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    • 9. 发明申请
    • Tunable microwave resonator for static dynamic nuclear polarization (DNP)
    • 用于静态动态核极化(DNP)的可调微波谐振器
    • US20160334476A1
    • 2016-11-17
    • US15112661
    • 2015-01-20
    • DOTY SCIENTIFIC, INC.
    • David Doty
    • G01R33/28G01R33/38
    • G01R33/282G01R33/38
    • A tunable millimeter-wave (mmw) DNP probe head is disclosed that is compatible with efficient H/X/Y/e− DNP in samples that may have volume large compared to λ03, where λ0 is the free-space wavelength at the frequency fe of the electron paramagnetic resonance (EPR) when placed in an external polarizing field B0, where B0 is typically in the range of 6.5 T to 35 T, corresponding to fe in the range of 180-1000 GHz, and corresponding to proton resonance frequency fH in the range of 280 MHz to 1500 MHz. The probe head comprises a tune cavity of adjustable volume, a sample cavity that is large compared to the sample wavelength, a tapered conical feed transition filled with a high dielectric material at the small end, and a selectively reflective wall that is substantially reflective of electromagnetic radiation at fe but substantially transparent to electromagnetic radiation at fH.
    • 公开了可调谐毫米波(mmw)DNP探针头,其与λ03相比可能具有体积大的样品中的有效H / X / Y / e-DNP兼容,其中λ0是频率fe的自由空间波长 的电子顺磁共振(EPR)放置在外部偏振场B0中,其中B0通常在6.5T至35T的范围内,对应于在180-1000GHz的范围内的fe,并且对应于质子谐振频率fH 在280MHz至1500MHz的范围内。 探头包括可调节体积的调谐空腔,与样品波长相比较大的样品腔,在小端填充有高电介质材料的锥形进给转变,以及基本反射电磁的选择性反射壁 在fH处的辐射,但在fH处的电磁辐射基本透明。