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    • 3. 发明授权
    • Unit for catalytic gas nitrogenation of steels and alloys
    • 钢和合金催化气体氮化装置
    • US07931854B2
    • 2011-04-26
    • US12535354
    • 2009-08-04
    • Vladimir Yakovlevich Syropyatov
    • Vladimir Yakovlevich Syropyatov
    • C21B7/24
    • F27B5/04F27B5/18F27D19/00F27D21/00F27D2019/0012
    • Equipment for thermochemical treatment of steels and alloys in gaseous mediums with automatic control includes a heating furnace with/without a muffle, a process gas catalyst impact block located in the furnace, a mechanism for supply, mixing, proportioning and extraction of process gases and a device of indirect monitoring and control of the nitrogen potential in the furnace atmosphere. The device of indirect monitoring and control of the nitrogen potential in the furnace atmosphere is an oxygen sensor, a secondary transducer with indication of the nitrogen potential in weight units of nitrogen content in iron and an actuator, while the process gas catalyst impact block is located in the furnace on the process gas supply line. The technical result achieved is that reliability and stability of processes are significantly increased, as well as the period of nitriding is reduced due to integrated process automation that is available.
    • 用于具有自动控制的气体介质中的钢和合金的热化学处理设备包括具有/不具有马弗的加热炉,位于炉中的工艺气体催化剂冲击块,用于提供,混合,配制和提取工艺气体的机构以及 间接监测和控制炉气中氮势的装置。 间接监测和控制炉气氛中氮势的装置是氧传感器,二次换能器,其中指示在铁和致动器中氮含量的重量单位为氮势,而处理气体催化剂冲击块位于 在炉内工艺气供应线。 获得的技术成果是可靠性和稳定性得到显着提高,并且由于可用的集成过程自动化,氮化时间减少。
    • 6. 发明申请
    • Method for performing thermal reactions between reactants and a furnace for same
    • 用于在反应物和与其相同的炉子之间进行热反应的方法
    • US20040126299A1
    • 2004-07-01
    • US10468866
    • 2003-11-05
    • Dag OvrebnullWilliam George Clark
    • C01B035/04C01B031/34
    • F27B7/06C01B21/06C01B21/0765C01B32/914C01B32/921C01B35/04C01P2004/61C01P2004/62C01P2006/80F27B7/26F27B7/34F27D5/0068F27D2019/0012F27D2099/0008
    • The present invention relates to thermal reactions performed at rapid transient temperatures, and a furnace (1) able to perform such reactions. The method and the furnace may suitably be applied to perform reactions between reactants where significant losses normally occur at certain transient temperatures or temperature ranges. One practical application of the present invention relates to a carbothermic method for producing Refractory Hard Metal powders, such as borides, nitrides and carbides, and a furnace designed for the performance of the method. In accordance with this method Refractory Hard Metal powders, such as boride powders can be produced with reduced loss of reactants such as C and B2O3. This can be achieved by rapid heating of the mixture containing the reactants in a critical temperature range. For the performance of this particular embodiment a two-step furnace has been applied, where the temperature in each individual temperature zone (37, 38) Is respectively below and above critical temperatures of the reaction. In accordance with one embodiment of the present invention high purified boride, carbide and nitride powders with a fine grain size can be produced in a simple and cost effective manner.
    • 本发明涉及在快速瞬态温度下进行的热反应,以及能够进行这种反应的炉(1)。 该方法和炉可以适当地用于在某些瞬时温度或温度范围内通常发生显着损失的反应物之间进行反应。 本发明的一个实际应用涉及用于制备耐火硬金属粉末的碳热还原法,例如硼化物,氮化物和碳化物,以及为实现该方法而设计的炉。 根据该方法,可以减少诸如C和B 2 O 3的反应物的损失来制备诸如硼化物粉末的耐火硬金属粉末。 这可以通过在临界温度范围内快速加热含有反应物的混合物来实现。 对于该特定实施例的性能,已经应用了两步骤炉,其中每个单独温度区(37,38)中的温度分别低于和高于反应的临界温度。 根据本发明的一个实施方案,可以以简单且成本有效的方式制备具有细晶粒度的高纯度硼化物,碳化物和氮化物粉末。