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1. 发明授权

US09981997B2 Chemical reagents for attaching affinity molecules on surfaces 有权
公开(公告)号：US09981997B2
公开(公告)日：2018-05-29
申请号：US15033004
申请日：2014-10-28
申请人： ARIZONA BOARD OF REGENTS ON BEHALF OF ARIZONA STATE UNIVERSITY
发明人： Peiming Zhang , Subhadip Senapati , Saikat Manna
IPC分类号： C07C317/00 , C07C247/04 , C07F7/18 , C07F7/10 , C07C315/00 , C07C317/28 , C07F7/04 , C07K5/12 , C12N15/115 , G01Q70/18 , G01Q60/42
CPC分类号： C07F7/1804 , C07C315/00 , C07C317/28 , C07F7/045 , C07F7/10 , C07F7/1876 , C07K5/126 , C12N15/115 , C12N2310/16 , C12N2310/351 , C12N2310/3517 , G01Q60/42 , G01Q70/18
摘要： Chemical linkage reagents, methods of making and method of using the same are provided. Chemical linkage reagents according to at least some of the embodiments of the present disclosure may be incorporated into or operatively-linked with affinity molecules for attachment to silicon oxide surfaces to, for example, measure interactions between an affinity molecule and its targeting biomolecules.

2. 发明申请

US20170313726A1 BIODEGRADABLE HYBRID POLYMERS USABLE IN MEDICAL TECHNOLOGY OR IN BIOLOGY, STARTING SILANES THEREFOR, AND PREPARATION PROCESS THEREFOR AND USES THEREOF 审中-公开
公开(公告)号：US20170313726A1
公开(公告)日：2017-11-02
申请号：US15509373
申请日：2015-08-28
申请人： Fraunhofer-Gesellschaft Zur Forderung der Angewandten Forschung E.V.
发明人： Herbert WOLTER , Somchith NIQUE , Kerstin OBEL
IPC分类号： C07F7/04 , C08G77/02 , C08G77/00
CPC分类号： C07F7/045 , C07F7/0834 , C08G77/02 , C08G77/20 , C08G77/70
摘要： The invention relates to a silane or silane mixture obtainable by reacting a hydrolysable silane of the formula (A): SiR4 in which R is a hydrolytically condensable group or hydroxyl with a compound R*(OH)x where x is 1, 2, 3 or greater 3, where R* has a straight-chain or branched hydrocarbon skeleton which, according to the number x, is monovalent, divalent, trivalent or multivalent, and has a hydrocarbonaceous chain interrupted by at least two —C(O)O— groups, wherein there are a maximum of 8 successive carbon atoms in the individual hydrocarbon units formed by interruptions within this chain and the, or in the case of branched structures at least one, end of the hydrocarbonaceous chain at the opposite end to the sole hydroxyl group or one of the hydroxyl groups bears an organically polymerizable group, wherein the alcohol is otherwise unsubstituted or has further substituents. The invention further relates to an organically modified silica polycondensate formed as a result of hydrolytic condensation of the silane or silane mixture and optionally a subsequent organic polymerization of the organically polymerizable groups, with optional addition of an organic, at least difunctional compound to the silica polycondensate prior to the organic polymerization.

3. 发明申请

US20110200513A1 METHOD FOR PRODUCING MONOSILANE AND TETRAALKOXYSILANE 有权
标题翻译：生产单烷基醚和四羟甲基纤维素的方法
公开(公告)号：US20110200513A1
公开(公告)日：2011-08-18
申请号：US13125606
申请日：2009-10-30
申请人： Hiromoto Ohno , Toshio Ohi , Haruaki Ito , Fanil Makhmutov
发明人： Hiromoto Ohno , Toshio Ohi , Haruaki Ito , Fanil Makhmutov
IPC分类号： C01B33/04
CPC分类号： C07F7/045 , C01B33/00 , C01B33/04 , C01B33/043
摘要： The present invention relates to method for producing monosilane and tetraalkoxysilane comprising subjecting alkoxysilane represented by formula (1) HnSi(OR) 4-n (1) wherein R represents alkyl group having 1 to 6 carbon atoms and n represents an integer of from 1 to 3, to dismutation reaction in a gaseous phase in the presence of a catalyst containing an alkali metal fluoride and a catalyst activator.The method can solve problems in a method for producing monosilane and tetraalkoxysilane by dismutation reaction of alkoxysilane in a liquid phase: i.e. problems such that separation from the solvent is difficult and that the reaction is too slow and not suitable for industrial production.
摘要翻译：本发明涉及制备单硅烷和四烷氧基硅烷的方法，其包括使由式（1）表示的烷氧基硅烷代表HnSi（OR）4-n（1）表示的烷氧基硅烷，其中R表示具有1至6个碳原子的烷基，n表示1的整数， 3，在含有碱金属氟化物和催化剂活化剂的催化剂存在下，在气相中进行歧化反应。该方法可以通过烷基硅烷在液相中的歧化反应来解决生产甲硅烷和四烷氧基硅烷的方法中的问题：即难以与溶剂分离的问题，并且反应太慢并且不适合于工业生产。

4. 发明授权

US07875412B2 Positive electrified charge control agent and positive electrified toner for developing electrostatic image 有权
标题翻译：正电充电控制剂和用于静电图像显影的正极带电调色剂
公开(公告)号：US07875412B2
公开(公告)日：2011-01-25
申请号：US11730446
申请日：2007-04-02
申请人： Osamu Yamate , Masashi Yasumatsu
发明人： Osamu Yamate , Masashi Yasumatsu
IPC分类号： G03G9/097
CPC分类号： G03G9/09741 , C07F7/045 , G03G9/09758
摘要： A positive electrified charge control agent comprising a silicon complex compound of an effective component represented by the following chemical formula (I) and/or chemical formula (II) (in the formula (I) and formula (II), [D-(SO3)2]2− is a bivalent anion of an organic acid having at least two sulfonic acid groups, p is 0 or 1, B is a bonding line when p is 0, B is a carbon atom or a nitrogen atom when p is 1, J is a carbon atom or a nitrogen atom, A is an organic group which forms a ring with (B)p and J, both of R are same or different to each other and are an organic group, and these both of R are independent or form a heterocyclic ring). A positive electrified toner for developing an electrostatic image comprises the positive electrified charge control agent. A charge control method of the positive electrified toner for developing the electrostatic image comprises a step for making the toner positively electrified by friction.
摘要翻译：一种正电荷电荷控制剂，其包含由以下化学式（I）和/或化学式（II）（式（I）和式（II）表示的有效成分的硅配位化合物，[D- ）2] 2-是具有至少两个磺酸基团的有机酸的二价阴离子，p为0或1，B为p为0时的键合线，当p为1时，B为碳原子或氮原子，J为碳原子或氮原子，A为与（B）p和J形成环的有机基团，R均相同或不同，为有机基团，R均为独立或形成杂环）。用于显影静电图像的正极带电调色剂包括正电荷电荷控制剂。用于显影静电图像的正带电调色剂的电荷控制方法包括通过摩擦使调色剂带正电的步骤。

5. 发明申请

US20090149554A1 WATER-SOLUBLE METAL ALCOHOLATE DERIVATIVES, PRODUCTION METHODS THEREOF, AND SOLID GELATINOUS EXTERNAL PREPARATIONS CONTAINING THE SAME 审中-公开
标题翻译：水溶性金属醇盐衍生物，其生产方法和含有其的固体外消旋制剂
公开(公告)号：US20090149554A1
公开(公告)日：2009-06-11
申请号：US12063275
申请日：2006-08-11
申请人： Yuko Ishikawa , Katzutami Sakamoto , Toshikhiko Seki , Isao Yajima , Shun Takahashi , Kei Watanabe
发明人： Yuko Ishikawa , Katzutami Sakamoto , Toshikhiko Seki , Isao Yajima , Shun Takahashi , Kei Watanabe
IPC分类号： A61K47/24 , C07F7/28 , C07F7/02
CPC分类号： C07F7/045 , A61K9/0014 , A61K47/10 , C07C31/20
摘要： The object of the present invention is to provide a production method of water-soluble silane derivatives, the separation and purification of which are easy, and the reaction for which can be conducted under an industrially practicable temperature condition (under the temperature condition of 90° C. or lower) and to provide compounds with which solid gelatinous external preparations, with excellent stability against a temperature change and against an effect of additives and with excellent usability, can be prepared. The water-soluble silane derivative could be formed by the substitution reaction of a metal alkoxide with a polyhydric alcohol under the presence of a solid catalyst. According to this production method, the separation of the catalyst from the product is very easy, and the reaction can be carried out under the temperature condition of 90° C. or lower. The obtained water-soluble metal alcoholate derivative can satisfactory solidify an aqueous formulation of an external preparation by its blending thereinto. The obtained solid gelatinous external preparation has excellent stability against a temperature change and against the effect of additives. In addition, the external preparation is easily disintegrated during use; thus the usability such as easiness to be scooped up with fingers and spreadability during application is excellent.
摘要翻译：本发明的目的是提供一种水溶性硅烷衍生物的制造方法，其分离纯化容易，其反应可以在工业上可行的温度条件下（在90℃的温度条件下进行） C.或更低），并且可以制备具有优异的耐温度变化稳定性和抗添加剂效果以及优异可用性的固体胶状外用制剂的化合物。水溶性硅烷衍生物可以通过金属醇盐与多元醇在固体催化剂存在下的取代反应形成。根据该制造方法，催化剂与产物的分离非常容易，反应可以在90℃以下的温度条件下进行。所得到的水溶性金属醇化物衍生物可以通过其混合来使外用制剂的水性制剂充分固化。所得固体凝胶状外用制剂对温度变化和添加剂的效果具有优异的稳定性。此外，外用制剂在使用过程中容易分解; 因此在使用时易于用手指舀起的可用性和铺展性优异。

6. 发明授权

US07534905B2 Reagents for asymmetric allylation, aldol, and tandem aldol and allyation reactions 有权
标题翻译：不对称烯丙基化，醛醇醛和串联醛醇缩合反应的试剂
公开(公告)号：US07534905B2
公开(公告)日：2009-05-19
申请号：US10504831
申请日：2003-03-03
申请人： James L. Leighton , Xiaolun Wang , James Kinnaird
发明人： James L. Leighton , Xiaolun Wang , James Kinnaird
IPC分类号： C07F7/10 , C07F7/08 , C07F7/18
CPC分类号： C07C403/08 , C07B2200/07 , C07C29/38 , C07C41/30 , C07C43/1787 , C07C43/23 , C07C241/04 , C07C2601/14 , C07F7/045 , C07F7/12 , C07F7/122 , C07F7/1804 , C07F7/1876 , C07F7/188 , C07C243/28 , C07C33/48 , C07C33/03 , C07C33/14 , C07C33/26 , C07C33/30
摘要： A new class of reagents and method of use of the reagents in the reaction of the reagents with electrophilic compounds. The invention in one embodiment is directed to a method for the formation of an alcohol of the formula (I). The method includes reacting a reagent of the formula (II) with an aldehyde of the formula R10CHO to form the alcohol. X3 is one of O and C(R4)(R5). Each of X1 and X2 is independently O or N—R. Each of Ca and Cb is independently an achiral center, an (S) chiral center or an (R) chiral center. Ra and Rb are (i) each independently C1-10 alkyl, C6-10 aryl or C3-9 heteroaryl, or (ii) taken together to form a C3—C4 alkylene chain which together with Ca and Cb forms a 5-membered or 6-membered aliphatic ring. Rc and Rd are each independently hydrogen, C1-10 alkyl, C6-10 aryl or C3-9 heteroaryl. R is C1-10 alkyl, C6-10 aryl or C3-9 heteroaryl. Each of R1, R2, R3, R4, R5 is independently hydrogen, C1—C10 alkyl, C6-10 aryl, C3-9 heteroaryl, C1-10 alkoxy, C6-10 aryloxy, C1-10 dialkylamino, C1-10 alkyl-C6-10 arylamino, C1-10 diarylamino, or halogen. R6 is halogen, hydrogen, C1-10 alkyl, C6-10 aryl, C3-9 heteroaryl, C1-10 alkoxy, C6-10 aryloxy, C1-10 alkyl-C6-10 arylamino, C1-10 diarylamino, OSO2CF3 or SR. R10 may be C1-10 alkyl, C6-10 aryl, or C3-9 heteroaryl.
摘要翻译：在试剂与亲电子化合物的反应中使用新一类试剂和试剂的使用方法。在一个实施方案中，本发明涉及形成式（I）的醇的方法。该方法包括使式（II）的试剂与式R 10 CHO的醛反应以形成醇。 X3是O和C（R4）（R5）之一。 X1和X2各自独立地为O或N-R。 Ca和Cb各自独立地是非手性中心，（S）手性中心或（R）手性中心。 R a和R b分别为（i）各自独立地为C 1-10烷基，C 6-10芳基或C 3-9杂芳基，或（ii）一起形成C 3 -C 4亚烷基链，其与Ca和Cb一起形成5元或 6元脂肪环。 R c和R d各自独立地为氢，C 1-10烷基，C 6-10芳基或C 3-9杂芳基。 R是C 1-10烷基，C 6-10芳基或C 3-9杂芳基。 R 1，R 2，R 3，R 4，R 5各自独立地为氢，C 1 -C 10烷基，C 6-10芳基，C 3-9杂芳基，C 1-10烷氧基，C 6-10芳氧基，C 1-10二烷基氨基，C 1-10烷基 - C6-10芳基氨基，C1-10二芳基氨基或卤素。 R6是卤素，氢，C1-10烷基，C6-10芳基，C3-9杂芳基，C1-10烷氧基，C6-10芳氧基，C1-10烷基-C6-10芳基氨基，C1-10二芳基氨基，OSO2CF3或SR。 R 10可以是C 1-10烷基，C 6-10芳基或C 3-9杂芳基。

7. 发明申请

US20070255067A1 PROCESS FOR PRODUCTION OF TRIALKOXYHALOSILANES 有权
标题翻译：生产试验羧甲基纤维素的方法
公开(公告)号：US20070255067A1
公开(公告)日：2007-11-01
申请号：US11751304
申请日：2007-05-21
申请人： Motozo Yoshikiyo , Yasuhiro Tanaka , Toshikazu Machida , Hiroshi Sato , Nobuyuki Kuroda , Mitsumasa Tsugawa , Sanae Hatakenaka , Mikio Fujimoto
发明人： Motozo Yoshikiyo , Yasuhiro Tanaka , Toshikazu Machida , Hiroshi Sato , Nobuyuki Kuroda , Mitsumasa Tsugawa , Sanae Hatakenaka , Mikio Fujimoto
IPC分类号： C07F7/02
CPC分类号： C07F7/045 , C07F7/025 , C08F10/00 , C08F4/6574
摘要： A process for the production of trialkoxyhalosilanes which comprises reacting a tetrahalosilane [37] with a tetra-alkoxysilane [38] in the presence of an alcohol whose alkoxy group is the same as those of the tetraalkoxysilane to thereby obtain a trialkoxyhalosilane [39], characterized in that the alcohol is used in an amount of 5 to 50% by mole based on the total amount of Si of the tetrahalosilane and the tetraalkoxysilane: SiX4[37] (wherein X is halogeno) Si(OR1)4[38] (wherein R1 is a hydrocarbon group having 1 to 6 carbon atoms) XSi(OR1)3[39] (wherein X and R1 are each as defined above).
摘要翻译：一种制备三烷氧基卤代硅烷的方法，包括四烷基硅烷[37]与四烷氧基硅烷[38]在醇的存在下，其烷氧基与四烷氧基硅烷相同，得到三烷氧基卤代硅烷[39]，其特征在于其中醇的用量相对于四卤代硅烷和四烷氧基硅烷的总量为5〜50摩尔％：SiX 4 [其中，X为卤素原子）Si（（其中R 1是具有1至6个碳原子的烃基）XSi（OR 1） 3，其中X和R 1各自如上所定义）。

8. 发明申请

US20070117893A1 Radiation absorbing compositions, methods and articles incorporating such compositions 失效
标题翻译：含有这些组合物的辐射吸收组合物，方法和制品
公开(公告)号：US20070117893A1
公开(公告)日：2007-05-24
申请号：US11451028
申请日：2006-06-12
申请人： Keith Keller , Daniel Connor , John Lever
发明人： Keith Keller , Daniel Connor , John Lever
IPC分类号： C08K5/00
CPC分类号： C07F9/005 , C07C215/82 , C07C251/22 , C07F7/04 , C07F7/045 , C07F7/1804
摘要： Infrared (IR) radiation absorbing compounds of metal or metalloids with ligands are beneficial for many applications. Schiff base biquinone (SBB) ligands surrounding a metal or metalloid center may be used for laser welding applications, as one example, wherein effective infared radiation absorption and heat resistance are required. These compounds may be known as Schiff base biquinone metal complexes (SBBC's). The compositions and methods of this invention provide examples of many different NIR absorbing compounds that exhibit high NIR absorbing strength, good thermal stability, and relatively low visible color. The IR absorbing compounds may employ one or more of the following elements: Si, Zr, Bi, Sb, Ce, Cs, K, Mo.
摘要翻译：具有配体的金属或准金属的红外（IR）辐射吸收化合物对于许多应用是有益的。围绕金属或准金属中心的席夫碱双醌（SBB）配体可用于激光焊接应用，作为一个例子，其中需要有效的辐射吸收和耐热性。这些化合物可以称为席夫碱双醌金属络合物（SBBC's）。本发明的组合物和方法提供了具有高NIR吸收强度，良好的热稳定性和相对低的可见颜色的许多不同的近红外吸收化合物的实例。 IR吸收化合物可以采用以下元素中的一种或多种：Si，Zr，Bi，Sb，Ce，Cs，K，Mo。

9. 发明授权

US07169872B2 Hybrid silicon-containing coupling agents for filled elastomer compositions 有权
标题翻译：用于填充弹性体组合物的混合含硅偶联剂
公开(公告)号：US07169872B2
公开(公告)日：2007-01-30
申请号：US10137463
申请日：2002-04-30
申请人： Richard W. Cruse
发明人： Richard W. Cruse
IPC分类号： C08G77/08
CPC分类号： C08K5/5415 , B60C1/00 , C07F7/045 , C07F7/1804 , C08K5/48 , C08K5/549 , C08L21/00
摘要： This invention describes novel chemical compounds whose structures are hybrids between sulfur-containing and non-sulfur-containing silanes wherein the two types of silanes are linked by siloxane bonds. The invention includes methods of preparation for the hybrid silanes as well as their use in filled rubbers as coupling agents. The hybrid silanes described are unique in that a certain amount of water in their preparation leads to superior performance in their intended application, and that they can thus be produced more efficiently and safely than coupling agents currently used in the art, from readily available hydrated raw materials.
摘要翻译：本发明描述了新型化合物，其结构是含硫和不含硫的硅烷之间的杂化物，其中两种类型的硅烷通过硅氧烷键连接。本发明包括制备混合硅烷的方法以及它们在填充橡胶中作为偶联剂的用途。所描述的混合硅烷是独特的，因为其制备中的一定量的水导致其预期应用中的优异性能，因此可以比现有技术中所用的偶联剂从易得的水合原料材料

10. 发明申请

US20050059835A1 Methods of refining silane compounds 审中-公开
标题翻译：硅烷化合物的精制方法
公开(公告)号：US20050059835A1
公开(公告)日：2005-03-17
申请号：US10938809
申请日：2004-09-10
申请人： Suzanne Wassmann-Wilken , Christian Werner , Joerg Wilken , Andreas Kanschik-Conradsen
发明人： Suzanne Wassmann-Wilken , Christian Werner , Joerg Wilken , Andreas Kanschik-Conradsen
IPC分类号： C07F7/04 , C07F7/18 , C07F7/20
CPC分类号： C07F7/20 , C07F7/045 , C07F7/1804
摘要： Provided are methods of producing refined silane compounds comprising providing a starting composition comprising a silane ester and an acidic halide and contacting the starting composition with an alkali metal salt selected from the group consisting of alkali metal salts derived from amides, imides, oxazolidinones, amines, sulfonamides, and combinations of two or more thereof.
摘要翻译：提供了生产精制硅烷化合物的方法，包括提供包含硅烷酯和酸性卤化物的起始组合物，并使起始组合物与选自酰胺，酰亚胺，恶唑烷酮，胺的碱金属盐，磺酰胺，以及其两种或更多种的组合。

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