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1. 发明授权

US08980460B2 Methods and electrolytes for electrodeposition of smooth films 有权
标题翻译：用于电沉积光滑膜的方法和电解质
公开(公告)号：US08980460B2
公开(公告)日：2015-03-17
申请号：US13495727
申请日：2012-06-13
申请人： Jiguang Zhang , Wu Xu , Gordon L. Graff , Xilin Chen , Fei Ding , Yuyan Shao
发明人： Jiguang Zhang , Wu Xu , Gordon L. Graff , Xilin Chen , Fei Ding , Yuyan Shao
IPC分类号： H01M4/04 , C09D5/44 , C25D3/02 , C25D3/12 , C25D3/20 , C25D3/22 , C25D3/30 , C25D3/38 , C25D3/42 , C25D3/46 , C25D3/48 , C25D3/50 , C25D5/00 , C25D13/22
CPC分类号： C25D3/56 , C09D5/4484 , C25D3/02 , C25D3/12 , C25D3/20 , C25D3/22 , C25D3/30 , C25D3/38 , C25D3/42 , C25D3/46 , C25D3/48 , C25D3/50 , C25D5/00 , C25D13/22
摘要： Electrodeposition involving an electrolyte having a surface-smoothing additive can result in self-healing, instead of self-amplification, of initial protuberant tips that give rise to roughness and/or dendrite formation on the substrate and/or film surface. For electrodeposition of a first conductive material (C1) on a substrate from one or more reactants in an electrolyte solution, the electrolyte solution is characterized by a surface-smoothing additive containing cations of a second conductive material (C2), wherein cations of C2 have an effective electrochemical reduction potential in the solution lower than that of the reactants.
摘要翻译：涉及具有表面平滑添加剂的电解质的电沉积可以导致在基材和/或膜表面上产生粗糙和/或枝晶形成的初始突起尖端的自愈而不是自我扩增。为了从电解质溶液中的一种或多种反应物在基底上电沉积第一导电材料（C1），电解质溶液的特征在于包含第二导电材料（C2）的阳离子的表面平滑添加剂，其中C2的阳离子溶液中的有效电化学还原电位低于反应物的电化学还原电位。

2. 发明申请

US20140166491A1 METHODS FOR PRODUCING TEXTURED ELECTRODE BASED ENERGY STORAGE DEVICE 审中-公开
标题翻译：用于生产基于纹理电极的能量储存装置的方法
公开(公告)号：US20140166491A1
公开(公告)日：2014-06-19
申请号：US14016406
申请日：2013-09-03
申请人： NANOSCALE COMPONENTS, INC.
发明人： Robert W. Grant , Matthew Sweetland
IPC分类号： H01G9/00 , H01M4/04
CPC分类号： H01M4/366 , C09D5/24 , C09D179/02 , C25D3/42 , C25D5/40 , C25D5/44 , C25D9/02 , C25D11/00 , C25D13/12 , C25F3/04 , H01G9/0029 , H01G9/042 , H01G11/24 , H01G11/48 , H01G11/52 , H01G11/86 , H01M2/1653 , H01M4/0452 , H01M4/0461 , H01M4/0466 , H01M4/134 , H01M4/137 , H01M4/1395 , H01M4/1399 , H01M10/052 , H01M10/0525 , Y02E60/13
摘要： This method enables the use of nanowire or nano-textured forms of Polyaniline and other conductive polymers in energy storage components. The delicate nature of these very high surface area materials are preserved during the continuous electrochemical synthesis, drying, solvent application and physical assembly. The invention also relates to a negative electrode that is comprised of etched, lithiated aluminum that is safer and lighter weight than conventional carbon based lithium-ion negative electrodes. The invention provides for improved methods for making negative and positive electrodes and for energy storage devices containing them. The invention provides sufficient stability in organic solvent and electrolyte solutions, where the prior art processes commonly fail. The invention further provides stability during repetitive charge and discharge. The invention also provides for novel microstructure protecting support membranes to be used in an energy storage device.
摘要翻译：该方法能够在能量存储组件中使用纳米线或纳米纹理形式的聚苯胺和其它导电聚合物。在连续电化学合成，干燥，溶剂应用和物理组装过程中，这些非常高的表面积材料的微妙性质得以保留。本发明还涉及一种负极，其由蚀刻的锂化铝组成，其比常规碳基锂离子负极更安全和更轻。本发明提供了用于制造负极和正极以及包含它们的储能装置的改进方法。本发明在有机溶剂和电解质溶液中提供足够的稳定性，其中现有技术的方法通常失效。本发明进一步提供重复充电和放电期间的稳定性。本发明还提供了用于能量存储装置中的用于新颖的微结构保护支撑膜。

3. 发明授权

US08529746B2 Methods for producing textured electrode based energy storage device 失效
标题翻译：用于生产基于感应电极的储能装置的方法
公开(公告)号：US08529746B2
公开(公告)日：2013-09-10
申请号：US13018586
申请日：2011-02-01
申请人： Robert W. Grant , Matthew Sweetland
发明人： Robert W. Grant , Matthew Sweetland
IPC分类号： H01M4/139 , C25D9/02
CPC分类号： H01M4/366 , C09D5/24 , C09D179/02 , C25D3/42 , C25D5/40 , C25D5/44 , C25D9/02 , C25D11/00 , C25D13/12 , C25F3/04 , H01G9/0029 , H01G9/042 , H01G11/24 , H01G11/48 , H01G11/52 , H01G11/86 , H01M2/1653 , H01M4/0452 , H01M4/0461 , H01M4/0466 , H01M4/134 , H01M4/137 , H01M4/1395 , H01M4/1399 , H01M10/052 , H01M10/0525 , Y02E60/13
摘要： This method enables the use of nanowire or nano-textured forms of Polyaniline and other conductive polymers in energy storage components. The delicate nature of these very high surface area materials are preserved during the continuous electrochemical synthesis, drying, solvent application and physical assembly. The invention also relates to a negative electrode that is comprised of etched, lithiated aluminum that is safer and lighter weight than conventional carbon based lithium-ion negative electrodes. The invention provides for improved methods for making negative and positive electrodes and for energy storage devices containing them. The invention provides sufficient stability in organic solvent and electrolyte solutions, where the prior art processes commonly fail. The invention further provides stability during repetitive charge and discharge. The invention also provides for novel microstructure protecting support membranes to be used in an energy storage device.
摘要翻译：该方法能够在能量存储组件中使用纳米线或纳米纹理形式的聚苯胺和其它导电聚合物。在连续电化学合成，干燥，溶剂应用和物理组装过程中，这些非常高的表面积材料的微妙性质得以保留。本发明还涉及一种负极，其由蚀刻的锂化铝组成，其比常规碳基锂离子负极更安全和更轻。本发明提供了用于制造负极和正极以及包含它们的储能装置的改进方法。本发明在有机溶剂和电解质溶液中提供足够的稳定性，其中现有技术的方法通常失效。本发明进一步提供重复充电和放电期间的稳定性。本发明还提供了用于能量存储装置中的用于新颖的微结构保护支撑膜。

4. 发明申请

US20110195293A1 METHODS FOR PRODUCING TEXTURED ELECTRODE BASED ENERGY STORAGE DEVICE 失效
标题翻译：用于生产基于纹理电极的能量储存装置的方法
公开(公告)号：US20110195293A1
公开(公告)日：2011-08-11
申请号：US13018586
申请日：2011-02-01
申请人： Robert W. Grant , Matthew Sweetland
发明人： Robert W. Grant , Matthew Sweetland
IPC分类号： H01M2/18 , H01M4/60 , B05D5/12 , B05D3/14 , B05D3/04 , B05D3/02 , B05D3/00 , H01G9/035 , B82Y99/00
CPC分类号： H01M4/366 , C09D5/24 , C09D179/02 , C25D3/42 , C25D5/40 , C25D5/44 , C25D9/02 , C25D11/00 , C25D13/12 , C25F3/04 , H01G9/0029 , H01G9/042 , H01G11/24 , H01G11/48 , H01G11/52 , H01G11/86 , H01M2/1653 , H01M4/0452 , H01M4/0461 , H01M4/0466 , H01M4/134 , H01M4/137 , H01M4/1395 , H01M4/1399 , H01M10/052 , H01M10/0525 , Y02E60/13
摘要： This method enables the use of nanowire or nano-textured forms of Polyaniline and other conductive polymers in energy storage components. The delicate nature of these very high surface area materials are preserved during the continuous electrochemical synthesis, drying, solvent application and physical assembly. The invention also relates to a negative electrode that is comprised of etched, lithiated aluminum that is safer and lighter weight than conventional carbon based lithium-ion negative electrodes. The invention provides for improved methods for making negative and positive electrodes and for energy storage devices containing them. The invention provides sufficient stability in organic solvent and electrolyte solutions, where the prior art processes commonly fail. The invention further provides stability during repetitive charge and discharge. The invention also provides for novel microstructure protecting support membranes to be used in an energy storage device.
摘要翻译：该方法能够在能量存储组件中使用纳米线或纳米纹理形式的聚苯胺和其它导电聚合物。在连续电化学合成，干燥，溶剂应用和物理组装过程中，这些非常高的表面积材料的微妙性质得以保留。本发明还涉及一种负极，其由蚀刻的锂化铝组成，其比常规碳基锂离子负极更安全和更轻。本发明提供了用于制造负极和正极以及包含它们的储能装置的改进方法。本发明在有机溶剂和电解质溶液中提供足够的稳定性，其中现有技术的方法通常失效。本发明进一步提供重复充电和放电期间的稳定性。本发明还提供了用于能量存储装置中的用于新颖的微结构保护支撑膜。

5. 发明申请

US20070114132A1 Device and method for separating metals and/or metal alloys from metallo-organic electrolytes 审中-公开
标题翻译：从金属有机电解质中分离金属和/或金属合金的装置和方法
公开(公告)号：US20070114132A1
公开(公告)日：2007-05-24
申请号：US10569658
申请日：2004-08-17
申请人： Jorg Heller , Hans De Vries
发明人： Jorg Heller , Hans De Vries
IPC分类号： C25D21/20
CPC分类号： C25D17/00 , C25D3/42 , C25D5/003 , C25D17/02
摘要： The invention relates to a device (1) for separating metals and/or metal alloys from metallo-organic electrolytes and depositing the same on products (7), said device comprising at least one coating section (3) for coating the products (7), at least one other treatment section (2,4), and at least one lock chamber (20,40) for introducing and discharging the products (7) into and out of the device (1) essentially without permeation of oxygen and/or humidity. The inventive device is provided with at least one siphon rinsing unit (60,61) comprising a separating element (53,54) for the gas-related separation of the other sections (2,4) of the device from the coating section (3), or for sealing said other sections (2,4) in relation to the coating section (3), and at least one hood part (5) that can be flooded with an inert gas and tightly surrounds essentially the coating section (3), the at least one siphon rinsing unit (60,61), and the at least one other treatment section (2,4). The invention also relates to a corresponding method whereby products (7) are introduced into the device in such a way that there is essentially no solvent loss, said products are delivered to at least one coating section (3) essentially in a gas-tight manner, they are then coated, and delivered to at least one output section (4) essentially in an gas-tight manner, and the finished products (7) are discharged. An inert-gas atmosphere cap is provided over all of the sections (50,51,52) of the inventive device.
摘要翻译：本发明涉及一种用于从金属 - 有机电解质中分离金属和/或金属合金并将其沉积在产品（7）上的装置（1），所述装置包括用于涂覆产品（7）的至少一个涂覆部分（3），至少一个其它处理部分（2,4）和至少一个用于将产品（7）引入和排出装置（1）的至少一个锁定室（20,40），基本上不渗透氧气和/或湿度。本发明的装置设置有至少一个虹吸冲洗单元（60,61），其包括分离元件（53,54），用于将装置的其它部分（2,4）与涂覆部分（3）进行气体分离）或用于相对于涂覆部分（3）密封所述其它部分（2,4），以及可以充满惰性气体的至少一个罩部分（5），并基本上紧密地围绕涂覆部分（3），所述至少一个虹吸冲洗单元（60,61）和所述至少一个其它处理部（2,4）。本发明还涉及一种相应的方法，其中产品（7）以基本上没有溶剂损失的方式引入装置中，所述产品基本上以气密方式输送到至少一个涂布部分（3）然后将它们涂覆并基本上以气密的方式输送到至少一个输出部分（4），并且成品（7）被排出。在本发明装置的所有部分（50,51,52）上提供惰性气体气体盖。

6. 发明授权

US3953234A Electrodeposition and electrodissolution of alkali metals in nonaqueous solution 失效
标题翻译：碱金属在非水溶液中的电沉积和电解
公开(公告)号：US3953234A
公开(公告)日：1976-04-27
申请号：US669373
申请日：1967-09-21
申请人： Arthur Kentaro Hoffmann
发明人： Arthur Kentaro Hoffmann
IPC分类号： C25C1/02 , C25D3/02 , C25D3/42 , H01M6/14 , H01M6/16 , H01M10/36 , H01M6/18
CPC分类号： H01M10/0563 , C25C1/02 , C25D3/02 , C25D3/42 , H01M10/05 , H01M6/14 , H01M6/16
摘要： Electrodepositing alkali metals from an electrolyte system comprising a mixture of sulfur dioxide, an organic solvent and an electrolyte salt substantially soluble in said sulfur dioxide and the organic solvent in admixture.
摘要翻译：从包含二氧化硫，有机溶剂和基本上可溶于所述二氧化硫的电解质盐和混合物中的有机溶剂的混合物的电解质体系电沉积碱金属。

7. 发明授权

US3278400A Electroforming of beryllium 失效
标题翻译：电铸铍
公开(公告)号：US3278400A
公开(公告)日：1966-10-11
申请号：US23588062
申请日：1962-11-06
申请人： ETHYL CORP
发明人： WALTER STROHMEIER
IPC分类号： C25C1/02 , C25D1/00 , C25D3/42 , C25D5/42
CPC分类号： C25D3/42 , C25C1/02 , C25D1/00 , C25D5/42

8. 发明授权

US09752245B2 Non-aqueous electrolyte for rechargeable magnesium ion cell 有权
公开(公告)号：US09752245B2
公开(公告)日：2017-09-05
申请号：US14309132
申请日：2014-06-19
申请人： PELLION TECHNOLOGIES INC.
发明人： Robert Ellis Doe , Ruoban Han , Yossef Gofer , Doron Aurbach , Nir Pour , Evgeny Sterenberg
IPC分类号： H01M10/054 , H01M10/056 , C25D3/66 , H01M10/0568 , H01M10/0569 , C25D3/42 , H01M4/46
CPC分类号： C25D3/66 , C25D3/42 , C25D3/665 , H01M4/466 , H01M10/054 , H01M10/0568 , H01M10/0569 , H01M2300/0025
摘要： A non-aqueous Magnesium electrolyte comprising: (a) at least one organic solvent; (b) at least one electrolytically active, soluble, inorganic Magnesium (Mg) salt complex represented by the formula: MgaZbXc wherein a, b, and c are selected to maintain neutral charge of the molecule, and Z and X are selected such that Z and X form a Lewis Acid, and 1≦a≦10, 1≦b≦5, and 2≦c≦30. Further Z is selected from a group consisting of aluminum, boron, phosphorus, titanium, iron, and antimony; X is selected from the group consisting of I, Br, Cl, F and mixtures thereof. Rechargeable, high energy density Magnesium cells containing an cathode, an Mg metal anode, and an electrolyte of the above-described type are also disclosed.

9. 发明申请

US20160380262A1 METHODS FOR PRODUCING TEXTURED ELECTRODE BASED ENERGY STORAGE DEVICE 审中-公开
标题翻译：用于生产基于纹理电极的能量储存装置的方法
公开(公告)号：US20160380262A1
公开(公告)日：2016-12-29
申请号：US15056342
申请日：2016-02-29
申请人： NANOSCALE COMPONENTS, INC.
发明人： Robert W. Grant , Matthew Sweetland
IPC分类号： H01M4/36 , H01G11/24 , H01G11/48 , H01G11/86 , H01M10/0525 , H01M4/1399 , H01M4/04 , H01M2/16 , C25F3/04 , C25D5/40 , C25D5/44 , C25D11/00 , C25D9/02 , C09D5/24 , C09D179/02 , H01G11/52
CPC分类号： H01M4/366 , C09D5/24 , C09D179/02 , C25D3/42 , C25D5/40 , C25D5/44 , C25D9/02 , C25D11/00 , C25D13/12 , C25F3/04 , H01G9/0029 , H01G9/042 , H01G11/24 , H01G11/48 , H01G11/52 , H01G11/86 , H01M2/1653 , H01M4/0452 , H01M4/0461 , H01M4/0466 , H01M4/134 , H01M4/137 , H01M4/1395 , H01M4/1399 , H01M10/052 , H01M10/0525 , Y02E60/13
摘要： This method enables the use of nanowire or nano-textured forms of Polyaniline and other conductive polymers in energy storage components. The delicate nature of these very high surface area materials are preserved during the continuous electrochemical synthesis, drying, solvent application and physical assembly. The invention also relates to a negative electrode that is comprised of etched, lithiated aluminum that is safer and lighter weight than conventional carbon based lithium-ion negative electrodes. The invention provides for improved methods for making negative and positive electrodes and for energy storage devices containing them. The invention provides sufficient stability in organic solvent and electrolyte solutions, where the prior art processes commonly fail. The invention further provides stability during repetitive charge and discharge. The invention also provides for novel microstructure protecting support membranes to be used in an energy storage device.
摘要翻译：该方法能够在能量存储组件中使用纳米线或纳米纹理形式的聚苯胺和其它导电聚合物。在连续电化学合成，干燥，溶剂应用和物理组装过程中，这些非常高的表面积材料的微妙性质得以保留。本发明还涉及一种负极，其由蚀刻的锂化铝组成，其比常规碳基锂离子负极更安全和更轻。本发明提供了用于制造负极和正极以及包含它们的储能装置的改进方法。本发明在有机溶剂和电解质溶液中提供足够的稳定性，其中现有技术的方法通常失效。本发明进一步提供重复充电和放电期间的稳定性。本发明还提供了用于能量存储装置中的用于新颖的微结构保护支撑膜。

10. 发明申请

US20140174935A1 SURFACE TREATING METHOD OF NEGATIVE ELECTRODE FOR MAGNESIUM SECONDARY BATTERY, NEGATIVE ELECTRODE FOR MAGNESIUM SECONDARY BATTERY, AND MAGNESIUM SECONDARY BATTERY 有权
标题翻译：镁二次电池负极电极表面处理方法，镁二次电池负极和镁二次电池
公开(公告)号：US20140174935A1
公开(公告)日：2014-06-26
申请号：US14136231
申请日：2013-12-20
申请人： DENSO CORPORATION
发明人： Nobuyoshi Sakakibara , Norikazu Adachi , Kenichirou Kami
IPC分类号： C25F3/04 , H01M4/38 , H01M10/054 , C25D3/42
CPC分类号： H01M4/381 , C25D3/42 , H01M10/049 , H01M10/054 , H01M10/446
摘要： A surface treating method of a negative electrode for a magnesium secondary battery is provided, wherein the magnesium secondary battery includes: a negative electrode capable of releasing magnesium ions during discharging and capable of precipitating elemental magnesium during charging; a positive electrode capable of precipitating a magnesium oxide during the discharging and capable of releasing magnesium ions during the charging; and a non-aqueous ion conductor for conducting magnesium ions as conduction species. The surface treating method comprises initializing the negative electrode by performing the discharging to form a bare surface at a surface of the negative electrode.
摘要翻译：提供了一种用于镁二次电池的负极的表面处理方法，其中所述镁二次电池包括：在放电期间能够释放镁离子并且在充电期间能够析出元素镁的负极; 在放电期间能够析出氧化镁并能够在充电期间释放镁离子的正极; 以及用于导电镁离子作为导电物质的非水离子导体。表面处理方法包括通过进行放电来初始化负极，以在负极的表面形成裸露的表面。

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