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1. 发明授权

US5683656A Decreased interference redox detection device 失效
标题翻译：减少干扰氧化还原检测装置
公开(公告)号：US5683656A
公开(公告)日：1997-11-04
申请号：US605746
申请日：1996-02-22
申请人： Klaus Habenstein , Dieter Zopf , Winfried Bursch
发明人： Klaus Habenstein , Dieter Zopf , Winfried Bursch
IPC分类号： G01N21/77 , C07C381/12 , C07C391/00 , C07F9/54 , C07F9/72 , C07F9/74 , C12Q1/26 , C12Q1/28 , G01N21/78 , G01N33/48
CPC分类号： C07F9/723 , C07C381/12 , C07C391/00 , C07F9/5456 , C07F9/743 , C12Q1/26 , C12Q1/28 , Y10T436/144444 , Y10T436/148888
摘要： The present invention relates to reagents and processes for the preparation of diagnostics which use a chromogenic redox detection system and whose chromogenic redox detection system essentially remains unaffected by interference from reducing compounds in the sample material.
摘要翻译：本发明涉及用于制备诊断的试剂和方法，其使用显色氧化还原检测系统，其显色氧化还原检测系统基本上不受样品材料中还原性化合物的干扰的影响。

2. 发明授权

US3497341A Method for desiccating and defoliating plants with arsinic acid derivatives 失效
标题翻译：用氨基酸衍生物去除和去除植物的方法
公开(公告)号：US3497341A
公开(公告)日：1970-02-24
申请号：US3497341D
申请日：1966-05-19
申请人： GAF CORP
发明人： CHIDDIX MAX EUGENE
IPC分类号： C07F9/72 , A01N9/00 , C07F9/70
CPC分类号： C07F9/723

3. 发明授权

US2496240A Diazotypes stabilized with sulfo amino benzoic acids 失效
标题翻译：用磺基氨基苯甲酸稳定的二亚类
公开(公告)号：US2496240A
公开(公告)日：1950-01-31
申请号：US75303447
申请日：1947-06-06
申请人： GEN ANILINE & FILM CORP
发明人： VON GLAHN WILLIAM H , STANLEY LESTER N
IPC分类号： C07F9/72
CPC分类号： C07F9/723

4. 发明授权

US2442372A Method of manufacturing sodium methyl arsonate 失效
标题翻译：制造钠甲基钠的方法
公开(公告)号：US2442372A
公开(公告)日：1948-06-01
申请号：US59030232
申请日：1932-02-01
申请人： US SEC WAR
发明人： MILLER GEORGE E , SEATON SIDNEY G
IPC分类号： C07F9/72
CPC分类号： C07F9/723

5. 发明授权

US2396258A Long chain alpphatic hydrocarbon compounds of arsenic 失效
标题翻译：长链氨基烃类化合物砷
公开(公告)号：US2396258A
公开(公告)日：1946-03-12
申请号：US46781142
申请日：1942-12-03
申请人： FRIEDHEIM ERNST A H
发明人： FRIEDHEIM ERNST A H
IPC分类号： C07F9/72
CPC分类号： C07F9/723

6. 发明授权

US5958906A Phospholipid derivatives containing higher elements of the fifth main group 失效
标题翻译：磷脂衍生物含有较高元素的第五主要组
公开(公告)号：US5958906A
公开(公告)日：1999-09-28
申请号：US852492
申请日：1997-05-07
申请人： Gerhard Nossner , Jurij Stekar, deceased , Peter Hilgard , Bernhard Kutscher , Jurgen Engel
发明人： Gerhard Nossner , Jurij Stekar, deceased , Peter Hilgard , Bernhard Kutscher , Jurgen Engel
IPC分类号： C07F9/72 , A61K31/66
CPC分类号： C07F9/723
摘要： Phospholipid derivatives containing higher elements of the Vth main group (P, As, Sb, Bi), their method of preparation and antineoplastic and antimicrobially active medications that can be prepared from the phospholipid derivatives.
摘要翻译：含有Th2主要组分（P，As，Sb，Bi）的更高元素的磷脂衍生物，它们的制备方法以及可从磷脂衍生物制备的抗肿瘤和抗微生物活性药物。

7. 发明授权

US5756359A Decreased interference redox detection system 失效
标题翻译：干扰氧化还原检测系统减少
公开(公告)号：US5756359A
公开(公告)日：1998-05-26
申请号：US859083
申请日：1997-05-20
申请人： Klaus Habenstein , Dieter Zopf , Winfried Bursch
发明人： Klaus Habenstein , Dieter Zopf , Winfried Bursch
IPC分类号： G01N21/77 , C07C381/12 , C07C391/00 , C07F9/54 , C07F9/72 , C07F9/74 , C12Q1/26 , C12Q1/28 , G01N21/78 , G01N33/48
CPC分类号： C07F9/723 , C07C381/12 , C07C391/00 , C07F9/5456 , C07F9/743 , C12Q1/26 , C12Q1/28 , Y10T436/144444 , Y10T436/148888
摘要： The present invention relates to reagents and processes for the preparation of diagnostics which use a chromogenic redox detection system and whose chromogenic redox detection system essentially remains unaffected by interference from reducing. compounds in the sample material.
摘要翻译：本发明涉及用于制备诊断的试剂和方法，其使用显色氧化还原检测系统，其显色氧化还原检测系统基本上不受来自还原的干扰的影响。样品中的化合物。

8. 发明授权

US4900855A Chemical process for obtaining high purification of monoalkylarsines and dialkylarsines and purified mono- and dialkylarsines 失效
标题翻译：用于获得单烷基胂和二烷基胂和纯化的单烷基和二烷基胂的高纯化的化学方法
公开(公告)号：US4900855A
公开(公告)日：1990-02-13
申请号：US284000
申请日：1988-12-14
申请人： Benjamin C. Hui , Ravindra K. Kanjolia , Jorg Lorberth
发明人： Benjamin C. Hui , Ravindra K. Kanjolia , Jorg Lorberth
IPC分类号： C07F9/72
CPC分类号： C07F9/723
摘要： A method is provided for highly pure mono- and dialkylarsines, particularly removing substantially all silicon-containing impurities. A mono- or dialkylarsine is reacted with either an alkali metal or an alkali metal hydrocarbyl, thereby producing an alkali metal alkylarsenide. Silicon, germanium, zinc and other metallic impurities are removed from the alkali alkylarsenide. Mono- and dialkylarsine is then regenerated by reaction of the alkali metal alkylarsenide with a proton donor.

9. 发明授权

US4734514A Hydrocarbon-substituted analogs of phosphine and arsine, particularly for metal organic chemical vapor deposition 失效
标题翻译：膦和胂的烃取代类似物，特别是用于金属有机化学气相沉积
公开(公告)号：US4734514A
公开(公告)日：1988-03-29
申请号：US828467
申请日：1986-02-10
申请人： Andreas A. Melas , Benjamin C. Hui , Jorg Lorberth
发明人： Andreas A. Melas , Benjamin C. Hui , Jorg Lorberth
IPC分类号： C07C391/00 , C07C395/00 , C07F3/00 , C07F3/02 , C07F3/06 , C07F3/08 , C07F3/12 , C07F5/00 , C07F5/02 , C07F5/06 , C07F9/50 , C07F9/72 , C07F9/90 , C07F9/94 , C23C16/18 , C23C16/30 , C07F9/70
CPC分类号： C07F9/505 , C07C391/00 , C07C395/00 , C07F3/00 , C07F3/02 , C07F3/06 , C07F3/08 , C07F3/12 , C07F5/00 , C07F5/027 , C07F5/06 , C07F9/723 , C07F9/90 , C07F9/94 , C23C16/18 , C23C16/301 , C23C16/306
摘要： Organometallic compounds having the formulas: ##STR1## wherein N is selected from phosphorus and arsenic, H is hydride, and X and Y are independently selected from hydride, lower alkyl cyclopentadienyl, and phenyl, except that Y cannot be hydrogen; andMR.sub.xwherein x is an integer from 2 to 4 inclusive, each said R substituent is independently selected from hydride, lower alkyl, phenyl, alkyl-substituted phenyl, cyclopentadienyl, and alkyl-substituted cyclopentadienyl, and M is selected from elements of Groups 2B, 2A, 3A, 5A, and 6A of the Periodic Table, except carbon, nitrogen, oxygen, and sulfur. The use of these compounds in chemical vapor deposition processes and methods for synthesizing these compounds are also disclosed.
摘要翻译：具有下式的有机金属化合物：其中N选自磷和砷，H是氢化物，X和Y独立地选自氢化物，低级烷基环戊二烯基和苯基，除了Y不能是氢; 和其中x是2至4的整数，其中每个所述R取代基独立地选自氢化物，低级烷基，苯基，烷基取代的苯基，环戊二烯基和烷基取代的环戊二烯基，M选自组2B的元素，2A，3A，5A和6A，除了碳，氮，氧和硫。还公开了这些化合物在化学气相沉积方法中的应用和合成这些化合物的方法。

10. 发明授权

US4529554A Process for the preparation of nickel ylides containing ylide ligands with a sulfonated group V component 失效
公开(公告)号：US4529554A
公开(公告)日：1985-07-16
申请号：US179080
申请日：1980-08-18
申请人： David L. Beach , James J. Harrison
发明人： David L. Beach , James J. Harrison
IPC分类号： B01J31/00 , B01J31/18 , B01J31/22 , B01J31/24 , C07B61/00 , C07C2/36 , C07F9/535 , C07F9/72 , C07F9/74 , C07F9/90 , C07F9/92 , C07F15/04 , C08F110/02
CPC分类号： B01J31/226 , B01J31/2247 , B01J31/2404 , C07C2/36 , C07F15/04 , C07F9/5352 , C07F9/723 , C07F9/743 , C07F9/904 , C07F9/92 , C08F110/02 , B01J2231/20 , B01J2531/847 , B01J2540/32 , B01J31/1895
摘要： A process is provided for preparing nickel ylides which are themselves novel compounds defined by the following Formula I: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3, R.sub.4, R.sub.5, R.sub.6, R.sub.7 and R.sub.8 are either alike or different members selected from the group consisiting of hydrogen, alkyl radicals having from about one to about 24 carbon atoms, preferably from about one to about 10 carbon atoms; aryl radicals having from about six to about 20 carbon atoms, preferably from about six to about 10 carbon atoms; alkenyl radicals having from about two to about 30 carbon atoms, preferably from about two to about 20 carbon atoms; cycloalkyl radicals having from about three to about 40 carbon atoms, preferably from about three to about 30 carbon atoms; aralkyl and alkaryl radicals having from about six to about 40 carbon atoms, preferably from about six to about 30 carbon atoms; a halogen radical selected from the group consisting of fluorine, chlorine, bromine and iodine, preferably chlorine; a hydroxyl group; an alkoxy or aryloxy group; a hydrocarbyl group, such as defined above, carrying halogen, hydroxyl or alkoxy or aryloxy; and a sulfonato group (--SO.sub.3 .sup.-) or an alkyl, aryl, alkenyl, cycloalkyl, aralkyl or alkaryl group carrying a sulfonato group; provided that at least one of R.sub.1, R.sub.2 and R.sub.3 is a sulfonato group or an alkyl, aryl, alkenyl, cycloalkyl, aralkyl or alkaryl, as defined above, carrying a sulfonato group; M is sulfur or oxygen, preferably oxygen; E is phosphorus, arsenic, antimony or nitrogen, preferably phosphorus; and F is phosphorus, arsenic or antimony, preferably phosphorus. The process comprises reacting a ligand defined by the following formula: ##STR2## with an alpha-substituted ketone or aldehyde or an alpha-substituted thioketone or thioaldehyde defined by the following formula: ##STR3## to obtain the metal salt defined by the following Formula II: ##STR4## wherein R.sub.1, R.sub.2, R.sub.3, R.sub.7, R.sub.8, F and M are as defined above and X is a halogen radical selected from the group consisting of fluorine, chlorine, bromine and iodine, preferably chlorine and bromine, a tosyl group (a tolune sulfonate group), or an acetate group. This metal salt is reacted with a base to obtain the novel ylide defined by the following Formula III: ##STR5## wherein R.sub.1, R.sub.2, R.sub.3, R.sub.7, R.sub.8, F and M are as defined above. This ylide is then reacted with (1) a zero valent nickel compound or any nickel compound convertible to a zero valent nickel compound in situ and (2) a ligand having the formula: ##STR6## wherein R.sub.4, R.sub.5, R.sub.6 and E are as defined above.

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