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    • 3. 发明授权
    • Low cost high speed titanium and its alloy production
    • 低成本高速钛及其合金生产
    • US06824585B2
    • 2004-11-30
    • US10309552
    • 2002-12-03
    • Adrian A. JosephJohn G. Whellock
    • Adrian A. JosephJohn G. Whellock
    • C22B406
    • C22B34/1286C22B4/005C22B34/1272C22B34/1295
    • A method for refining a titanium metal containing ore such as rutile or ilmenite or mixtures to produce titanium ingots or titanium alloys and compounds of titanium involves production of titanium tetrachloride by processing the ore with a chlorinating procedure and removing various impurities by a distillation or similar procedures to form a relatively pure titanium tetrachloride. Thereafter, the titanium tetrachloride is introduced continuously into a reactor at the focal point of a plasma under atmospheric pressures of inert gas along with molten metallic reductant for the initial reduction of gas phase titanium tetrachloride into molten titanium drops which are collected in a set of skulled crucibles. Thereafter, further processing is carried out at atmospheric pressures in under inert gas where the titanium is heated by plasma guns to maximize titanium purity and, in a final optional stage, alloying compounds are added under the same controlled environment and high temperature conditions.
    • 用于精炼含有金属矿的钛金属如金红石或钛铁矿或混合物以生产钛锭或钛合金和钛的化合物的方法涉及通过用氯化方法加工矿石并通过蒸馏或类似程序除去各种杂质来生产四氯化钛 以形成相对纯的四氯化钛。 此后,将四氯化钛连续引入反应器中的等离子体的大气压下的惰性气体与熔融金属还原剂的反应器中,用于将气相四氯化钛初始还原成熔融的钛滴,这些钛液滴被收集在一组头骨 坩埚 此后,在大气压下在惰性气体中进行进一步处理,其中钛被等离子体枪加热以使钛纯度最大化,并且在最终的任选阶段中,在相同的受控环境和高温条件下加入合金化合物。
    • 9. 发明申请
    • Fine Particle Recovery Methods For Valve Metal Powders
    • 阀门金属粉末的细颗粒回收方法
    • US20100158747A1
    • 2010-06-24
    • US12622806
    • 2009-11-20
    • Hitoshi Iijima
    • Hitoshi Iijima
    • C22C27/02B22F9/20C22B3/02
    • C22B34/24B22F9/20C22B5/04C22B34/1268C22B34/1286C22C27/02
    • A process and system for producing tantalum or other valve metal particles is provided comprising forming tantalum particles in a reduction process carried out in a reactor vessel, and using a siphon to transfer fine tantalum particles out of the reaction mixture to a recovery vessel. This particle transfer can occur while the reaction mixture is agitated. The tantalum particles can be automatically withdrawn when the reaction mixture has a depth level greater than the fluid level of the tantalum fine particle recovery vessel, and outflow automatically stops when the fluid levels of the reactor and particle recovery vessel equilibrate. Tantalum or other valve metal powders made by the processes, and capacitors made with valve metal powders are also provided.
    • 提供一种用于生产钽或其它阀金属颗粒的方法和系统,包括在反应器容器中进行的还原过程中形成钽颗粒,并使用虹吸将细小的钽颗粒从反应混合物中转移到回收容器中。 当搅拌反应混合物时,可能发生该颗粒转移。 当反应混合物的深度水平高于钽细颗粒回收容器的液位时,可以自动地取出钽颗粒,当反应器和颗粒回收容器的液面平衡时,流出物自动停止。 还提供了通过该方法制造的钽或其他阀金属粉末,以及由阀金属粉末制成的电容器。