热稳定化。纤维素和氧化胺的降解也大大地被防止。

10. 发明授权

US5216144A Method of producing shaped cellulosic articles 失效
标题翻译：生产形状纤维素制品的方法
公开(公告)号：US5216144A
公开(公告)日：1993-06-01
申请号：US804335
申请日：1991-12-06
申请人： Dieter Eichinger , Raimund Jurkovic , Stephan Astegger , Heinrich Firgo , Peter Hinterholzer , Karin Weinzierl , Stefan Zikeli
发明人： Dieter Eichinger , Raimund Jurkovic , Stephan Astegger , Heinrich Firgo , Peter Hinterholzer , Karin Weinzierl , Stefan Zikeli
IPC分类号： D01F2/02 , C08B1/00 , C08L1/02 , D01F2/00
CPC分类号： D01F2/00 , C08B1/003 , C08L1/02
摘要： Shaped cellulosic bodies and especially cellulosic fibers or filaments are produced by precipitating cellulose from a solution containing cellulose and NMMO. To allow elevated concentrations of NMMO in the precipitating bath without detriment to the properties of the fibers or filaments produced, the temperature of the precipitating bath is held at most at 0.degree. C.
摘要翻译：通过从含有纤维素和NMMO的溶液中沉淀纤维素而产生成型的纤维素体，特别是纤维素纤维或长丝。为了使沉淀池中的NMMO浓度升高而不损害所生产的纤维或长丝的性质，沉淀浴的温度最多保持在0℃。

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