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1. 发明授权

US09056881B2 Process for the preparation of phosphinic acid esters 有权
标题翻译：次膦酸酯的制备方法
公开(公告)号：US09056881B2
公开(公告)日：2015-06-16
申请号：US14382344
申请日：2013-02-12
申请人： Merck Patent GmbH
发明人： Nikolai Mykola Ignatyev , Michael Schulte , Christoph Alexander Jablonka , Karsten Koppe , Walter Frank
IPC分类号： C07F9/32 , C07F9/6571
CPC分类号： C07F9/3205 , C07F9/3211 , C07F9/3264 , C07F9/327 , C07F9/3282 , C07F9/657163
摘要： The invention relates to a process for the preparation of alkyl phosphinates, alkenyl phosphinates, alkynyl phosphinates or phenyl phosphinates by reaction of a corresponding phosphine oxide with an alcohol or phenol in the presence of alkali-metal fluoride or tetraalkylammonium fluoride.
摘要翻译：本发明涉及通过在碱金属氟化物或四烷基氟化铵存在下，通过相应的氧化膦与醇或苯酚的反应来制备烷基次膦酸酯，次膦酸烷基酯，炔基次膦酸酯或苯基次膦酸酯的方法。

2. 发明申请

US20150045572A1 PROCESS FOR THE PREPARATION OF PHOSPHINIC ACID ESTERS 有权
标题翻译：制备磷酸酯的方法
公开(公告)号：US20150045572A1
公开(公告)日：2015-02-12
申请号：US14382344
申请日：2013-02-12
申请人： MERCK PATENT GmbH
发明人： Nikolai Mykola Ignatyev , Michael Schulte , Christoph Alexander Jablonka , Karsten Koppe , Walter Frank
IPC分类号： C07F9/32 , C07F9/6571
CPC分类号： C07F9/3205 , C07F9/3211 , C07F9/3264 , C07F9/327 , C07F9/3282 , C07F9/657163
摘要： The invention relates to a process for the preparation of alkyl phosphinates, alkenyl phosphinates, alkynyl phosphinates or phenyl phosphinates by reaction of a corresponding phosphine oxide with an alcohol or phenol in the presence of alkali-metal fluoride or tetraalkylammonium fluoride.
摘要翻译：本发明涉及通过在碱金属氟化物或四烷基氟化铵存在下，通过相应的氧化膦与醇或苯酚的反应来制备烷基次膦酸酯，次膦酸烷基酯，炔基次膦酸酯或苯基次膦酸酯的方法。

3. 发明授权

US3077431A Phosphinothioates 失效
标题翻译：膦酸硫代磷酸酯
公开(公告)号：US3077431A
公开(公告)日：1963-02-12
申请号：US233760
申请日：1960-01-14
申请人： MONSANTO CHEMICALS
发明人： BAKER JOSEPH W , NEWALLIS PETER E , CHUPP JOHN P
IPC分类号： C07F9/32
CPC分类号： C07F9/327

4. 发明授权

US3059017A Organic esters of polyphosphorus compounds 失效
标题翻译：多磷化合物的有机酯
公开(公告)号：US3059017A
公开(公告)日：1962-10-16
申请号：US7141860
申请日：1960-11-25
申请人： MONSANTO CHEMICALS
发明人： DEVER JAMES L , BIRUM GAIL H
IPC分类号： C07F9/113 , C07F9/143 , C07F9/32 , C07F9/40 , C07F9/6574 , C08K5/5313 , C08K5/5397
CPC分类号： C08K5/5397 , C07F9/113 , C07F9/143 , C07F9/327 , C07F9/40 , C07F9/4078 , C07F9/65742 , C08K5/5313

5. 发明授权

US09647294B2 Non-aqueous electrolytic solution, electrochemical element using same, and alkynyl compound used therefor 有权
公开(公告)号：US09647294B2
公开(公告)日：2017-05-09
申请号：US13576182
申请日：2011-02-02
申请人： Koji Abe , Kazuhiro Miyoshi , Masahide Kondo
发明人： Koji Abe , Kazuhiro Miyoshi , Masahide Kondo
IPC分类号： H01M10/056 , C07C309/70 , C07C309/68 , C07C309/67 , H01M10/0567 , H01M10/052 , C07F9/113 , C07F9/32
CPC分类号： H01M10/0567 , C07C309/67 , C07F9/113 , C07F9/327 , H01M10/052 , H01M2300/0025 , Y02E60/122 , Y02T10/7011
摘要： The present invention provides an excellent nonaqueous electrolytic solution capable of improving low-temperature and high-temperature cycle properties and load characteristics after high-temperature charging storage, an electrochemical element using it, and an alkynyl compound used for it.The nonaqueous electrolytic solution of the present invention comprises containing at least one alkynyl compound represented by the following general formula (I) in an amount of from 0.01 to 10% by mass in the nonaqueous electrolytic solution. R1(O)n—X1—R2 (I) (In the formula, X1 represents a group —C(═O)—, a group —C(═O)—C(═O)—, a group —S(═O)2—, a group —P(═O) (—R3)—, or a group —X3—S(═O)2O—. R1 represents an alkenyl group, a formyl group, an alkyl group, an acyl group, an arylcarbonyl, an alkanesulfonyl group, an alkynyloxysulfonyl group, an arylsulfonyl group, a dialkylphosphoryl group, an alkyl(alkoxy)phosphoryl group, or a dialkoxyphosphoryl group; R2 represents an alkynyl group or an alkynyloxy group; R3 represents an alkyl group, an alkenyl group, an alkynyl group, an aryl group, an alkoxy group, an alkenyloxy group, an alkynyloxy group, or an aryloxy group; n indicates 0 or 1.

6. 发明授权

US09546189B2 Surface modified lithium titanate and preparation method thereof 有权
标题翻译：表面改性钛酸锂及其制备方法
公开(公告)号：US09546189B2
公开(公告)日：2017-01-17
申请号：US14072445
申请日：2013-11-05
申请人： Ningde Amperex Technology Ltd.
发明人： Chuanmiao Yan , Kaifu Zhong
IPC分类号： C07F9/09 , C07F9/28 , H01M4/60 , C07F9/53 , C07F9/32 , C07F9/40 , H01M4/36 , H01M4/485 , H01M4/62 , H01M4/131 , H01M10/42
CPC分类号： C07F9/091 , C07F9/3211 , C07F9/327 , C07F9/4006 , C07F9/4015 , C07F9/5304 , H01M4/131 , H01M4/366 , H01M4/485 , H01M4/62 , H01M10/4235 , Y02E60/122
摘要： A surface modified lithium titanate and preparation method thereof is provided. In the surface modified lithium titanate, the deactivating groups distributed on the surface of the lithium titanate are —O—P—RR′R″, —O—P—(OR)R′R″, —O—P—(OR)(OR′)R″, and —O—P—(OR)(OR′)(OR″), where R, R′ and R″ are identical or different C1˜C8 alkyl or alkenyl groups. The deactivating groups are bonded to the lithium titanate via a bond or a bridge. The exemplary surface modified lithium titanate can effectively lower its catalytic activity, reduce the gassing of lithium ion batteries, and therefore improve the high temperature storage and high temperature cycle performance of lithium titanate batteries. The exemplary preparation method is simple, has great repeatability, a low cost, low pollution to the environment, and is suitable for industrial production.
摘要翻译：提供了表面改性的钛酸锂及其制备方法。在表面改性的钛酸锂中，分布在钛酸锂表面上的失活基团是-O-P-RR'R“，-O-P-（OR）R'R”，-O-P-（OR）（OR'）R“和-O-P-（OR）（OR'）（OR”），其中R，R'和R“是相同或不同的C 1-8烷基或链烯基。失活基团通过键或桥键合到钛酸锂上。表面改性的钛酸锂可以有效地降低其催化活性，减少锂离子电池的放气，从而改善钛酸锂电池的高温储存和高温循环性能。制备方法简单，重复性好，成本低，对环境污染低，适合工业生产。

7. 发明授权

US08912124B2 Use of derivatives of (1-cyanocyclopropyl)phenylphosphinic acid, esters thereof and/or salts thereof for enhancing tolerance in plants to abiotic stress 有权
标题翻译：（1-氰基环丙基）苯基次膦酸的衍生物，其酯和/或其盐用于增强植物对非生物胁迫的耐受性
公开(公告)号：US08912124B2
公开(公告)日：2014-12-16
申请号：US13081309
申请日：2011-04-06
申请人： Lothar Willms , Hans-Joachim Zeiβ , Marco Busch , Christopher Hugh Rosinger , Ines Heinemann , Isolde Häuser-Hahn , Martin Jeffrey Hills , Pascal Von Koskull-Döring
发明人： Lothar Willms , Hans-Joachim Zeiβ , Marco Busch , Christopher Hugh Rosinger , Ines Heinemann , Isolde Häuser-Hahn , Martin Jeffrey Hills , Pascal Von Koskull-Döring
IPC分类号： A01N57/22 , C07F9/58 , C07F9/30 , C07F9/32
CPC分类号： A01N57/22 , C07F9/304 , C07F9/3229 , C07F9/3264 , C07F9/327 , C07F9/3276 , C07F9/3288 , C07F9/58
摘要： The invention relates to derivatives of (1-cyanocyclopropyl)phenylphosphinic acid of the formula (I) and to salts thereof, of the formula (II), for enhancing stress tolerance in plants to abiotic stress, preferably to drought stress, especially for enhancing plant growth and/or for increasing plant yield.
摘要翻译：本发明涉及式（I）的（1-氰基环丙基）苯基次膦酸衍生物及其式（II）的盐，用于增强植物对非生物胁迫的胁迫耐受性，优选干旱胁迫，特别是用于增强植物生长和/或提高植物产量。

8. 发明授权

US3904711A Preparing unsymmetrical dithiophosphonic acid diesters 失效
标题翻译：制备不对称二硫代磷酸二酯
公开(公告)号：US3904711A
公开(公告)日：1975-09-09
申请号：US17131171
申请日：1971-08-12
申请人： EXXON RESEARCH ENGINEERING CO
发明人： OSWALD ALEXIS A , SCHMIT GEORGE N
IPC分类号： A01N57/18 , C07F9/32 , C07F9/40 , A01N9/36 , C10M1/48
CPC分类号： C07F9/327 , A01N57/18 , C07F9/4075
摘要： Dithiophosphonic and dithiophosphinic acid esters can be prepared by free radical addition of the corresponding dithiophosphonic and dithiophosphinic acids to unsaturated compounds, such as olefinic and acetylene compounds, e.g. vinyl chloride, butadiene, allene, methylacetylene, etc. The unsaturated products of this novel process can be further reacted with a sulfhydryl containing compound such as methanethiol, O,O''-diethyl dithiophosphoric acid to provide SH addition thereto. Furthermore, both the dithiophosphonate adducts of the free radical addition process and also the dithiophosphonate adducts of the sulfhydryl containing compound addition step can be isomerized to form unsymmetrical dithiophosphonic acid S,S''diesters. In addition thereto the unsaturated unsymmetrical dithiophosphonic acid S,S''-diesters can also be further reacted with a sulfhydryl containing compound to provide SH addition thereto. The novel thiophosphonic and thiophosphinic compounds produced by the above described processes are useful as pesticides, particularly as insecticides, nematocides and lubricating oil additive such as antioxidants, etc.
摘要翻译：二硫代膦酸和二硫代次膦酸酯可以通过相应的二硫代膦酸和二硫代次膦酸对不饱和化合物例如烯属和乙炔化合物例如，氯乙烯，丁二烯，丙烯，甲基乙炔等

9. 发明授权

US3742098A Process for the preparation of s-vinylic esters of thiophosphorus acids 失效
标题翻译：制备硫代酸的S-乙酸酯的方法
公开(公告)号：US3742098A
公开(公告)日：1973-06-26
申请号：US3742098D
申请日：1969-07-07
申请人： EXXON RESEARCH ENGINEERING CO
发明人： OSWALD A , LESSER J
IPC分类号： C08F30/00 , A01N57/02 , A01N57/12 , A01N57/22 , B01J31/00 , C07B61/00 , C07F9/173 , C07F9/32 , C07F9/40 , C08F30/02 , C07F9/16 , A01N9/36
CPC分类号： C07F9/3264 , C07F9/173 , C07F9/327 , C07F9/4078
摘要： Phosphoryl disulfides can be added to acetylenes to form Svinylic thiophosphate esters. The additions occur by way of a free radical mechanism in the presence of radiation and/or chemical initiators. The adducts are highly effective as pesticides.
摘要翻译：可将磷酰二硫化物加入到乙炔中以形成S-乙烯基硫代磷酸酯。在辐射和/或化学引发剂存在下，通过自由基机理进行添加。加合物作为杀虫剂非常有效。

10. 发明授权

US3658953A Process for the preparation of substituted vinyl esters of acids of phosphorus 失效
标题翻译：磷酸酯取代的乙烯基酯的制备方法
公开(公告)号：US3658953A
公开(公告)日：1972-04-25
申请号：US3658953D
申请日：1969-01-21
申请人： SHELL OIL CO
发明人： POEL DIRK E , MEDEMA DIRK , HELDEN ROBERT VAN , FEKKES NANNO , BERGMAN ELLIOT , WOOD JACK
IPC分类号： A01N57/06 , C07C45/46 , C07C45/63 , C07C49/80 , C07F9/02 , C07F9/113 , C07F9/173 , C07F9/32 , C07F9/38 , C07F9/40 , C07F9/6574 , C07D105/04 , C07F9/08
CPC分类号： C07F9/113 , A01N57/06 , C07C45/46 , C07C45/63 , C07C49/80 , C07F9/02 , C07F9/173 , C07F9/327 , C07F9/4078
摘要： VINYL ESTERS OF PHOSPHORUS ACIDS HAVING BIOLOGICAL ACTIVITY AS PESTICIDES ARE PREPARED BY REACTING DIALKYL PHOSPHITES OR THIOPHOSPHITES AND/OR MONOALKYL PHOSPHONITES, SECONDARY PHOSPHINE OXIDES AND THEIR CORRESPONDING THIO-ANALOGUES WITH AN ALPHA-HALOKETONE IN THE PRESENCE OF A BASE SUCH AS GASEOUS AMMONIA AND DI- OR TRIALKYL AMINES. THE AMOUNT OF BASE USED IS AT LEAST 0.5 GRAM EQUIVALENTS OF BASE PER MOLE OF ALPHA-HALOKETONE.

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