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    • 1. 发明授权
    • Low cost high speed titanium and its alloy production
    • 低成本高速钛及其合金生产
    • US06824585B2
    • 2004-11-30
    • US10309552
    • 2002-12-03
    • Adrian A. JosephJohn G. Whellock
    • Adrian A. JosephJohn G. Whellock
    • C22B406
    • C22B34/1286C22B4/005C22B34/1272C22B34/1295
    • A method for refining a titanium metal containing ore such as rutile or ilmenite or mixtures to produce titanium ingots or titanium alloys and compounds of titanium involves production of titanium tetrachloride by processing the ore with a chlorinating procedure and removing various impurities by a distillation or similar procedures to form a relatively pure titanium tetrachloride. Thereafter, the titanium tetrachloride is introduced continuously into a reactor at the focal point of a plasma under atmospheric pressures of inert gas along with molten metallic reductant for the initial reduction of gas phase titanium tetrachloride into molten titanium drops which are collected in a set of skulled crucibles. Thereafter, further processing is carried out at atmospheric pressures in under inert gas where the titanium is heated by plasma guns to maximize titanium purity and, in a final optional stage, alloying compounds are added under the same controlled environment and high temperature conditions.
    • 用于精炼含有金属矿的钛金属如金红石或钛铁矿或混合物以生产钛锭或钛合金和钛的化合物的方法涉及通过用氯化方法加工矿石并通过蒸馏或类似程序除去各种杂质来生产四氯化钛 以形成相对纯的四氯化钛。 此后,将四氯化钛连续引入反应器中的等离子体的大气压下的惰性气体与熔融金属还原剂的反应器中,用于将气相四氯化钛初始还原成熔融的钛滴,这些钛液滴被收集在一组头骨 坩埚 此后,在大气压下在惰性气体中进行进一步处理,其中钛被等离子体枪加热以使钛纯度最大化,并且在最终的任选阶段中,在相同的受控环境和高温条件下加入合金化合物。
    • 4. 发明授权
    • Metallurgical lance and method of cooling the lance
    • 冶金喷枪和冷却喷枪的方法
    • US5350158A
    • 1994-09-27
    • US39287
    • 1993-04-19
    • John G. Whellock
    • John G. Whellock
    • C21C5/46F27D3/16F27D9/00
    • F27D9/00C21C5/4606C21C5/4646C21C2005/4626
    • A metallurgical lance incorporates an indirect cooling system, separate from and independent of the reactants which are fed through a center passageway (12) to a melt, bath or the like. An outer passageway (10) extends around the center passageway (12) and its outer wall (14) is exposed to heat flux. A coolant flows through the outer passageway (10). Auxiliary means (22) are positioned within the outer passageway (10) to enhance the take-up of heat from the outer wall (14). The coolant is a two-phase mixture, preferably gas and water. The auxiliary means may be a helical fin (22) or a wire packing within the coolant flow path. Enhanced cooling is achieved by (a) the extended metal surface area provided by the auxiliary means, and/or (b) surface evaporation of a film of liquid deposited on the auxiliary means and/or on the inside of the outer wall (14).
    • PCT No.PCT / GB91 / 01902 371日期:1993年4月19日 102(e)日期1993年4月19日PCT 1991年10月30日PCT PCT。 出版物WO92 / 07965 日期:1992年5月14日。冶金枪具有间接冷却系统,与通过中心通道(12)进料至熔体,浴槽等的反应物分开并独立。 外部通道(10)围绕中心通道(12)延伸,并且其外壁(14)暴露于热通量。 冷却剂流过外部通道(10)。 辅助装置(22)位于外部通道(10)内以增强从外壁(14)吸收热量。 冷却剂是两相混合物,优选气体和水。 辅助装置可以是冷却剂流动路径内的螺旋翅片(22)或钢丝填料。 通过(a)由辅助装置提供的延伸的金属表面积和/或(b)沉积在辅助装置和/或外壁(14)的内部上的液体膜的表面蒸发来实现增强的冷却, 。
    • 10. 发明授权
    • Method of effecting a bioreaction
    • 进行生物反应的方法
    • US5021069A
    • 1991-06-04
    • US286944
    • 1988-12-20
    • John G. WhellockJonathan Goodbody
    • John G. WhellockJonathan Goodbody
    • C12M1/04C12M1/08C12P19/06C22B3/18
    • C22B3/18C12P19/06Y02P10/234Y10S423/17
    • A bioreaction is affected by oxygenating a liquid/solids mixture containing a micro-organism to enable the bioreaction to proceed, wherein the said mixture is confined in a reaction vessel and circulated around a loop, the loop including a column in which gas transfer is effected, at least the liquid being introduced into the top of the column in the form of at least one stream, the velocity of which stream is sufficient to generate and maintain, at least in an upper region of the column, a substantially continuous foam formed of close-packed bubbles of the gas in the liquid extending across the entire cross-section of the column, driven to violent agitation and backmixing by the incoming stream of liquid, and of relatively uniform bubble size, the velocity of the inlet stream of liquid and the rate of introduction of the gas being sufficient to prevent gas accumulating at the top of the column.
    • 生物反应受含氧化含有微生物的液体/固体混合物的影响,使得能够进行生物反应,其中所述混合物被限制在反应容器中并在环路周围循环,所述环包括其中进行气体转移的柱 至少将液体以至少一种流的形式引入塔的顶部,其流速足以至少在柱的上部区域中产生并维持由 液体中气体的紧密堆积的气体延伸穿过柱的整个横截面,被液体进入剧烈的搅拌和回混,并具有相对均匀的气泡尺寸,液体入口流的速度和 气体的引入速率足以防止在塔顶积聚的气体。